Emerson Rosemount 396/396VP/397/398/398VP pH/ORP Sensors Instruction Manual

Instruction Manual LIQ-MAN-396-396VP-397-398-398VP Rev. M March 2017 Rosemount™ 396/396VP/397/398/398VP pH/ORP Sensors hasgkas Essential Instructions Read this page before proceeding! Emerson designs, manufactures and tests its products to meet many national and international standards. Because these sensors are sophisticated technical products, you MUST properly install, use, and maintain them to ensure they continue to operate within their normal specifications. The following instructions MUST be adhered to and integrated into your safety program when installing, using, and maintaining Rosemount products. Failure to follow the proper instructions may cause any one of the following situations to occur: loss of life; personal injury; property damage; damage to this sensor; and warranty invalidation. • Read all instructions prior to installing, operating, and servicing the product. • If you do not understand any of the instructions, contact your Emerson representative for clarification. • Follow all warnings, cautions, and instructions marked on and supplied with the product. • Inform and educate your personnel in the proper installation, operation, and maintenance of the product. • Install your equipment as specified in the Installation Instructions of the appropriate Instruction Manual and per applicable local and national codes. Connect all products to the proper electrical and pressure sources. • To ensure proper performance, use qualified personnel to install, operate, update, program, and maintain the product. • When replacement parts are required, ensure that qualified people use replacement parts specified by Emerson. Unauthorized parts and procedures can affect the product's performance, place the safe operation of your process at risk, and VOID YOUR WARRANTY. Third-party substitutions may result in fire, electrical hazards, or improper operation. • Ensure that all equipment doors are closed and protective covers are in place, except when maintenance is being performed by qualified persons, to prevent electrical shock and personal injury. The information contained in this document is subject to change without notice. DANGER Hazardous Area InstallationN This sensor is not Intrinsically Safe. or Explosion Proof. Installations near flammable liquids or in hazardous area locations must be carefully evaluated by qualified on site safety personnel. To secure and maintain an intrinsically safe installation, an appropriate transmitter/safety barrier/sensor combi nation must be used. The installation system must be in accordance with the governing approval agency (FM, CSA or BASEEFA/CENELEC) hazardous area classification requirements. Consult your transmitter instruc tion manual for details. Proper installation, operation and servicing of this sensor in a Hazardous Area Instal lation is entirely the responsibility of the user. CAUTION Sensor/Process Application Compatibility The wetted sensor materials may not be compatible with process composition and operating conditions. Application compatibility is entirely the responsibility of the user. About This Document This manual contains instructions for installation and operation of the Rosemount 396, 396VP, 397, 398, and 398VP pH/ORP Sensors. The following list provides concerning all revisions of this document. Rev. Level 0 Date 03/99 A B C D E F G H I J 12/01 2/02 6/02 8/02 10/02 4/03 8/03 3/04 10/04 2/06 K L M 1/07 11/10 03/17 Notes This is the initial release of the product manual. The manual has been reformatted to reflect the Emerson documentation style and updated to reflect any changes in the product offering. Revised wiring diagram on page 24. Added info to page 1. Updated multiple drawings. Added drawing #40105549, rev. D. Revised drawing #40039601, rev. J, on page 10. Revised Model 397 specs on page 2, and revised drawing on page 27. Added Silcore information. Added Xmt wiring drawings. Added 5081 wiring drawing and updated 1055 wiring. Changed drawing 40039603 rev. C, on page 13. Added a note on page 15. Miscellaneous revisions. Removed mention of patents and updated dnv logo. Updated Ordering Information, Wiring Diagrams, Accessories, Emerson Logo and Address. Also, added FM Installation drawing and EC Declaration of Conformity Instruction Manual LIQ-MAN-396-396VP-397-398-398VP Table of Contents March 2017 Contents Section 1: Description and Specifications 1.1 TUpH Features and Applications ..........................................................................1 1.2 Specifications ......................................................................................................3 1.3 Product Certifications ..........................................................................................4 1.4 Ordering Information...........................................................................................6 Section 2: Installation 2.1 First Time Installation ..........................................................................................9 2.2 Unpacking and Inspection .................................................................................10 2.3 Mounting...........................................................................................................10 2.4 Electrical Installation..........................................................................................17 