Emerson 1066 Liquid Analytical Transmitter Instruction Manual

1066 Instruction Manual 1066 Liquid Analytical Transmitter LIQ_MAN_1066 Rev. G December 2014 This page left intentionally blank Essential Instructions Read this page before proceeding Emerson designs, manufactures, and tests its Rosemount Analytical products to meet many national and international standards. Because these instruments are sophisticated technical products, you must properly install, use, and maintain them to ensure they continue to operate within their normal specifications. The following instructions must be adhered to and integrated into your safety program when installing, using, and maintaining Rosemount Analytical products. Failure to follow the proper instructions may cause any one of the following situations to occur: Loss of life; personal injury; property damage; damage to this instrument; and warranty invalidation. • Read all instructions prior to installing, operating, and servicing the product. If this Instruction Manual is not the correct manual, telephone 1-800-854-8257 and the requested manual will be provided. Save this Instruction Manual for future reference. • If you do not understand any of the instructions, contact your Emerson representative for clarification. • Follow all warnings, cautions, and instructions marked on and supplied with the product. • Inform and educate your personnel in the proper installation, operation, and maintenance of the product. • Install your equipment as specified in the Installation Instructions of the appropriate Instruction Manual and per applicable local and national codes. Connect all products to the proper electrical and pressure sources. • To ensure proper performance, use qualified personnel to install, operate, update, program, and maintain the product. • When replacement parts are required, ensure that qualified people use replacement parts specified by Rosemount. Unauthorized parts and procedures can affect the product’s performance and place the safe operation of your process at risk. Look alike substitutions may result in fire, electrical hazards, or improper operation. • Ensure that all equipment doors are closed and protective covers are in place, except when maintenance is being performed by qualified persons, to prevent electrical shock and personal injury. WArnInG: ExpLoSIon hAzArD Do noT opEn WhILE CIrCuIT IS LIvE. onLy CLEAn WITh DAMp CLoTh. noTICE If a 475 universal hArT® Communicator is used with these transmitters, the software within the 475 may require modification. If a software modification is required, please contact your local Emerson processs Management Service Group or national response Center at 1-800-654-7768. Electrostatic ignition hazard. Special condition for safe use (when installed in hazardous area) 1. The plastic enclosure, excepting the front panel, must only be cleaned with a damp cloth. The surface resistivity of the non-metallic enclosure materials is greater than one gigaohm. Care must be taken to avoid electrostatic charge build-up. The 1066 Transmitter must not be rubbed or cleaned with solvents or a dry cloth. 2. The panel mount gasket has not been tested for type of protection IP66 or Class II and III. Type of protection IP66 and Class II, III refer the enclosure only. Essential Instructions I 3. The surface resistivity of the non-metallic enclosure materials is greater than one gigaohm. Care must be taken to avoid electrostatic charge build-up. The Model 1066 Transmitter must not be rubbed or cleaned with solvents or a dry cloth. 4. Special Condition of Use of 1066-C-FF/FI-67 and 1066-T-FF/FI-67. For use with simple apparatus model series 140, 141, 142, 150, 400, 401, 402, 402VP, 403, 403VP, 404, and 410VP contacting conductivity sensors and model series 222, 225, 226, 228 toroidal sensors. About this document This manual contains instructions for installation and operation of the 1066 Smart Transmitter. The following list provides notes concerning all revisions of this document. II rev. Level A Date 1/2012 notes This is the initial release of the product manual. The manual has been reformatted to reflect the Emerson documentation style and updated to reflect any changes in the product offering. B 3/2012 This product manual version adds specifications and instrument instructions for Contacting Conductivity, Toroidal Conductivity, Chlorine, Oxygen, and Ozone measurements. C 9/2012 This product manual version adds FM agency approval. D 3/2013 Updated CSA Intrinsically Safe Installation drawings. E 7/2013 F G 9/2013 11/2014 Updated CSA test Standards and Intrinsically Safe installation drawings and update CE certificates. Added FM temperature specifications to Non-Incendive Hazardous Location Approval. Added Section 10: HART® Communications Changed agency water exposure testing description to “Type”. 1066 Instruction Manual Table of Contents LIQ_MAN_1066 December 2014 Contents Section 1: Quick Start Guide 1.1 Quick start guide..........................................................................................................1 Section 2: Description and Specifications 2.1 Features and Applications ............................................................................................3 2.2 General specifications...................................................................................................4 2.3 pH/ORP ........................................................................................................................4 2.4 2.5 2.6 2.7 2.8 2.9 2.3.1 Performance Specifications - Transmitter (pH input) ......................................6 2.2.2 Performance Specifications - Transmitter (ORP input) ....................................6 Contacting Conductivity (Codes – C) ...........................................................................7 2.4.1 Performance Specifications.............................................................................7 2.4.2 Recommended Sensors for Conductivity .......................................................8 Toroidal Conductivity (Codes – T) ................................................................................8 2.5.1 Performance Specifications.............................................................................8 2.5.2 Recommended Sensors for Conductivity........................................................9 Chlorine (Codes – CL) ...................................................................................................9 2.6.1 Free and Total Chlorine....................................................................................9 2.6.2 Performance Specifications.............................................................................9 2.6.3 Recommended Sensors ..................................................................................9 2.6.4 Monochloromine ............................................................................................9 2.6.5 Performance Specifications...........................................................................10 2.6.6 Recommended Sensors ................................................................................10 Dissolved Oxygen (Codes – DO).................................................................................10 2.7.1 Free and Total Chlorine..................................................................................10 2.7.2 Performance Specifications...........................................................................10 Dissolved Oxygen (Codes – DO).................................................................................10 2.8.1 Free and Total Chlorine..................................................................................10 2.8.2 Performance Specifications...........................................................................10 Ordering Information .................................................................................................11 Section 3: Installation 3.1 Unpacking and Inspection..........................................................................................13 3.2 Installation – general information ..............................................................................13 3.3 Preparing conduit openings .......................................................................................13 Section 4: Wiring 4.1 4.2 Table of Contents General ...................................................................................................................... 