Section 3: Startup and Calibration 3.1 Sensor Preparation ............................................................................................33 3.2 Calibration Using Buffer Solution or Grab Sample...............................................33 Section 4: Maintenance 4.1 Electrode Cleaning.............................................................................................35 4.2 Automatic Temperature Compensator...............................................................36 Section 5: Troubleshooting ..................................................................................37 Section 6: Accessories 6.1 Accessories ........................................................................................................39 EC Declaration of Conformity.............................................................................41 Intrisicallly Safe Sensor Installation Drawing - FM ................................43 Table of Contents i Table of Contents March 2017 ii Instruction Manual LIQ-MAN-396-396VP-397-398-398VP Table of Contents Instruction Manual LIQ-MAN-396-396VP-397-398-398VP Description and Specifications March 2017 Section 1: Description and Specifications 1.1 1.1.1 TUpH Features and Applications The low maintenance and disposable Rosemount 396, 396VP, 397, 398, and 398VP TUpH sensors offer long life and high performance in measuring pH or ORP in aqueous solutions in pipelines, open tanks, or ponds. These TUpH sensors feature a large area reference junction for maximum resistance to process coatings, generally found in dirty, high solid applications. In addition, the secondary helical reference pathway serves as added protection from poisoning ions. The simplified construction, designed with user convenience in mind, does not require electrolyte replenishment or any component replacement. All models feature a large glass bulb for increased resistance to the effects of aging for longer life. Rosemount 396 and 396VP Sensor Features and Applications Rosemount 396/396VP sensors are constructed of polypropylene and stainless steel and are completely sealed by EP (ethylene propylene) to eliminate process intrusion. Sesnors are specially designed for improved life in harsh, dirty applications such as lime slurry waste treatment and paper machine headbox and pigment/dye applications where large quantities of suspended solids are present. Installation is easily achieved through a wide variety of mounting configurations. 1.1.2 Rosemount 397 Sensor Features and Applications 1.1.2 Rosemount 398 and 398VP Sensor Features and Applications The Rosemount 397 is housed in a highly chemical resistant polypropylene body and completely sealed with EP to eliminate process intrusion. The Rosemount 397 body is specifically designed for use with the Quik-Loc Kit which consists of an adapter and coupler. The PEEK (poly etheretherke tone) adapter enables the Rosemount 397 sensor to fit into a 1 in. MNPT Dixon coupler for quick and easy removal without sensor cable twisting. The 316 stain less steel DIxon coupler is sealed with EP an features locking arms. The Quik-Loc Kit is not recommended for use in processes with hazardous, corrosive, or strong oxidizing chemicals due to a risk of spray and bodily hazards. The chemical-resistant construction of Tefzel, titanium, and the TUpH reference junction make the Rosemount 398 and 398VP the ideal sensors for measuring pH in harsh process liquids. Use these sensors to measure pH in sour water strippers, in pulp bleaching towers that use chlorine dioxide, and in process streams containing a variety of organic solvents. Rosemount 398 and 398VP sensors use the highest quality materials to provide superior chemical resistance. The sensors are housed in a titanium tube and features an optional 1 inch MNPT process connector for insertion, submersion, or flow-through applications. The molded Tefzel TUpH construction is offered with a choice of seals (Viton, EPDM, or Kalrez). Description and Specifications 1 Description and Specifications March 2017 Instruction Manual LIQ-MAN-396-396VP-397-398-398VP Figure 1-1: Cross Section Diagram of the TUpH Reference Technology All TUpH sensors are designed with a large area reference junction, helical reference pathway, and an AccuGlass pH glass bulb. This sensor technology ensures superior performance while only requiring minimal maintenance. 2 Description and Specifications Instruction Manual Description and Specifications LIQ-MAN-396-396VP-397-398-398VP 1.2 March 2017 Specifications Table 1-1: Percent linearity over pH pH Range 396, 396VP, 397, 398, 398VP 396, 396VP, 397, 398, 398VP 94% 93% GPHT Hemi 0-2 pH 2-12 pH 99% 12-13 pH Rosemount 396 396VP 0 to 14 pH Measured Ranges Process Connection Temperature Range 95% 92% Table 1-2: Rosemount 396, 396VP, 397, 398 and 398VP Specifications Wetted Materials 98% 97% 13-14 pH Available pH ACCUGLASS Types GPLR Hemi GPHT hemi bulb or GPLR flat bulb 316 SST, Polypropylene, EPDM, glass None, use 1 in. NPT process connector, PN 23166-00 or 23166-01 (sold separately) 0-100 °C (32-212 °F) 100-1136 kPa abs (0-150 psig) Pressure RangeHemi bulb 100-790 kPa abs (0-100 psig) Pressure RangeFlat bulb Rosemount 398 398VP 0 to 14 pH ORP: -1500 mV to 1500 mV GPHT hemi bulb or GPLR flat bulb -- Rosemount 397 0 to 14 pH GPHT hemi bulb None, use 1 in. NPT None, must use Quik-Loc process connector, kit which includes 1 in. PN 23166-00 or 23166-01 MNPT process (sold separately) connection 0-100 °C (32-212 °F) 100-1825 kPa abs (0-250 psig) 100-790 kPa abs (0-100 psig) 0-100 °C (32-212 °F) 100-790 kPa abs (0-100 psig) _ 75 µS/cm, nominal 75 µS/cm, nominal 75 µS/cm, nominal Weight/Shipping Weight Remote 0.45 kg/0.9 kg (1 lb/2 lb) Remote Remote Description and Specifications _ _ Titanium, Tefzel, glass, choice of Kalrez, Viton, or Polypropylene, EP, glass 316 SST, EP, PEEK EPDM (platinum: ORP only) Minimum Conductivity Preamplifier Options Quik-loc Kit 0.45 kg/0.9 kg (1 lb/2 lb) 0.45 kg/0.9 kg (1 lb/2 lb) 1-in. MNPT _ _ 0.45 kg/0.9 kg (1 lb/2 lb) 3 Description and Specifications Instruction Manual March 2017 1.3 LIQ-MAN-396-396VP-397-398-398VP Product Certifications Please see online certificates for further details. Rosemount 396/396VP: IECEx Sensors without preamp (pH and ORP) – Ex ia IIC T4 Ga (-20 °C ≤ Ta ≤ +60 °C) Sensors with SMART preamp (pH only) – Ex ia IIC T4 Ga (-20 °C ≤ Ta ≤ +60 °C) Sensors with standard preamp (396P only) – Ex ia IIC T4 Ga (-20 °C ≤ Ta ≤ +80 °C) or Ex ia IIC T5 Ga (-20 °C ≤ Ta ≤ +40 °C) Per standards IEC60079-0 : 2011, IEC 60079-11 : 2011 ATEX Sensors without preamp (pH and ORP) – Sensors with SMART preamp (pH only) – Sensors with standard preamp (396P only) – II 1 G Ex ia IIC T5 Ga (-20 °C ≤ Ta ≤ +40 °C) II 1 G Ex ia IIC T4 Ga (-20 °C ≤ Ta ≤ +60 °C) II 1 G Ex ia IIC T4 Ga (-20 °C ≤ Ta ≤ +60 °C) II 1 G Ex ia IIC T4 Ga (-20 °C ≤ Ta ≤ +80 °C) or Per standards EN 60079-0: 2012+A11:2013, EN 60079-11:2012 FM See online FM Certificate of Compliance for applicable sensor options: Intrinsically Safe for use in Class I, II, and III, Division 1, Groups A, B, C, D, E, F, and G; Temperature Class T6 Ta = -20 °C to +60 °C Intrinsically Safe for use in Class I, Zone 0, AEx ia IIC T6 Ta = -20 °C to +60 °C Nonincendive for use in Class I, Division 2, Groups A, B, C, and D; Temperature Class T6 Ta = -20 °C to +60 °C Suitable for use in Class II and III, Division 2, Groups E, F, and G; Temperature Class T6 Ta = -20 °C to +60 °C Hazardous (Classified) Locations IS/I,II,III/1/ABCDEFG/T6 Ta = 60 °C - 1400332; Entity; I/0/AEx ia IIC/T6 Ta = 60 °C - 1400332; Entity; NI/I/2/ABCD/T6 Ta = 60 °C; S/II,III/2/EFG/T6 Ta = 60 °C Per standards 3600:1998, 3610:2010, 3611:2004, 3810:2005 CSA See online CSA Certificate of Compliance for applicable sensor options: Sensors with preamp – Intrinsically Safe: Class I, Division 1, Groups ABCD; Class II, Division 1, Groups EFG; Class III; Class I, Division 2, Groups ABCD; Ambient temperature rating -20 °C to +60 °C; Ex ia IIC; T6 Sensors without preamp – Intrinsically Safe and Non-Incendive: Class I, Division 1, Groups ABCD; Class II, Division 1, Groups EFG; Class III; Class I, Division 2, Groups ABCD; Ex ia IIC; T6; Ambient temperature rating -20 °C to +60 °C: (Simple Apparatus) Per standards C22.2 No. 0-10, C22.2 No. 0.4-M2004, C22.2 No. 94-M1991, C22.2 No. 142 – M1987, C22.2 No 157 – M1992, CAN/CSA E60079-0:07, CAN/CSA E60079- 11:02, UL50 11th Ed, UL508 17th Ed, UL913 7th Ed,, UL 60079-0: 2005, UL 60079-11: 2002 4 Description and Specifications Instruction Manual LIQ-MAN-396-396VP-397-398-398VP Description and Specifications March 2017 Rosemount 397/398/398VP: IECEx Ex ia IIC T4 Ga (-20 °C ≤ Ta ≤ +60 °C) Per standards IEC60079-0 : 2011, IEC 60079-11 : 2011 ATEX II 1 G Ex ia IIC T4 Ga (-20 °C ≤ Ta ≤ +60 °C) Per standards EN 60079-0: 2012+A11:2013, EN 60079-11:2012 FM Intrinsically Safe for use in Class I, II, and III, Division 1, Groups A, B, C, D, E, F, and G; Temperature Class T6 Ta = -20 °C to +60 °C Intrinsically Safe for use in Class I, Zone 0, AEx ia IIC T6 Ta = -20 °C to +60˚C Nonincendive for use in Class I, Division 2, Groups A, B, C, and D; Temperature Class T6 Ta = -20 °C to +60 °C Suitable for use in Class II and III, Division 2, Groups E, F, and G; Temperature Class T6 Ta = -20 °C to +60 °C Hazardous (Classified) Locations IS/I,II,III/1/ABCDEFG/T6 Ta = 60 °C - 1400332; Entity; I/0/AEx ia IIC/T6 Ta = 60 °C - 1400332; Entity; NI/I/2/ABCD/T6 Ta = 60 °C; S/II,III/2/EFG/T6 Ta = 60 °C; Entity Parameters Per standards 3600:1998, 3610:2010, 3611:2004, 3810:2005 CSA Intrinsically Safe and Non-Incendive: Class I, Division 1, Groups ABCD; Class II, Division 1, Groups EFG; Class III; Class I, Division 2, Groups ABCD; Ex ia IIC; T6; Ambient temperature rating -20°C to +60°C: (Simple Apparatus) Per standards C22.2 No. 0-10, C22.2 No. 0.4-M2004, C22.2 No. 94-M1991, C22.2 No. 142 – M1987, C22.2 No 157 – M1992, CAN/CSA E60079-0:07, CAN/CSA E60079- 11:02, UL50 11th Ed, UL508 17th Ed, UL913 7th Ed, UL 60079-0: 2005, UL 60079-11: 2002 Description and Specifications 5 Description and Specifications March 2017 1.4 Instruction Manual LIQ-MAN-396-396VP-397-398-398VP Ordering Information The Rosemount 396 pH sensor features either a standard hemi bulb or flat glass electrode. The sensor is housed in a stainless steel body and must be used with a 1 inch MNPT threaded process connector (sold separately). The Rosemount 396 is not available with an integral preamplifier and comes standard with a 15 ft integral cable. Table 1-3: Rosemount 396 ordering information Model Sensor type pH/ORP Sensor 396 Transmitter/TC Compatibility 50 54 3K TC (1) Pt-100 _ 62 No Selection Cable without BNC (2) Cable Option Electrode Option _ No Selection (3) 71 pH - GPHT Flat Glass Typical Model Number: 396-54-62-71 1. 2. 