17 4.1.1 General Information ......................................................................................17 4.1.2 Digital Communication.................................................................................17 Power Supply/Current Loop – 1066-HT......................................................................17 III Table of Contents 1066 Instruction Manual December 2014 LIQ_MAN_1066 4.3 4.2.1 Power Supply and Load Requirements ..........................................................17 4.2.2 Power Supply-Current Loop Wiring...............................................................18 4.2.3 Current Output wiring...................................................................................19 Power Supply Wiring For 1066-FF...............................................................................19 4.3.1 4.4 Power Supply Wiring .....................................................................................19 Sensor Wiring to Main Board ......................................................................................21 Section 5: Intrinsically Safe Installation 5.1 All Intrinsically Safe Installations ................................................................................27 Section 6: Display and operation 6.1 User Interface.............................................................................................................37 6.2 Instrument Keypad.....................................................................................................37 6.3 Main Display ...............................................................................................................38 6.4 Menu System..............................................................................................................38 Section 7: programming – Basics 7.1 General.......................................................................................................................41 7.2 Changing the Startup Settings ...................................................................................41 7.3 7.4 7.5 7.6 7.7 7.8 IV 7.2.1 Purpose .........................................................................................................41 7.2.2 Procedure......................................................................................................42 Choosing Temperature Units & Automatic/Manual Temperature Compensation......42 7.3.1 Purpose .........................................................................................................42 7.3.2 Procedure......................................................................................................42 Contacting Conductivity Calibration..........................................................................42 7.4.1 Purpose .........................................................................................................42 7.4.2 Definitions.....................................................................................................43 7.4.3 Procedure: Configure Outputs ......................................................................43 7.4.4 Procedure: Assigning Measurements the Low and High Current Outputs ....43 7.4.4 Procedure: Ranging the Current Outputs......................................................43 Setting a Security Code ..............................................................................................43 7.5.1 Purpose .........................................................................................................43 7.5.2 Procedure......................................................................................................44 Security Access...........................................................................................................45 7.6.1 How the Security Code Works.......................................................................45 7.6.2 Procedure......................................................................................................45 Using Hold..................................................................................................................45 7.7.1 Purpose .........................................................................................................45 7.7.2 Using the Hold Function................................................................................45 Resetting Factory Default Settings .............................................................................46 7.8.1 Purpose .........................................................................................................46 7.8.2 Procedure......................................................................................................46 Table of Contents 1066 Instruction Manual Table of Contents LIQ_MAN_1066 December 2014 Section 8: programming – Measurements 8.1 Introduction ..............................................................................................................47 8.2 pH Measurement Programming ................................................................................48 8.3 8.4 8.2.1 Description....................................................................................................48 8.2.2 Measurement................................................................................................48 8.2.3 Preamp..........................................................................................................48 8.2.4 Solution Temperature Correction .................................................................49 8.2.5 Temperature Coefficient ...............................................................................49 8.2.6 Resolution .....................................................................................................49 8.2.7 Filter ..............................................................................................................49 8.2.8 Reference Impedance....................................................................................49 ORP Measurement Programming ..............................................................................49 8.3.1 Measurement................................................................................................50 8.3.2 Preamp..........................................................................................................50 8.3.3 Filter ..............................................................................................................50 8.3.4 Reference Impedance....................................................................................50 Contacting Conductivity ............................................................................................51 8.4.1 Description....................................................................................................51 8.4.2 Sensor Type ...................................................................................................51 8.4.3 Measure ........................................................................................................52 8.4.4 Range ............................................................................................................52 8.4.5 Cell Constant.................................................................................................52 8.4.6 RTD Offset.....................................................................................................52 8.4.7 RTD Slope......................................................................................................52 8.4.8 Temp Comp ..................................................................................................52 8.4.9 Slope .............................................................................................................53 8.4.10 Reference Temp ............................................................................................53 8.4.11 Filter ..............................................................................................................53 8.4.12 Custom Setup ...............................................................................................53 8.4.13 Cal Factor ......................................................................................................53 8.5 Toroidal Conductivity .................................................................................................54 8.5.1 Description....................................................................................................54 8.5.2 Sensor Type ...................................................................................................54 8.5.3 Measure ........................................................................................................55 8.5.4 Range ............................................................................................................55 8.5.5 Cell Constant.................................................................................................55 8.5.6 Temp Comp ..................................................................................................55 8.5.7 Slope .............................................................................................................56 8.5.8 Reference Temp ............................................................................................56 8.5.9 Filter ..............................................................................................................56 8.5.10 Custom Setup ...............................................................................................56 8.6 Chlorine Measurement...............................................................................................57 8.6.1 Table of Contents Free Chlorine .................................................................................................57 