3. For use with legacy transmitter models 1181, 1050, and 1003. For wiring to Rosemount 1056, 1066, 1057, 56, and 5081 transmitters. No selection will configure the sensor with a standard hemi bulb glass electrode. The Rosemount 396VP sensor features a Variopol cable connection for use with a mating Variopol interconnecting cable (sold separately). Table 1-4: Rosemount 396VP ordering information Model 396VP Sensor type pH/ORP Sensor Temperature Compensation 50 54 55 3K TC (1) Pt-100 Pt-100 (for SMART Preamp) (2) _ 71 No Selection (3) pH - GPHT Flat Glass Electrode Option Preamplifier Option _ No Selection 70 SMART Preamplifier (4) Typical Model Number: 396VP-55-71-70 1. 2. 3. 4. 6 For use with legacy transmitter models 1181, 1050, 1003. Must be selected with Option 70 for SMART Preamplifier. No selection will configure the sensor with a standard hemi bulb glass electrode. Must be selected with Option 55. Description and Specifications Instruction Manual LIQ-MAN-396-396VP-397-398-398VP Description and Specifications March 2017 The Rosemount 398 sensor is housed in a titanium tube and made with a Tefzel reference junction. Sensors must be used with a 1 inch MNPT process connector (sold separately). These sensors come with a standard 15 ft. integral cable. A preamplifier must be used if the sensor is installed more than 15 ft. from the connected transmitter. Table 1-5: Rosemount 398 ordering information Model Sensor type 398 pH/ORP Sensor Measuring Electrode Type 10 12 13 pH - GPHT Glass ORP pH - GPLR Flat Glass 30 31 32 EPDM Viton Kalrez 50 54 3K TC (1) Pt-100 O-ring Material Transmitter/TC Compatibility Cable Option _ No Selection 62 Cable without BNC (2) Typical Model Number: 398-10-30-54-62 1. 2. For use with legacy transmitter model 1181. Not available with option 62. If selected with ORP, sensor will not come with TC. For use with Rosemount transmitter models 1056, 1066, 1057, 56, and 5081. Only available with option 54. The Rosemount 398VP sensor features a Variopol cable connection for use with a mating Variopol interconnecting cable (sold separately). Table 1-6: Rosemount 398VP ordering information Model Sensor type 398VP pH/ORP Sensor Measuring Electrode Type 10 12 13 pH - GPHT Glass ORP pH - GPLR Flat Glass 30 31 32 EPDM Viton Kalrez O-ring Material Transmitter/TC Compatibility 50 3K TC (1) 54 Pt-100 Typical Model Number: 398VP-10-30-54 1. For use with legacy transmitter model 1181. If selected with ORP, sensor will not come with TC. Description and Specifications 7 Description and Specifications March 2017 Instruction Manual LIQ-MAN-396-396VP-397-398-398VP The Rosemount 397 pH sensor is housed in a polypropylene body and is designed to be used with the Quik-Loc Kit (sold separately). Table 1-7: Rosemount 397 ordering information Model Sensor type 397 pH/ORP Sensor Preamplifier/Cable 02 Without Integral Preamplifier, 15 ft (4.6 m) Cable 10 12 pH - GPHT Glass ORP 50 54 3K TC (1) Pt-100 Measuring Electrode Type Transmitter/TC Compatibility Other Options _ No Selection 62 Cable without BNC (2) 64 Tefzel Body Material Typical Model Number: 397-02-10-54-62 1. 2. 8 For use with legacy transmitter model 1181. For use with Rosemount transmiter models 1056, 1066, 1057, 56, and 5081. Description and Specifications Instruction Manual LIQ-MAN-396-396VP-397-398-398VP Installation Section 2: Installation 2.1 March 2017 First Time Installation For first time Rosemount 397 installations, using the following guide is recommended: 1. Quik-Loc Mounting (required for all first time installations) 2. Remote Junction Boxes (optional, recommended for sensor to analyzer distances of more than 15 ft) Choose one: PN 23757-00, Quik-Loc Kit: for use in 1 in. tees; insertion depth 1.4 in. (35 mm) Choose one: PN 23555-00 includes preamplifier 3. Extension cables (used with remote junction boxes) Choose one: PN 23646-01, 11 conductor, shielded, prepped PN 9200273, 11 conductor, shielded, unprepped For first time Rosemount 396/396VP/398/398VP installations, using the following guide is recommended: 1. Process Connector Accessories (required for all first time installations with 1-inch process connection threads) Choose one: PN 23166-00, 316 SST, 1 in. x 1 in. NPT process connector, with EPDM O-ring PN 23166-01, Titanium, 1 in. x 1 in. NPT process connector, with EPDM O-ring PN 9510066, Nylon, 1 in. x 1 in. NPT process connector (submersion only) Choose one (optional process connector o-rings) PN 9550220, Kalrez o-ring, 2-214 2. PN 9550099, Viton o-ring, 2-214 Variopol Cable (required for all first time installations) of Models 396VP and 398VP Choose one: PN 24281-00, 15 ft cable with mating VP connector 3. PN 24281-06, 10 ft cable with mating VP connector Mounting Accessories (optional) Choose one: PN 915240-03 PVC flow through tee, 3/4 in. NPT process connection PN 915240-04 PVC flow through tee, 1 in. NPT process connection 4. PN 915240-05 PVC flow through tee, 1 1/2 in. NPT process connection PN 11275-01 Sensor handrail mounting assembly PN 2002011 1-1/2 in. CPVC Tee with 1 in. FNPT connection PN 24091-00 Low Flow Cell Remote Junction Boxes (optional, recommended for sensor to analyzer distances of more than 15 ft) Choose one: PN 23555-00 includes preamplifier 5. Extension cables (used with remote junction boxes) Choose one: PN 23646-01, 11 conductor, shielded, prepped PN 9200273, 11 conductor, shielded, unprepped Installation 9 Installation Instruction Manual March 2017 2.2 LIQ-MAN-396-396VP-397-398-398VP Unpacking and Inspection Inspect the outside of the carton for any damage. If damage is detected, contact the carrier immediately. Inspect the instrument and hardware. Make sure all the items in the packing list are present and in good condition. Notify the factory if any part is missing. If the sensor appears to be in satisfactory condition, proceed to Section 2.2, Mounting. Note: Save the original packing cartons and materials as most carriers require proof of damage due to mishandling, etc. Also, if it is necessary to return the instrument to the factory, you must pack the instrument in the same manner as it was received. Refer to Section 6 for return instructions. If the sensor is to be stored, the vinyl boot should be filled with pH buffer solution and replaced on sensor tip until ready to use. WARNING Glass electrode must be wetted at all times (in storage and in line) to maximize sensor life. 2.3 2.3.1 2.3.2 Mounting Each sensor has been designed to be located in industrial process environments. Temperature and pressure limitations must not be exceeded at any time. A caution or warning label regarding this matter is attached to each sensor. For insertion, transfer the label as shown on label instructions. See Figure 2-2. For submersion applications, first note limits then remove and discard label. Note: Before mounting the sensor, shake down the sensor to remove any air bubbles that may be present at the tip of the pH glass bulb. In most cases, the pH sensor can simply be installed as shipped and readings with an accuracy of ±0.6 pH may be obtained. To obtain greater accuracy or to verify proper operation, the sensor must be calibrated as a loop with its compatible analyzer or transmitter. Flow Through and Insertion Mounting for Rosemount 396, 396VP, 398, and 398VP Sensors. These sensors can be used with a 1 inch MNPT process connector at the front of the sensor for mounting into a 1-1/2 inch tee or the process. See Figure 2-1 for instal lation configurations. Submersion Mounting for Rosemount 396, 396VP, 398, and 398VP Sensors. These sensors also have a 1 inch MNPT process connector available for use on the back of the sensor. Tapered pipe threads in plastic fittings tend to loosen after installation. It is therefore recom mended that Teflon tape be used on the threads and that the tightness of the connection be checked frequently to assure that no loosening has occurred. To prevent rain water or condensation from running into the sensor, a weatherproof junction box is recommended (see Figure 2-4). The sensor cable must be run through a protective conduit for isolation from electrical interference or physical abuse from the process. The sensor should be installed within 80° of vertical, with the electrode facing down. The sensor’s cable should not be run with power or control wiring. 10 Installation Instruction Manual LIQ-MAN-396-396VP-397-398-398VP 2.3.2 Installation March 2017 Quik-Loc Mounting for Rosemount 397 The Quik- Loc mounting is used with the Rosemount 397 sensor only. WARNING Once the Quik-Loc unit is installed the operator should wait for the process to cool to a safe temperature, use the pressure drain valve to relieve all process pressure and observe the pressure on the pressure gauge for proper removal of the sensor without spray or bodily injury. The Quik-Loc kit used with the Rosemount 397 sensor is not recommended for use with hazardous, corrosive, or strong oxidizing chemi cals due to a risk of spray or bodily injury. WARNING It is recommended that a thermometer, drain valve to relieve pressure and pressure gauge be inserted near the Quik-Loc assembly (see Figure 2-5). Wrap the pipe threads of the Twin-Kam Kamloc coupler with Teflon tape before placing it into the process pipe. The coupler can be connected to any 1 in. process connection and must be mounted within 80° of vertical, with the electrode facing down. Once the coupler is in place, the adapter should be positioned onto the back end of the sensor. (See Figure 2-5) Remove the parafilm wrap ping from the two 0-rings on the sensor, grease the o-rings with the lube provided, and feed the sensor cable through the adapter. Once the adapter is slipped over the sensor’s back end, the retaining ring (which is included with every Rosemount 397 sensor) should be installed on the black, grooved, back end of the sensor body. The retaining ring secures the sensor into the adapter. The adapter/sensor assembly is now ready to be inserted into the coupler. With both arms of the coupler in the released position, insert the adapter/sensor assembly into the coupler. Note: The adapter can not be inserted completely or properly unless both arms are in the fully released position (see Figure 2-5). Once the adapter has been properly placed in the coupler, both arms should be positioned in the locked position. A Sur- Loc™ spring arm has been provided on one arm so that the arm cannot be opened until the spring is released. Note: The sensor may obstruct flow through smaller pipes. Once the arms of the coupler have been locked in position, use tamper-evident safety wire on the metal rings of the Twin-Kam arms to prevent unauthorized and/or untrained personnel from using the Quik-Loc unit. WARNING It is the responsibility of each company using the Quik-Loc Kit/ 397 TUpH Sensor to train personnel of the injury risks associated with using a quick-release coupler that is placed in a hot or