V Table of Contents 1066 Instruction Manual December 2014 LIQ_MAN_1066 8.6.1.1 Measure..........................................................................................58 8.6.1.2 Units ...............................................................................................58 8.6.1.3 Filter................................................................................................58 8.6.1.4 Free Chlorine pH Correction ...........................................................58 8.6.1.5 Manual pH Correction ....................................................................58 8.6.1.6 Resolution.......................................................................................58 8.6.2 Total Chlorine ................................................................................................59 8.6.2.1 Description .....................................................................................59 8.6.2.2 Measure..........................................................................................59 8.6.2.3 Units ...............................................................................................59 8.6.2.4 Filter................................................................................................59 8.6.2.5 Resolution.......................................................................................60 8.6.3 Monochloramine ..........................................................................................60 8.6.3.1 Measure: Monochloramine.............................................................60 8.6.3.2 Units ...............................................................................................60 8.6.3.3 Filter................................................................................................61 8.6.3.4 Resolution.......................................................................................61 8.7 8.8 Oxygen.......................................................................................................................61 8.7.1 Oxygen Measurement Application .................................................62 8.7.2 Units ...............................................................................................62 8.7.3 Partial Press.....................................................................................62 8.7.4 Salinity............................................................................................62 8.7.5 Filter................................................................................................62 8.7.6 Pressure Units .................................................................................62 Ozone.........................................................................................................................63 8.8.1 Units ...............................................................................................63 8.8.2 Filter................................................................................................63 8.8.3 Resolution.......................................................................................63 Section 9: Calibration 9.1 Introduction ..............................................................................................................71 9.2 Calibration..................................................................................................................71 9.2.1 Auto Calibration .........................................................................................................72 9.3 9.2.2 Manual Calibration – pH................................................................................73 9.2.3 Entering a Known Slope Value – pH ..............................................................73 9.2.4 Standardization – pH.....................................................................................73 9.2.5 SMART sensor auto calibration upload – pH..................................................73 ORP Calibration ..........................................................................................................74 9.3.1 9.4 VI Standardization – ORP...................................................................................74 Contacting Conductivity Calibration..........................................................................75 9.4.1 Entering the Cell Constant.............................................................................76 9.4.2 Zeroing the Instrument .................................................................................76 Table of Contents 1066 Instruction Manual Table of Contents LIQ_MAN_1066 December 2014 9.5 9.6 9.4.3 Calibrating the Sensor in a Conductivity Standard (in process cal)................76 9.4.4 Calibrating the Sensor To A Laboratory Instrument (meter cal) ....................77 9.4.5 Cal Factor ......................................................................................................77 Toroidal Conductivity Calibration...............................................................................78 9.5.1 Entering the Cell Constant.............................................................................78 9.5.2 Zeroing the Instrument .................................................................................79 9.5.3 Calibrating the Sensor in a Conductivity Standard (in process cal)................79 Calibration – Chlorine.................................................................................................80 9.6.1 Calibration – Free Chlorine ............................................................................80 9.6.1.1 Zeroing the Sensor..........................................................................81 9.6.1.2 In Process Calibration......................................................................81 9.6.2 Calibration – Total Chlorine...........................................................................81 9.6.2.1 Zeroing the Sensor..........................................................................82 9.6.2.2 In Process Calibration......................................................................82 9.6.3 Calibration – Monochloromine ..................................................................................83 9.7 9.8 9.9 9.6.4 Zeroing the Sensor ........................................................................................84 9.6.5 In Process Calibration ....................................................................................84 Calibration – Chlorine.................................................................................................84 9.7.1 Zeroing the Sensor ........................................................................................86 9.7.2 Calibrating the Sensor in Air ..........................................................................86 9.7.3 Calibrating the Sensor Against A Standard Instrument (in process cal) .........87 Calibration – Ozone....................................................................................................87 9.8.1 Zeroing the Sensor ........................................................................................88 9.8.2 In Process Calibration ....................................................................................88 Calibrating Temperature ............................................................................................89 9.9.1 Calibration.....................................................................................................89 Section 10: hArT® Communications 10.1 Introduction ...............................................................................................................97 10.2 Physical Installation and Configuration ......................................................................97 10.3 Measurements Available via HART .............................................................................99 10.4 Diagnostics Available via HART.................................................................................100 10.5 HART Hosts ..............................................................................................................101 10.6 Wireless Communication using the 1066 ................................................................104 10.7 Field Device Specification (FDS) ...............................................................................104 10.6 Wireless Communication using the 1066 ................................................................104 APPENDIX 10.1 Device Variables .......................................................................................105 APPENDIX 10.2 Additional Transmitter Status –Command 48 Status Bits ........................107 APPENDIX 10.3 1066 HART Configuration Parameters......................................................112 APPENDIX 10.4 475 Menu Tree for 1066 HART 7...............................................................119 Table of Contents VII Table of Contents 1066 Instruction Manual December 2014 LIQ_MAN_1066 Section 11: return of Material 11.1 General.....................................................................................................................125 11.2 Warranty Repair .......................................................................................................125 11.3 Non-Warranty Repair ...............................................................................................125 EC Declarations of Conformity..........................................................................................................126 VIII 1066 Instruction Manual LIQ_MAN_1066 Section 1: Quick Start Guide December 2014 Section 1: Quick Start Guide 1.1 Quick Start Guide 1. For mechanical installation instructions, see page 14 for panel mounting and page 15 for pipe or wall mounting. 2. Wire the sensor to the main circuit board. See pages 21-23 for wiring instructions. Refer to the sensor instruction sheet for additional details. Make loop power connections. 3. Once connections are secured and verified, apply DC power to the transmitter. 4. When the transmitter is powered up for the first time, Quick Start screens appear. Quick Start operating tips are as follows: a. A highlighted field shows the position of the cursor. b. To move the cursor left or right, use the keys to the left or right of the ENTER key. To scroll up or down or to increase or decrease the value of a digit use the keys above and below the ENTER key. Use the left or right keys to move the decimal point. c. Press ENTER to store a setting. Press EXIT to leave without storing changes. Pressing EXIT during Quick Start returns the display to the initial start-up screen (select language). 5. Choose the desired language and press ENTER. 6. Choose measurement and press ENTER. a. For pH, choose preamplifier location. Select Analyzer to use the integral preamplifier in the transmitter; select Sensor/J-Box if your sensor is SMART or has an integral preamplifier or if you are using a remote preamplifier located in a junction box. 5. If applicable, choose units of measurement. 6. For contacting and toroidal conductivity, choose the sensors type and enter the numeric cell constant using the keys. 7. Choose temperature units: °C or °F. 8. After the last step, the main display appears. The outputs are assigned to default values. 9. To change output settings, to scale the 4-20mA current outputs, to change measurementrelated settings from the default values, and to enable pH diagnostics, press MENU. Select Program and follow the prompts. Refer to the appropriate menu. 10. To return the transmitter to the factory default settings, choose Program under the main menu, and then scroll to Reset. 11. Please call the Rosemount Analytical Customer Support Center at 1-800-854-8257 if you need further support. 1 Section 2: Description and specifications December 2014 1066 Instruction Manual LIQ_MAN_1066 This page left intentionally blank 2 Description and Specifications 1066 Instruction Manual Section 2: Description and specifications LIQ_MAN_1066 December 2014 Section 2: Description and Specifications 2.1 Features and Applications This loop-powered multi-parameter unit serves industrial, commercial and municipal applications with the widest range of liquid measurement inputs available for a two-wire liquid transmitter. The 1066 Smart transmitter supports continuous measurement of one liquid analytical input. The design supports easy internal access and wiring connections. AnALyTICAL InpuTS: Ordering options for pH/ORP, Resistivity/Conductivity, % Concentration, Total Chlorine, Free Chlorine, Monochloramine, Dissolved Oxygen, and Ozone. LArGE DISpLAy: The high-contrast LCD provides live measurement readouts in large digits and shows up to four additional variables or diagnostic parameters. DIGITAL CoMMunICATIonS: HART® version 7 digital communications are standard on 1066. MEnuS: Menu screens for calibrating and programming are simple and intuitive. Plain language prompts and help screens guide the user through the procedures. All menu screens are available in eight languages. Live process values are displayed during programming and calibration. QuICK STArT proGrAMMInG: Popular Quick Start screens appear the first time the unit is powered. The instrument prompts the user to configure the sensor loop in a few quick steps for immediate commissioning. uSEr hELp SCrEEnS: Fault and warning messages include help screens similar to PlantWeb™ alerts that provide useful troubleshooting tips to the user. These on-screen instructions are intuitive and easy to use. DIAGnoSTICS: The transmitter continuously monitors itself and the sensor for problems. A display banner on the screen alerts Technicians to Fault and/or Warning conditions. LAnGuAGES: Rosemount Analytical extends its worldwide reach by offering eight languages – English, French, German, Italian, Spanish, Portuguese, Chinese and Russian. CurrEnT ouTpuTS: HART units include two 4-20 mA electrically isolated current outputs giving the ability to transmit the live measurement value and the process temperature reported from the sensor. InpuT DAMpEnInG: is automatically enabled to suppress noisy process readings. SMArT-EnABLED ph: Rosemount Analytical’s SMART pH capability eliminates field calibration of pH probes through automatic upload of calibration data and history. AuToMATIC TEMpErATurE CoMpEnSATIon: Most measurements require temperature compensation. The 1066 will automatically recognize Pt100, Pt1000 or 22k NTC RTDs built into the sensor. SMArT WIrELESS ThuM ADApTor CoMpATIBLE: Enable wireless transmissions of process variables and diagnostics from hard-to-reach locations. Specifications 3 Section 2: Description and specifications 1066 Instruction Manual December 2014 LIQ_MAN_1066 Specifications - General 2.2 Case: Polycarbonate. IP66 (CSA, FM), Type 4X (CSA) Dimensions: Overall 155 x 155 x 131mm (6.10 x 6.10 x 5.15 in.). Cutout: 1/2 DIN 139mm x 139mm (5.45 x 5.45 in.) Conduit openings: Six. Accepts PG13.5 or 1/2 in. conduit fittings Display: Monochromatic graphic liquid crystal display. No backlight. 128 x 96 pixel display resolution. Active display area: 58 x 78mm (2.3 x 3.0 in.). All fields of the main instrument display can be customized to meet user requirements. Ambient temperature and humidity: -20 to 65°C (-4 to 149°F), RH 5 to 95% (non-condensing). Storage Temperature: -20 to 70°C (-4 to 158°F) hArT® Communications: PV, SV, TV, and 4V assignable to measurement, temperature and all live HART diagnostics. rFI/EMI: EN-61326 Complies with the following Standards: CSA: C22.2 No 0 – 10; C22.2 No 0.4 – 04; C22.2 No. 25-M1966: , C22.2 No. 94-M91: , C22.2 No.142-M1987: , C22.2 No. 157-M1992: , C22.2 No. 213-M1987: , C22.2 No. 60529:05. UL: 50; 508; 913; 1203. ANSI/ISA: 12.12.02-2011. ATEX: IEC 60079-0:2011, 60079-11:2011 IECEx: IEC 60079-0: 2011 Edition: 6.0, I EC 60079-11 : 2011-06 Edition: 6.0 FM: 3600: 2011, 3610: 2010, 3611: 2004, 3810: 2005, IEC 60529:2004, ANSI/ISA 60079-0: 2009, ANSI/ISA 60079-11: 2009 hazardous Location Approvals Intrinsic Safety (with appropriate safety barrier): Class I, II, III, Div. 1* Groups A-G T4 Tamb = -20°C to 65°C Enclosure 4X, IP66 ATEx 1180 II 1 G Baseefa11ATEX0195X Ex ia IIC T4 Ga T4 Tamb = -20°C to 65° For Non-Incendive Field Wiring Installation, see drawing 1400670 IECEx BAS 11.0098X Ex ia IIC T4 Ga T4 Tamb = -20°C to 65°C Class I, II & III, Division 1, Groups A-G T4 Tamb = -20°C to 40°C for -FI option Tamb = -20°C to 65°C for -HT and -FF options IP66 enclosure Class I, Zone 0, AEx ia IIC T4 Tamb = -20°C to 40°C for -FI option Tamb = -20°C to 65°C for -HT and -FF options For Non-Incendive Field Wiring Installation, see drawing 1400669 Non-Incendive: Class I, Div. 2, Groups A-D* Dust Ignition Proof Class II & III, Div 1, Groups EFG Class II & III, Div. 1, Groups E-G Type 4/4X Enclosure T4 Tamb = -20°C to 65°C Class I, Division 2 Groups A-D Dust Ignition proof Class II & III, Div 1, Groups EFG Class II & III, Division 1, Groups E-G IP66 enclosure For Non-Incendive Field Wiring Installation, see drawing 1400670 For Non-Incendive Field Wiring Installation, see drawing 1400669 *Additionally approved as a system with models 140,141,142, 150, 400, 400VP, 401, 402, 402VP, 403,403VP, 404 & 410VP contacting conductivity sensors and models 222, 225, 226 & 228 inductive conductivity sensors. 