pressurized process. The Quik-Loc unit should be used only within the pressure and temperature limits stated for the Rosemount 397 sensor in Section 1.2. Installation 11 Installation March 2017 Instruction Manual LIQ-MAN-396-396VP-397-398-398VP Figure 2-1: Recommended Flow Through and Insertion Installation for Rosemount 396, 396VP, 398, and 398VP Sensors 1-1/2 inch Pipe Tee (PN 2002011) with 1 inch threaded connections. Figure 2-2: Recommended Flow-Through and Insertion Installation For Rosemount 397 12 Calibration and Maintenance Instruction Manual LIQ-MAN-396-396VP-397-398-398VP Installation March 2017 Figure 2-3: Dimensional Drawing For Rosemount 396 and 398 Sensors Calibration and Maintenance 13 Installation Instruction Manual March 2017 LIQ-MAN-396-396VP-397-398-398VP Figure 2-4: Rosemount 396VP and 398VP Sensor Dimensional Drawings (Shown with Process Connector) Metal Process Connector PN 23166-xx (xx = 00 for 316 SST and xx = 01 for titanium) can be used for insertion or submersion mounting of Rosemount 396VP/398VP sensors in 1-inch fittings. 14 The metal process connector gives the sensor various insertions depths, depending on where the user locates the compression fitting. Also the threads can be switched to face the cable end of the sensor for connection to submersion pipes. Installation Instruction Manual LIQ-MAN-396-396VP-397-398-398VP Installation March 2017 Figure 2-5: Submersion Installations for Rosemount 396, 396VP, 398, and 398VP Sensors Installation 15 Installation March 2017 Instruction Manual LIQ-MAN-396-396VP-397-398-398VP Figure 2-6: Dimensional Drawings For Rosemount 397 in the Quik-Loc Unit 16 Installation Instruction Manual LIQ-MAN-396-396VP-397-398-398VP 2.4 Installation March 2017 Electrical Installation Rosemount 396, 396VP, 397, 398, and 398VP sensors are for use with a remote preamplifier. Each sensor comes with either a special 15 ft low noise coax cable or a Variopol (VP) connector, which is used with a mating Variopol cable. The cable should be handled carefully, and kept dry and free of corrosive chemicals at all times. Extreme care should be used to prevent the cable from being twisted, damaged or scraped by rough, sharp edges or surfaces. For additional wiring information on this product, please refer to Wiring Diagrams. DANGER DO NOT CONNECT SENSOR CABLE TO POWER LINES. SERIOUS INJURY MAY RESULT. Note: Remove electrical tape or shrink sleeve from gray reference wire before connecting wire to terminal. Figure 2-7: Wiring for Rosemount 396/397/398 to Rosemount 5081-P Installation 17 Installation March 2017 Instruction Manual LIQ-MAN-396-396VP-397-398-398VP Figure 2-8: Wiring for Rosemount 396-54, 397-54, and 398-54 (Pt-100 RTD). For Use With Junction Box (PN 23555-00) and Remote Preamplifier. 18 Installation Instruction Manual LIQ-MAN-396-396VP-397-398-398VP Installation March 2017 Figure 2-9: Wiring for Rosemount 396, 397, and 398. For Use With Model 1181 pH. Installation 19 Installation March 2017 Instruction Manual LIQ-MAN-396-396VP-397-398-398VP Figure 2-10: Wiring for Rosemount 396-54 , 397-54, and 398-54. For Use With Rosemount 54, 54e, 81, 3081, 4081, and 5081. 20 Installation Instruction Manual LIQ-MAN-396-396VP-397-398-398VP Installation March 2017 Figure 2-11: Wiring for Rosemount 396VP and 398VP to Rosemount 3081, 4081, and 5081 through a Remote Junction Box. Installation 21 Installation March 2017 Instruction Manual LIQ-MAN-396-396VP-397-398-398VP Figure 2-12: Rosemount 396-54-62-xx Wiring to Rosemount 1056/1057/56 Transmitters Figure 2-13: Rosemount 396-54-62-xx Wiring to Rosemount 1066 Transmitter 22 Installation Instruction Manual LIQ-MAN-396-396VP-397-398-398VP Installation March 2017 Figure 2-14: Rosemount 396-54-62-xx Wiring to Rosemount 5081 Transmitter Figure 2-15: Rosemount 396VP Wiring for Rosemount 1056/56 Transmitters Installation 23 Installation March 2017 Instruction Manual LIQ-MAN-396-396VP-397-398-398VP Figure 2-16: Rosemount 396VP Wiring for Rosemount 1066 Transmitter Figure 2-17: Rosemount 396VP Wiring for Rosemount 1057 Transmitter 24 Installation Instruction Manual LIQ-MAN-396-396VP-397-398-398VP Installation March 2017 Figure 2-18: Rosemount 396VP Wiring for Rosemount 5081 Transmitter Figure 2-19: Rosemount 396VP-70 Wiring for Rosemount 1066 Transmitter Installation 25 Installation March 2017 Instruction Manual LIQ-MAN-396-396VP-397-398-398VP Figure 2-20: Rosemount 396VP-70 Wiring for Rosemount 1056/1057/56 Transmitters Figure 2-21: Rosemount 397-02-10-54-xx Wiring to Rosemount 1056/1057/56 Transmitter 26 Installation Instruction Manual LIQ-MAN-396-396VP-397-398-398VP Installation March 2017 Figure 2-22: Rosemount 397-02-10-54-xx Wiring to Rosemount 1066 Transmitter Figure 2-23: Rosemount 397-02-10-54-xx Wiring to Rosemount 5081 Transmitter Installation 27 Installation March 2017 Instruction Manual LIQ-MAN-396-396VP-397-398-398VP Figure 2-24: Rosemount 398-xx-xx-xx-62 Wiring to Rosemount 1056/1057/56 Transmitters Figure 2-25: Rosemount 398-xx-xx-xx-62 Wiring to Rosemount 1066 Transmitter 28 Installation Instruction Manual LIQ-MAN-396-396VP-397-398-398VP Installation March 2017 Figure 2-26: Rosemount 398-xx-xx-xx-62 Wiring to Rosemount 5081 Transmitter Figure 2-27: Rosemount 398VP Wiring to Rosemount 1056/56 Transmitters Installation 29 Installation March 2017 Instruction Manual LIQ-MAN-396-396VP-397-398-398VP Figure 2-28: Rosemount 398VP Wiring to Rosemount 1057 Transmitter