4 Specifications 1066 Instruction Manual Section 2: Description and specifications LIQ_MAN_1066 December 2014 Input: One isolated sensor input. Measurement choices of pH/ORP, resistivity/conductivity/TDS, % concentration, total and free chlorine, monochloramine, dissolved oxygen, dissolved ozone, and temperature. For contacting conductivity measurements, temperature element can be a PT1000 RTD or a PT100 RTD. Other measurements (except ORP) and use PT100 or PT1000 RTDs or a 22k NTC (D.O. only). power & Load requirements: Supply voltage at the transmitter terminals should be at least 12.7Vdc. Power supply voltage should cover the voltage drop on the cable plus the external load resistor required for HART communications (250 Ω minimum). Minimum power supply voltage is 12.7Vdc. Maximum power supply voltage is 42.4 Vdc (30 Vdc for intrinsically safe operation). The graph shows the supply voltage required to maintain 12 Vdc (upper line) and 30 Vdc (lower line) at the transmitter terminals when the current is 22 mA. FIGurE 2-1. Load/power Supply requirements 1500 1364 ohms 1250 Load, ohms 1000 750 545 ohms with HART communication 500 250 without HART communication 0 12 18 24 30 36 42 Power supply voltage, Vdc HART option Analog outputs: Two-wire loop powered (Output 1 only). Two 4-20 mA electrically isolated current outputs (Output 2 must be externally powered). Superimposed HART digital signal on Output 1. Fully scalable over the operating range of the sensor. Weight/Shipping Weight: 2 lbs/3 lbs (1 kg/1.5 kg) Specifications 5 Section 2: Description and specifications 1066 Instruction Manual December 2014 2.3 LIQ_MAN_1066 ph/orp (ordering Code – p) For use with any standard pH or ORP sensor. SMART pH sensor with SMART pre-amplifiers from Rosemount Analytical. Measurement choices are pH, ORP, or Redox. The automatic buffer recognition feature uses stored buffer values and their temperature curves for the most common buffer standards available worldwide. The transmitter will recognize the value of the buffer being measured and perform a self stabilization check on the sensor before completing the calibration. Manual or automatic temperature compensation is menu selectable. Change in pH due to process temperature can be compensated using a programmable temperature coefficient. 2.3.1 Performance Specifications - Transmitter (pH input) Measurement range [ph]: 0 to 14 pH Accuracy: ±0.01 pH Buffer recognition: NIST, DIN 19266, JIS 8802, and BSI. Input filter: Time constant 1 - 999 sec, default 4 sec. response time: 5 seconds to 95% of final reading recommended Sensors for ph: All standard pH sensors. Supports SMART pH sensors from Rosemount Analytical 2.3.2 Performance Specifications - Transmitter (ORP input) Measurement range [orp]: -1400 to +1400 mV Accuracy: ± 1 mV Input filter: Time constant 1 - 999 sec, default 4 sec. response time: 5 seconds to 95% of final reading recommended Sensors for orp: All standard ORP sensors FIGurE 2-2. General purpose and high performance ph sensors 3900, 396pvp and 3300hT 6 Specifications 1066 Instruction Manual Section 2: Description and specifications LIQ_MAN_1066 December 2014 Contacting Conductivity (Codes – C) 2.4 Measures conductivity in the range 0 to 600,000 μS/cm (600mS/cm). Measurement choices are conductivity, resistivity, total dissolved solids, salinity, and % concentration. In addition, the “Custom Curve” feature allows users to define a three to five point curve to measure ppm, %, or a no unit variable. The % concentration selection includes the choice of five common solutions (012% NaOH, 0-15% HCl, 0-20% NaCl, and 0-25% or 96-99.7% H2SO4). The conductivity concentration algorithms for these solutions are fully temperature compensated. Three temperature compensation options are available: manual slope (X%/°C), high purity water (dilute sodium chloride), and cation conductivity (dilute hydrochloric acid). Temperature compensation can be disabled, allowing the transmitter to display raw conductivity. For more information concerning the use of the contacting conductivity sensors, refer to the product data sheets. Note: The 410VP 4-electrode high-range conductivity sensor is compatible with the 1066. 2.4.1 Performance Specifications ENDURANCE series of conductivity sensors TM Temperature specifications: Temperature range 0-200°C Temperature Accuracy, Pt-1000, 0-50°C ± 0.1°C Temperature Accuracy, Pt-1000, Temp. > 50°C ± 0.5°C Input filter: Time constant 1 - 999 sec, default 2 sec. response time: 3 seconds to 95% of final reading using the default input filter Salinity: Uses Practical Salinity Scale Total Dissolved Solids: Calculated by multiplying conductivity at 25ºC by 0.65 TABLE 2-1. performance Specifications: recommended range – Contacting Conductivity Cell 0.01S/cm Constant 0.01 0.1mS/cm 1.0mS/cm 10mS/cm 100mS/cm 0.1mS/cm to 2000mS/cm 1.0 10mS/cm 1000mS/cm 2000mS/cm to 20mS/cm 1 mS/cm to 20mS/cm 20mS/cm to 200mS/cm 4-electrode Linearity for Standard Cable ≤ 50 ft (15 m) 100mS/cm 200mS/cm to 2000mS/cm 0.01mS/cm to 200mS/cm 0.1 1000mS/cm 2mS/cm to 1400mS/cm ±0.6% of reading in recommended range ±2% of reading outside high recommended range ±5% of reading outside low recommended range ±4% of reading in recommended range Specifications 7 Section 2: Description and specifications 1066 Instruction Manual December 2014 2.4.2 LIQ_MAN_1066 Recommended Sensors for Conductivity All Rosemount Analytical ENDURANCE 400 series conductivity sensors (Pt 1000 RTD) and 410VP 4-electrode sensor. 2.5 Toroidal Conductivity (Codes – T) Measures conductivity in the range of 1 μS/cm to 2,000,000 μS/cm (2 S/cm). Measurement choices are conductivity, resistivity, total dissolved solids, salinity, and % concentration. The % concentration selection includes the choice of five common solutions (0-12% NaOH, 0-15% HCl, 0-20% NaCl, and 025% or 96-99.7% H2SO4). The conductivity concentration algorithms for these solutions are fully temperature compensated. For other solutions, a simple-to-use menu allows the customer to enter his own data. The transmitter accepts as many as five data points and fits either a linear (two points) or a quadratic function (three to five points) to the data. Reference temperature and linear temperature slope may also be adjusted for optimum results. Two temperature compensation options are available: manual slope (X%/°C) and neutral salt (dilute sodium chloride). Temperature compensation can be disabled, allowing the transmitter to display raw conductivity. For more information concerning use of the toroidal conductivity sensors, refer to the product data sheets. 2.5.1 Performance Specifications High performance 225 Toroidal & 226 Conductivity sensors Temperature specifications: Temperature range -25 to 210°C (-13 to 410ºF) Temperature Accuracy, Pt-100, -25 to 50°C ± 0.5°C Temperature Accuracy, Pt-100, 50 to 210°C ± 1°C TABLE 2-2. performance Specifications: recommended range – Toroidal Conductivity Model 1mS/cm 10mS/cm 226 225 & 228 242 222 (1in & 2in) Loop performance (Following Calibration) 100mS/cm 1000mS/cm 10mS/cm 100mS/cm 1000mS/cm 2000mS/cm 50mS/cm to 500mS/cm 500mS/cm to 2000mS/cm 50mS/cm to 1500mS/cm 1500mS/cm to 2000mS/cm 100mS/cm to 2000mS/cm 500mS/cm to 2000mS/cm 226: ±1% of reading ±5mS/cm in recommended range 225 & 228: ±1% of reading ±15mS/cm in recommended range 222, 242: ±4% of reading ±5mS/cm in recommended range 225, 226 & 228: ±5% of reading outside high recommended range 8 Specifications 1066 Instruction Manual Section 2: Description and specifications LIQ_MAN_1066 December 2014 repeatability: ±0.25% ±5 μS/cm after zero cal Input filter: time constant 1 - 999 sec, default 2 sec. response time: 3 seconds to 95% of final reading Salinity: Uses Practical Salinity Scale Total Dissolved Solids: Calculated by multiplying conductivity at 25ºC by 0.65 2.5.2 Recommended Sensors for Conductivity All Rosemount Analytical submersion/immersion and flow-through toroidal sensors. 2.6 Chlorine (Codes – CL) 2.6.1 Free and Total Chlorine The 1066 is compatible with the 499ACL-01 free chlorine sensor and the 499ACL-02 total chlorine sensor. The 499ACL-02 sensor must be used with the TCL total chlorine sample conditioning system. The 1066 fully compensates free and total chlorine readings for changes in membrane permeability caused by temperature changes. For free chlorine measurements, both automatic and manual pH correction are available. For automatic pH correction select an appropriate pH sensor. For more information concerning the use and operation of the amperometric chlorine sensors and the TCL measurement system, refer to the product data sheets. 2.6.2 Performance Specifications resolution: 0.001 ppm or 0.01 ppm – selectable Input range: 0nA – 100μA Automatic ph correction for Free Chlorine: (user selectable for code -CL): 6.0 to 10.0 pH Temperature compensation: Automatic (via RTD) or manual (050°C). Input filter: Time constant 1 - 999 sec, default 5 sec. response time: 6 seconds to 95% of final reading 2.6.3 499ACL-01 Chlorine sensor Recommended Sensors Chlorine: 499ACL-01 Free Chlorine or 499ACL-02 Total Residual Chlorine ph: These pH sensors are recommended for automatic pH correction of free chlorine readings: 3900-02-10, 3900-01-10, and 3900VP-02-10. 2.6.4 Monochloramine The 1066 is compatible with the 499A CL-03 Monochloramine sensor. The 1066 fully compensates readings for changes in membrane permeability caused by temperature changes. Because monochloramine measurement is not affected by pH of the process, no pH sensor or correction is required. For more information concerning the use and operation of the amperometric chlorine sensors, refer to the product data sheets. Specifications 9 Section 2: Description and specifications 1066 Instruction Manual December 2014 2.6.5 LIQ_MAN_1066 Performance Specifications resolution: 0.001 ppm or 0.01 ppm – selectable Input range: 0nA – 100μA Temperature compensation: Automatic (via RTD) or manual (0-50°C). Input filter: Time constant 1 - 999 sec, default 5 sec. response time: 6 seconds to 95% of final reading 2.6.6 Recommended Sensors Rosemount Analytical 499ACL-03 Monochloramine sensor 2.7 Dissolved oxygen (Codes –Do) The 1066 is compatible with the 499ADO, 499ATrDO, Hx438, Gx438 and Bx438 dissolved oxygen sensors and the 4000 percent oxygen gas sensor. The 1066 displays dissolved oxygen in ppm, mg/L, ppb, μg/L, % saturation, % O2 in gas, ppm O2 in gas. The transmitter fully compensates oxygen readings for changes in membrane permeability caused by temperature changes. Automatic air calibration, including salinity correction, is standard. The only required user entry is barometric pressure. For more information on the use of amperometric oxygen sensors, refer to the product data sheets. 