Figure 2-29: Rosemount 398VP Wiring to Rosemount 5081 Transmitter 30 Installation Instruction Manual LIQ-MAN-396-396VP-397-398-398VP Installation March 2017 Figure 2-30: Rosemount 398VP Wiring to Rosemount 1066 Transmitter Installation 31 Installation March 2017 32 Instruction Manual LIQ-MAN-396-396VP-397-398-398VP Installation Instruction Manual LIQ-MAN-396-396VP-397-398-398VP Startup and Calibration Section 3: Startup and Calibration March 2017 3.1 Sensor Preparation 3.2 Calibration Using Buffer Solution or Grab Sample Shake down the sensor to remove any air bubbles that may be present at the tip of the pH glass bulb. In most cases, the pH sensor can simply be installed as shipped and readings with an accuracy of ±0.6 pH may be obtained. To obtain greater accuracy or to verify proper operation, the sensor must be calibrated as a loop with its compatible analyzer or transmitter. The pH sensor-transmitter loop may be calibrated by submersing the sensor in a buffer solution (standard solutions of known pH values) or in a process grab sample whose pH value maybe checked by a calibrated laboratory or portable pH meter. Please refer to the transmitter instruction manual for proper calibration procedures. Startup and Calibration 33 Startup and Calibration March 2017 34 Instruction Manual LIQ-MAN-396-396VP-397-398-398VP Startup and Calibration Instruction Manual LIQ-MAN-396-396VP-397-398-398VP Section 4: Maintenance Maintenance March 2017 Rosemount 396, 396VP, 397, 398, and 398VP sensors are disposable type sensors and therefore require minimum maintenance. Every sensor should be kept clean and free of debris and sediment at all times. The frequency of cleaning by wiping or brushing with a soft cloth or brush is determined by the nature of the solution being measured. The sensor should be removed from the process periodically and checked in buffer solutions. DANGER SENSOR IS IN PRESSURIZED SYSTEM! May cause spray and bodily injury. Before removing sensor, be absolutely certain that the process pressure is reduced to 0 psig and the process temperature is lowered to a safe level. If the sensor will not calibrate, refer to your transmitter instruction manual for proper test procedures. If it is determined that the sensor has failed, it should be discarded and replaced. 4.1 Electrode Cleaning If the electrode is coated or dirty, clean as follows: 1. Remove the sensor from process. 3. Wash the glass bulb in a strong detergent solution and rinse it in clean water. If this does not clean the glass bulb, go to Step 4. 2. Wipe the glass bulb with a soft, clean, lint free cloth or tissue. If this does not remove the dirt or coating, go to Step 3. (Detergents clean oil and grease; acids remove scale.) CAUTION The solution used during the following check is an acid and should be handled with care. Follow the directions of the acid manufacturer. Wear the proper protective equipment. Do not let the solution come in contact with skin or clothing. If contact with skin is made, immediately rinse with clean water. 4. Wash the glass bulb in a dilute 5% hydro chloric acid solution and rinse with clean water. Soaking the sensor overnight in the acid solution can improve cleaning action. NOTICE Erroneous pH results may occur immediately after acid soak, due to reference junction potential buildup. Replace the sensor if cleaning does not restore sensor operation. Maintenance 35 Maintenance Instruction Manual March 2017 4.2 LIQ-MAN-396-396VP-397-398-398VP Automatic Temperature Compensator The temperature compensator element is temp erature sensitive and can be checked with an ohmmeter. Resistance increases with temperature. The 3K element will read 3000 ohms ±1% at 25°C (77°F) and a Pt-100 will read 110 ohms. Resistance varies with temperature for a 3K and Pt-100 element and can be determined according to Table 42 or the following formula: RT=R0 [l+R1 (T-20)] Where RT = Resistance T = Temperature in °C Refer to Table 4-1 for R0 and R1 values Table 4-1: R0 and R1 Values for Temperature Compensation Elements Temperature Element 3K PT-100 R0 2934 R1 0.0045 107.7 0.00385 Table 4-2: Temperature vs Resistance of Automatic Temperature Compensator Elements Temperature °C 0 2670 20 2934 10 25 30 40 50 60 70 80 90 100 36 3K 2802 3000 3066 3198 3330 3462 3594 3726 3858 3990 Resistance (Ohms) ±1% PT-100 100.0 103.8 107.7 109.6 111.5 115.4 119.2 123.1 126.9 130.8 134.6 138.5 Maintenance Instruction Manual Troubleshooting LIQ-MAN-396-396VP-397-398-398VP March 2017 Section 5: Troubleshooting Table 5-1: Troubleshooting Trouble Meter reads off scale. (Display reads overrange.) Probable Cause T.C. element shorted. Remedy Check T.C. element as instructed in Section 4.2 and replace sensor if defective. Sensor not in process or sample stream is low. Make sure sensor is in process with sufficient sample stream (refer to Section 2.0 for installation details). Open glass electrode. Reference element open - no contact. Display reads between 3 and 6 Electrode cracked. pH regardless of actual pH of solution or sample. Replace sensor. Replace sensor. Replace sensor. Meter or display indication swings or jumps widely in AUTO T.C. Mode. T.C. element shorted. Check T.C. element as instructed in Section 4.2 and replace sensor if defective. T.C. element open. Check T.C. element as instructed in Section 4.2 and replace sensor if defective. Sluggish or slow meter indication for real changes in pH