2.7.1 Performance Specifications resolution: 0.01 ppm; 0.1 ppb for 499A TrDO sensor (when O2 <1.00 ppm); 0.1% Input range: 0nA – 100μA Temperature Compensation: Automatic (via RTD) or manual (0-50°C). Input filter: Time constant 1 - 999 sec, default 5 sec. response time: 6 seconds to 95% of final reading 2.7.2 Recommended Sensors Dissolved Oxygen 499ADO sensor with Variopol connection Rosemount Analytical amperometric membrane and steam-sterilizable sensors listed above 2.8 Dissolved ozone (Codes –oz) The 1066 is compatible with the 499AOZ sensor. The 1066 fully compensates ozone readings for changes in membrane permeability caused by temperature changes. For more information concerning the use and operation of the amperometric ozone sensors, refer to the product data sheets. 2.8.1 Performance Specifications resolution: 0.001 ppm or 0.01 ppm – selectable Input range: 0nA – 100μA Temperature Compensation: Automatic (via RTD) or manual (0-35°C) Input filter: Time constant 1 - 999 sec, default 5 sec. response time: 6 seconds to 95% of final reading 2.8.2 Recommended Sensors Dissolved Ozone 499AOZ sensors with Variopol connection Rosemount Analytical 499A OZ ozone sensor 10 Specifications 1066 Instruction Manual Section 2: Description and specifications LIQ_MAN_1066 December 2014 ordering Information 2.9 The 1066 2-Wire Transmitter is intended for the continuous determination of pH, ORP (Redox), conductivity, (both contacting and toroidal), and for measurements using membrane-covered amperometric sensors (oxygen, ozone, free and total chlorine, and monochloramine). For free chlorine measurements, which often require continuous pH correction a second input for a pH sensor is available. Two 4-20mA analog outputs are standard on HART units. The 1066 is compatible with SMART pH sensors from Rosemount Analytical. HART digital communications is standard and FOUNDATION® fieldbus digital communications is offered as an option. Communication with the 1066 is through:  Local keypad interface  475 HART® and FOUNDATION fieldbus Communicator  HART protocol version 7  FOUNDATION fieldbus  AMS (Asset Management Solutions) Aware  SMART Wireless THUM™ Adapter TABLE 2-3. ordering Information Description 1066 ph/orp, Conductivity, Chlorine, oxygen, and ozone 2-Wire Transmitter Measurement P pH/ORP C Contacting Conductivity T Toroidal Conductivity CL Chlorine DO Dissolved Oxygen OZ Ozone Communication HT HART® Digital Communication Superimposed on 4-20mA Output FF FOUNDATION™ fieldbus Digital Output FI FOUNDATION™ fieldbus Digital Output with FISCO Agency Approval 60 None Required Specifications 67 FM Approved, Intrinsically Safe (appropriate sensor & safety barrier required), and Non-Incendive 69 CSA Approved , Intrinsically Safe (appropriate sensor & safety barrier required), and Non-Incendive 73 ATEX/IECEx Approved, Intrinsically Safe (safety barrier required) 11 Section 2: Description and specifications December 2014 1066 Instruction Manual LIQ_MAN_1066 This page left intentionally blank 12 Specifications 1066 Instruction Manual LIQ_MAN_1066 Section 3: Installation December 2014 Section 3: Installation 3.1 unpacking and inspection Inspect the shipping container. If it is damaged, contact the shipper immediately for instructions. Save the box. If there is no apparent damage, unpack the container. Be sure all items shown on the packing list are present. If items are missing, notify Rosemount Analytical immediately. 3.2 Installation – general information 1. Although the transmitter is suitable for outdoor use, installation is direct sunlight or in areas of extreme temperatures is not recommended unless a sunshield is used. 2. Install the transmitter in an area where vibration and electromagnetic and radio frequency interference are minimized or absent. 3. Keep the transmitter and sensor wiring at least one foot from high voltage conductors. Be sure there is easy access to the transmitter. 4. The transmitter is suitable for panel, pipe, or surface mounting. 5. The transmitter case has six 1/2-inch (PG13.5) conduit openings. Use separate conduit openings for the power/output cable, the sensor cable, and the other the sensor cable as needed (pH input for free chlorine with continuous pH correction). 6. Use weathertight cable glands to keep moisture out to the transmitter. If conduit is used, plug and seal the connections at the transmitter housing to prevent moisture from getting inside the instrument. 3.3 preparing conduit openings There are six conduit openings in all configurations of 1066. Conduit openings accept 1/2-inch conduit fittings or PG13.5 cable glands. To keep the case watertight, block unused openings with Type 4X or IP66 conduit plugs. To maintain ingress protection for outdoor use, seal unused conduit holes with suitable conduit plugs. noTE: Use watertight fittings and hubs that comply with your requirements. Connect the conduit hub to the conduit before attaching the fitting to the transmitter. Electrical installation must be in accordance with the national Electrical Code (AnSI/nFpA-70) and/or any other applicable national or local codes. Installation 13 Section 3: Installation December 2014 1066 Instruction Manual LIQ_MAN_1066 FIGurE 3-1. panel Mounting Dimensions 14 Installation 1066 Instruction Manual LIQ_MAN_1066 Section 3: Installation December 2014 FIGurE 3-2. pipe and wall mounting dimensions (Mounting bracket pn: 23820-00) Installation 15 Section 3: Installation 1066 Instruction Manual December 2014 LIQ_MAN_1066 This page left intentionally blank 16 Installation 1066 Instruction Manual Section 4: Wiring LIQ_MAN_1066 December 2014 Section 4: Wiring 4.1 General 4.1.1 General Information The 1066 is easy to wire. All wiring connections are located on the main circuit board. The front panel is hinged at the bottom. The panel swings down for easy access to the wiring locations. 4.1.2 Digital Communication HART and FOUNDATION fieldbus communications are available as ordering options for 1066. HART units support Bell 202 digital communications over analog 4-20mA current output 1. 4.2 power Supply/Current Loop – 1066-hT 4.2.1 Power Supply and Load Requirements Refer to Figure 4-1. The supply voltage must be at least 12.7 Vdc at the transmitter terminals.. The power supply must be able to cover the voltage drop on the cable as well as the load resistor (250 Ω minimum) required for HART communications. The maximum power supply voltage is 42.0 Vdc. For intrinsically safe installations, the maximum power supply voltage is 30.0 Vdc. The graph shows load and power supply requirements. The upper line is the power supply voltage needed to provide 12.7 Vdc at the transmitter terminals for a 22 mA current. The lower line is the power supply voltage needed to provide 30 Vdc for a 22 mA current. The power supply must provide a surge current during the first 80 milliseconds of startup. The maximum current is about 24 mA. For digital communications, the load must be at least 250 ohms. To supply the 12.7 Vdc lift off voltage at the transmitter, the power supply voltage must be at least 17.5 Vdc. FIGurE 4-1. Load/power Supply requirements 1500 1364 ohms 1250 Load, ohms 1000 750 545 ohms with HART communication 500 250 without HART communication 0 12 18 24 30 36 42 Power supply voltage, Vdc HART option Wiring 17 Section 4: Wiring December 2014 4.2.2 1066 Instruction Manual LIQ_MAN_1066 Power Supply-Current Loop Wiring Refer to Figure 4-2. Run the power/signal wiring through the opening nearest TB-2. For optimum EMI/RFI protection: 1. Use shielded power/signal cable and ground the shield at the power supply. 2. Use a metal cable gland and be sure the shield makes good electrical contact with the gland. 3. Use the metal backing plate when attaching the gland to transmitter enclosure. The power/signal cable can also be enclosed in an earth-grounded metal conduit. Do not run power supply/signal wiring in the same conduit or cable tray with loop power lines. Keep power supply/signal wiring at least 6 ft (2 m) away from heavy electrical equipment. FIGurE 4-2. hArT Communications 18 Wiring 1066 Instruction Manual LIQ_MAN_1066 4.2.3 Section 4: Wiring December 2014 Current Output wiring The 1066 HART units are shipped with two 4-20mA current outputs. Current Output 1 is loop power; it is the HART communications channel. Current output 2 is available to report process temperature measured by the temperature sensing element or RTD within the sensor. Wiring locations for the outputs are on the main board which is mounted on the hinged door of the instrument. Wire the output leads to the correct position on the main board using the lead markings (+/positive, -/negative) on the board. FIGurE 4-3. 