level. Electrode coated. Clean sensor as instructed in Sections 4.1 Replace sensor if cracked. Transmitter cannot be standardized. Electrode coated or cracked. Span between buffers extremely short in AUTO T.C. Mode. Transmitter short spans between two different buffer values. Electrode at end of life. Replace sensor. Clean sensor as instructed in Sections 4.1 Replace sensor if cracked. Electrode at end of life, due to old glass or high Replace sensor. temperature exposure. Coated glass. Clean sensor as instructed in Sections 4.1 Replace sensor if cracked. Note: For any repair or warranty inquiries please contact our Customer Care group. Troubleshooting 37 Troubleshooting March 2017 38 Instruction Manual LIQ-MAN-396-396VP-397-398-398VP Troubleshooting Instruction Manual LIQ-MAN-396-396VP-397-398-398VP Section 6: Accessories 6.1 Accessories March 2017 Accessories Table 6-1: Additional Accessories for Rosemount 396/396VP/398/398VP Sensors Part Number Description 33211-00 Adapter retrofit for PN 915240-04 33046-00 9310100 9310096 Ferrule 1 in., split 316 SS Ferrule, 1 in. Teflon Nut, Swage, 1 in. stainless steel Table 6-2: Additional Accessories for Rosemount 397 Sensor Part Number Description 23753-01 PEEK replacement adapter for Quik-Loc kit (PN 23757-00) 23753-00 9160441 9160447 2002011 PEEK replacement adapter for Quik-Loc kit (PN 23757-01) 1 in. MNPT 316 stainless steel coupler 1 in. EP Gasket for coupler 1-1/2 in. CPVC Tee with 1 in. FNPT Connection Table 6-3: Other Accessories Part Number Description 9210013 Buffer solution, 6.86 pH, 16 oz. 9210012 9210014 2001492 Accessories Buffer solution, 4.01 pH, 16 oz. Buffer solution, 9.18 pH, 16 oz. Stainless Steel Tag, Specify Marking 39 Accessories March 2017 40 Instruction Manual LIQ-MAN-396-396VP-397-398-398VP Accessories Instruction Manual LIQ-MAN-396-396VP-397-398-398VP EC Declaration of Conformity March 2017 EC Declaration of Conformity Note: Please see website for most recent Declaration. EC Declaration of Conformity 41 EC Declaration of Conformity March 2017 42 Instruction Manual LIQ-MAN-396-396VP-397-398-398VP EC Declaration of Conformity FM Installation 13 Ci INCLUDES THE CAPACITANCE OF 500 FEET OF SENSOR CABLE. 396/VP 396R/VP 396P/VP 398R/VP 399/VP 389/VP 385/385+ 1. NO REVISION TO THIS DRAWING IS PERMITTED WITHOUT FM APPROVAL. 2. Umax > Ut; I max > It; (C i OF ALL LOOPS + C CABLE) < Ca ; (L i OF ALL LOOPS + L CABLE) < L a, Pmax OR Pi > P 0. 3. SINGLE MULTI-CHANNEL IS BARRIER OR APPARATUS MUST BE FM APPROVED, 4. SINGLE MULTI-CHANNEL IS BARRIER OR APPARATUS MANUFACTURE'S CONTROL DRAWINGS MUST BE FOLLOWED WHEN INSTALLING THE SYSTEM. IS BARRIER OR EQUIPMENT MAY BE INSTALLED WITHIN THE HAZARDOUS (CLASSIFIED) LOCATION FOR WHICH IT IS APPROVED. 5. INSTALLATION MUST BE IN ACCORDANCE WITH ARTICLE 500 OF THE NEC (ANSI/NFPA 70) AND ANSI/ISA RP 12.6. WARNING: SUBSTITUTION OF COMPONENTS MAY IMPAIR INTRINSIC SAFETY. 6. pH & AMPEROMETRIC SENSORS WITHOUT PREAMPS ARE SIMPLE APPARATUS. 7. CONTROL EQUIPMENT CONNECTED TO THE ASSOCIATED APPARATUS MUST NOT USE OR GENERATE MORE THAN 250V. 8. RESISTANCE BETWEEN INTRINSICALLY SAFE GROUND AND EARTH GROUND MUST BE LESS THAN OR EQUAL TO 1 OHM. 3900/VP 3500/VP 3300HT/VP 3400HT/VP 9. pH/ORP SENSOR MODELS THAT MAY CONTAIN THE PREAMPLIFIER: 10. WARNING: TO PREVENT IGNITION OF FLAMMABLE OR COMBUSTIBLE ATMOSPHERES, DISCONNECT POWER BEFORE SERVICING. 11. THE ENTITY CONCEPT ALLOWS INTECONNECTION OF INTRINSICALLY SAFE APPARATUS WITH ASSOCIATED APPARATUS WHEN THE FOLLOWING IS TRUE: Ui > Uo; Ii > Io; Pi > Po; Co > C i + C CABLE; Lo > Li + L CABLE. 12. COPY REVISIONS TO 1400332 TO pH/ORP SHIPPING MANUALS. ANY FM APPROVED ASSOCIATED APPARATUS HAVING ENTITY PARAMETERS NON-HAZARDOUS (UNCLASSIFIED) AREA MULTIPLE DEVICES, NUMBER IS LIMITED BY REQUIREMENTS TO MEET ALL OTHER IS REQUIREMENTS FOR THE NETWORK) WITH EQUIVALENT HAZARDOUS AREA APPROVALS. FM APPROVED EQUIPMENT (MAY BE ANY FM APPROVED TRANSMITTER FOR DIVISION 1 WITH INTRINSICALLY SAFE OUTPUT PARAMETERS. THIS FM APPROVED DEVICE MUST BE INSTALLED PER ITS INSTALLATION DRAWING. SENSOR HAZARDOUS (CLASSIFIED)AREA 13 INTRISICALLY SA FE DWG NO. 1400332 ENTITY PARAMETERS Ui = 13.1U, Ii = 358mA Pi = 698 mW Ci = 0.967 µF, Li = 0.1mH ZONE 0 ZON E CLASS I, II, III, DIVISION 1, GROUPS A-G T6 Ta = 60°C Instruction Manual LIQ-MAN-396-396VP-397-398-398VP FM Installation March 2017 Intrisicallly Safe Sensor Installation Drawing - FM 43 LIQ-MAN-396-396VP-397-398-398VP Rev. M March 2017 www.Emerson.com/RosemountLiquidAnalysis Youtube.com/user/Rosemount Analyticexpert.com Twitter.com/Rosemount_News facebook.com/Rosemount Emerson 8200 Market Blvd. Chanhassen, MN 55317, USA Tel +1 800 999 9307 Fax +1 952 949 7001 Liquid.CSC@Emerson.com ©2017 Emerson. All rights reserved. The Emerson logo is a trademark and service mark of Emerson Electric Co. Rosemount is a mark of one of the Emerson family of companies. All other marks are the property of their respective owners. The contents of this publication are presented for information purposes only, and while effort has been made to ensure their accuracy, they are not to be construed as warranties or guarantees, express or implied, regarding the products or services described herein or their use or applicability. All sales are governed by our terms and conditions, which are available on request. We reserve the right to modify or improve the designs or specifications of our products at any time without notice.