1066 hArT Loop power Wiring 4.3 power Supply Wiring For 1066-FF 4.3.1 Power Supply Wiring Run the power/signal wiring through the opening nearest TB2. Use shielded cable and ground the shield at the power supply. To ground the transmitter, attach the shield to TB2-3. Wiring 19 Section 4: Wiring 1066 Instruction Manual December 2014 LIQ_MAN_1066 noTE: For optimum EMI/RFI immunity, the power supply/output cable should be shielded and enclosed in an earth-grounded metal conduit. Do not run power supply/signal wiring in the same conduit or cable tray with loop power lines. Keep power supply/signal wiring at least 6 ft (2 m) away from heavy electrical equipment. FounDATIon fieldbus Figure 4-4 shows a 1066-P-FF being used to measure and control pH and chlorine levels in drinking water. The figure also shows three ways in which Fieldbus communication can be used to read process variables and configure the transmitter. FIGurE 4-4. Configuring 1066-p Transmitter with FounDATIon fieldbus 1066 Transmitter FIGurE 4-5. Typical Fieldbus network Electrical Wiring Configuration 20 Wiring 1066 Instruction Manual LIQ_MAN_1066 4.4 Section 4: Wiring December 2014 Sensor Wiring to Main Board Wire the correct sensor leads to the main board using the lead locations marked directly on the board. Rosemount Analytical SMART pH sensors can be wired to the 1066 using integral cable SMART sensors or compatible VP8 pH cables. After wiring the sensor leads, carefully take up the excess sensor cable through the cable gland. Keep sensor and output signal wiring separate from loop power wiring. Do not run sensor and power wiring in the same conduit or close together in a cable tray. FIGurE 4-6. ph/orp sensor wiring to the 1066 printed circuit board Wiring 21 Section 4: Wiring 1066 Instruction Manual December 2014 LIQ_MAN_1066 FIGurE 4-7. Contacting and Toroidal Conductivity sensor wiring to the 1066 circuit board 22 Wiring 1066 Instruction Manual Section 4: Wiring LIQ_MAN_1066 December 2014 FIGurE 4-8. Chlorine, oxygen, ozone sensor wiring to 1066 printed circuit board (1066-CL, 1066-Do, 1066-oz) HINGE SIDE OF FRONT PANEL OUTPUT 2 (OUTPUT1) LOOP PWR TB5 SENSOR WIRING TB3 TB2 +24V ANODE RTN REF GND GND CATHODE SNS SHLD RTN IN GND SOL TB7 TB6 THUM +24V +V SHLD pH -V TB4 TB1 1066 CIRCUIT BOARD ASSY 24359- 00 CHLORINE, OXYGEN, OZONE SENSOR WIRING (FOLLOW RECOMMENDED ORDER) 1) TB5/ANODE & CATHODE ANODE CATHODE 2) TB3/RTD RETURN SENSE RTD IN 3) TB2/ SOLUTION GROUND NO CONNECTION NO CONNECTION SOLUTION GROUND NOTE: A) TB1, TB4, TB6 AND TB7 NOT USED FOR OXYGEN AND OZONE SENSOR WIRING. B) TB1, TB2 AND TB4 MAY BE USED FOR pH SENSOR WIRING IF FREE CHLORINE MEASEMENT REQUIRES LIVE pH INPUT. 1066 AMP SENSOR WIRING 40106611 A Wiring 23 Section 4: Wiring December 2014 1066 Instruction Manual LIQ_MAN_1066 FIGurE 4-9. power/Current Loop wiring with wireless ThuM Adaptor 24 Wiring 1066 Instruction Manual LIQ_MAN_1066 Section 4: Wiring December 2014 FIGurE 4-10. hArT Loop power Wiring Wiring 25 Section 4: Wiring 1066 Instruction Manual December 2014 LIQ_MAN_1066 This page left intentionally blank 26 Wiring 1066 Instruction Manual Section 4: Wiring LIQ_MAN_1066 December 2014 Section 5: Intrinsically Safe Installation 5.1 All Intrinsically Safe Installations SCHEMATIC, INSTALLATION MODEL 1066 XMTR, (CSA) FIGurE 5-1. CSA Installation Intrinsically Safe Installation 27 Section 4: Wiring 1066 Instruction Manual December 2014 LIQ_MAN_1066 SCHEMATIC, INSTALLATION MODEL 1066 XMTR, (CSA) FIGurE 5-2. CSA Installation 28 Intrinsically Safe Installation Instruction Manual Section 5: Intrinsically Safe Installation LIQ_MAN_1066-P-HT December 2014 SCHEMATIC, INSTALLATION MODEL 1066 XMTR, (CSA) FIGurE 5-3. CSA Installation Intrinsically Safe Installation 29 Section 5: Intrinsically Safe Installation 1066 Instruction Manual December 2014 LIQ_MAN_1066 LABEL, INFO, 1066 CSA FIGurE 5-4. CSA Label Information 30 Intrinsically Safe Installation 1066 Instruction Manual Section 5: Intrinsically Safe Installation LIQ_MAN_1066 December 2014 Intrinsically Safe Installation 9241717-00 LABEL, INFO, 1066 ATEX FIGurE 5-5. ATEx, IECEx Label Information 31 Section 5: Intrinsically Safe Installation December 2014 1066 Instruction Manual LIQ_MAN_1066 SCHEMATIC, INSTALLATION MODEL 1066 XMTR, (FM) FIGurE 5-6. FM installation 32 Intrinsically Safe Installation 1066 Instruction Manual Section 5: Intrinsically Safe Installation LIQ_MAN_1066 December 2014 SCHEMATIC, INSTALLATION MODEL 1066 XMTR, (FM) FIGurE 5-7. FM installation Intrinsically Safe Installation 33 Section 5: Intrinsically Safe Installation 1066 Instruction Manual December 2014 LIQ_MAN_1066 SCHEMATIC, INSTALLATION MODEL 1066 XMTR, (FM) FIGurE 5-8. FM installation 34 Intrinsically Safe Installation 1066 Instruction Manual Section 5: Intrinsically Safe Installation LIQ_MAN_1066 December 2014 LABEL, INFO, 1066 FM FIGurE 5-9. FM label information Intrinsically Safe Installation 35 Section 5: Intrinsically Safe Installation 1066 Instruction Manual December 2014 LIQ_MAN_1066 This page left intentionally blank 36 Intrinsically Safe Installation 1066 Instruction Manual Section 6: Display and operation LIQ_MAN_1066 December 2014 Section 6: Display and Operation 6.1 user Interface The 1066 has a large display which shows the measurement readout and temperature in large digits and up to four additional process variables or diagnostic parameters concurrently. The displayed variables can be customized to meet user requirements. This is called display Format. The intuitive menu system allows access to Calibration, Hold (of current outputs), Programming, and Display functions. In addition, a dedicated DIAG button is available to provide access to useful operational information on installed sensor(s) and any problematic conditions that might occur. The display flashes Fault and/or Warning when these conditions occur. Help screens are displayed for most fault and warning conditions to guide the user in troubleshooting. During calibration and programming, key presses cause different displays to appear. The displays are self-explanatory and guide the user step-by-step through the procedure. 6.2 Instrument Keyboard There are four Function keys and four Selection keys on the instrument keypad. Function Keys: The MEnu key is used to access menus for programming and calibrating the instrument. Four toplevel menu items appear when pressing the MENU key: • Calibrate: calibrate the attached sensor and analog output(s). • Hold: Suspend current output(s). • Program: Program outputs, measurement, temperature, security and reset. • Display: Program display format, language, warnings, and contrast Pressing MEnu from the main (live values) screen always causes the main menu screen to appear. Pressing MENU followed by EXIT causes the main screen to appear. Pressing the DIAG key displays active Faults and Warnings, and provides detailed instrument information and sensor diagnostics including: Faults, Warnings, Sensor information, Out 1 and Out 2 live current values, model configuration string e.g. 1066-P-HT-60 and Instrument Software version. Pressing DIAG provides useful diagnostics and information (as applicable): Measurement, Sensor Type, Raw signal value, Cell constant, Zero Offset, Temperature, Temperature Offset, selected measurement range, Cable Resistance, Temperature Sensor Resistance, software version. The EnTEr key. Pressing ENTER stores numbers and settings and moves the display to the next screen. The ExIT key. Pressing EXIT returns to the previous screen without storing changes. Display and Operation 37 Section 6: Display and operation December 2014 1066 Instruction Manual LIQ_MAN_1066 Selection Keys: Surrounding the ENTER key, four Selection keys – up, down, right and left, move the cursor to all areas of the screen while using the menus. Selection keys are used to: 1. 2. 3. 4. 5. 6.3 Select items on the menu screens Scroll up and down the menu lists Enter or edit numeric values Move the cursor to the right or left Select measurement units during operations Main Display The 1066 displays the primary measurement value and temperature, and up to four secondary measurement values, a fault and warning banner, and a digital communications icon. process Measurements: One process variable and process temperature is displayed by default. For all configurations, the Upper display area shows the live process variable and the Center display area shows the Temperature (default screen settings). Secondary values: Up to four secondary values are shown in display quadrants at the bottom half of the screen. All four secondary value positions can be programmed by the user to any displayable parameter available. Fault and Warning Banner: If the transmitter detects a problem with itself or the sensor the word Fault or Warning will appear at the bottom of the display. A fault requires immediate attention. A warning indicates a problematic condition or an impending failure. For troubleshooting assistance, press Diag. Formatting the Main Display The main display screen can be programmed to show primary process variables, secondary process variables and diagnostics. 1. Press MENU 2. Scroll down to Display. Press EnTEr. 3. Main Format will be highlighted. Press EnTEr. 4. The sensor 1 process value will be highlighted in reverse video. Press the selection keys to navigate down to the screen sections that you wish to program. Press EnTEr. 5. Choose the desired display parameter or diagnostic for each of the four display sections in the lower screen. 6. Continue to navigate and program all desired screen sections. Press MEnu and ExIT. The screen will return to the main display. 38 Display and Operation 1066 Instruction Manual Section 6: Display and operation LIQ_MAN_1066 December 2014 The default display shows the live process measurement in the upper display area and temperature in the center display area. The user can elect to disable the display of temperature in the center display area using the Main Format function. See Fig. 4-1 to guide you through programming the main display to select process parameters and diagnostics of your choice. 6.4 Menu System The 1066 uses a scroll and select menu system. Pressing the MENU key at any time opens the top-level menu including Calibrate, Hold, Program and Display functions. To find a menu item, scroll with the up and down keys until the item is highlighted. Continue to scroll and select menu items until the desired function is chosen. To select the item, press ENTER. To return to a previous menu level or to enable the main live display, press the EXIT key repeatedly. To return immediately to the main display from any menu level, simply press MENU then EXIT. The selection keys have the following functions: • The Up key (above ENTER) increments numerical values, moves the decimal place one place to the right, or selects units of measurement. • The Down key (below ENTER) decrements numerical values, moves the decimal place one place to the left, or selects units of measurement • The Left key (left of ENTER) moves the cursor to the left. • The Right key (right of ENTER) moves the cursor to the right. To access desired menu functions, use the Quick Reference. During all menu displays (except main display format and Quick Start), the live process measurement and temperature value are displayed in the top two lines of the Upper display area. This conveniently allows display of the live values during important calibration and programming operations. Menu screens will time out after two minutes and return to the main live display. Display and Operation 39 Section 6: Display and operation 1066 Instruction Manual December 2014 LIQ_MAN_1066 This page left intentionally blank 40 Display and Operation 1066 Instruction Manual Section 7: Transmitter programming LIQ_MAN_1066 December 2014 Section 7: Programming the Transmitter – Basics 7.1 General Typical programming steps include the following listed procedures. Each of these programming functions are easily and quickly accomplished using the intuitive menu system. • Changing the measurement type, measurement units and temperature units. • Choose temperature units and manual or automatic temperature compensation mode • Configure and assign values to the current outputs • Set a security code for two levels of security access • Accessing menu functions using a security code • Enabling and disabling Hold mode for current outputs • Resetting all factory defaults, calibration data only, or current output settings only 7.2 Changing Startup Settings 7.2.1 Purpose To change the measurement type, measurement units, or temperature units that were initially entered in Quick Start, choose the Reset analyzer function or access the Program menus for the sensor. The following choices for specific measurement type, measurement units are available for each sensor measurement board. TABLE 7-1. Measurements and Measurement units Signal board Available measurements Measurements units: pH/ORP – P pH, ORP, Redox pH, mV (ORP, Redox) Contacting conductivity – C Conductivity, Resistivity, TDS, Salinity, NaOH (0-12%), HCl (0-15%), Low H2SO4, High H2SO4, NaCl (0-20%), Custom Curve Toroidal conductivity –T Chlorine – CL Conductivity, Resistivity, TDS, Salinity, NaOH (0-12%), HCl (0-15%), Low H2SO4, High H2SO4, NaCl (0-20%), Custom Curve Free Chlorine, Total Chlorine, Monochloramine Oxygen – DO Oxygen (ppm), Trace Oxygen (ppb), Percent Oxygen in gas Ozone – OZ Ozone Transmitter Programming μS/cm, mS/cm, S/cm % (concentration) μS/cm, mS/cm, S/cm % (concentration) ppm, mg/L ppm, mg/L, ppb, µg/L % Sat, Partial Pressure, % Oxygen In Gas, ppm Oxygen In Gas ppm, mg/L, ppb, μg/L 41 Section 7: Transmitter programming 1066 Instruction Manual December 2014 7.2.2 LIQ_MAN_1066 Procedure Follow the Reset Analyzer procedure (Sec 7.8) to reconfigure the transmitter to display new measurements or measurement units. To change the specific measurement or measurement units for each measurement type, refer to the Program menu for the appropriate measurement (Sec. 6.0). 7.3 Choosing Temperature units and Automatic/Manual Temperature Compensation 7.3.1 Purpose Most liquid analytical measurements (except ORP and Redox) require temperature compensation. The 1066 performs temperature compensation automatically by applying internal temperature correction algorithms. Temperature correction can also be turned off. If temperature correction is off, the 1066 uses the temperature entered by the user in all temperature correction calculations. 1.234µS/cm 25.0ºC Temperature Units: °C Temp Comp: Auto Manual: +25.0°C 7.4 Configuring and ranging Current outputs 7.4.1 Purpose The 1066 has two analog current outputs. Ranging the outputs means assigning values to the low (4 mA) and high (20 mA) outputs. This section provides a guide for configuring and ranging the outputs. ALWAYS CONFIGURE THE OUTPUTS FIRST. 7.4.2 Definitions 1. CURRENT OUTPUTS. The transmitter provides a continuous output current (4-20 mA) directly proportional to the process variable or temperature. The low and high current outputs can be set to any value. 2. ASSIGNING OUTPUTS. Assign a measurement or temperature to Output 1 or Output 2. 3. DAMPEN. Output dampening smooths out noisy readings. It also increases the response time of the output. Output dampening does not affect the response time of the display. 4. MODE. The current output can be made directly proportional to the displayed value (linear mode) or directly proportional to the common logarithm of the displayed value (log mode). 7.4.3 Procedure: Configure Outputs Under the Program/Outputs menu, the adjacent screen will appear to allow configuration of the outputs. Follow the menu screens in Fig. 7-1 to configure the outputs. 1.234µS/cm 25.0ºC OutputM Configure Assign: Meas Scale: Linear Dampening: 0sec Fault Mode: Fixed Fault Value: 21.00mA 42 Transmitter Programming 1066 Instruction Manual Section 7: Transmitter programming LIQ_MAN_1066 December 2014 FIGurE 7-1. Configuring and ranging the Current outputs 1.234µS/cm Program MAIN MENU Range 1.234µS/cm 25.0ºC Program Outputs Outputs Measurement Temperature 25.0ºC 1.234µS/cm Output Range 1.234µS/cm 25.0ºC Outputs Range Configure Simulate Security Diagnostic Setup Reset Analyzer O1 SN 4mA: O1 SN 20mA: O2 SN 4mA: S2 20mA: 1.234µS/cm Configure 0.000 20.00 0ºC 100ºC 25.0ºC Output Configure Output1 Output2 OM 4mA: 1.000 OM 20mA: 1.000% OM 4mA: 1.000% OM 20mA: 7.0 pH 1.234µS/cm 1.234µS/cm 25.0ºC 25.0ºC OutputM Assign OutputM Configure Assign: Range: Scale: Dampening: Simulate 25.0ºC Output Range S1 Measurement S1 Temperature S1 Meas 4-20mA Linear 0sec 1.234µS/cm 25.0ºC OutputM Range 1.234µS/cm 25.0ºC Simulate Output 1 Output 2 1.234µS/cm 4-20mA 0-20mA 25.0ºC OutputN Hold At 12.00mA 1.234µS/cm 25.0ºC Scale Linear Log 7.4.4 Procedure: Ranging the Current Outputs The adjacent screen will appear under Program/Output/Range. Enter a value for 4mA and 20mA for each output. Follow the menu screens in Fig. 7-1 to assign values to the outputs. 7.5 Setting a Security Code 7.5.1 Purpose 1.234µS/cm O1 O1 O2 O2 SN SN SN SN 25.0ºC Output 4mA: 20mA: 4mA: 20mA: Range 0.000µS/cm 20.00µS/cm 0°C 100°C The security codes prevent accidental or unwanted changes to program settings, displays, and calibration. The 1066 has two levels of security code to control access and use of the instrument to different types of users. The two levels of security are: • All: This is the Supervisory security level. It allows access to all menu functions, including Programming, Calibration, Hold and Display. • Calibration/hold: This is the operator or technician level menu. It allows access to only calibration and Hold of the current outputs. 7.5.2 Procedure 1. Press MENU. The main menu screen appears. Choose program. 2. Scroll down to Security. Select Security. 3. The security entry screen appears. Enter a three digit security code for each of the desired security levels. The security code takes effect two minutes after the last key stroke. Record the security code(s) for future access and communication to operators or technicians as needed. 4. The display returns to the security menu screen. Press EXIT to return to the previous screen. To return to the main display, press MENU followed by EXIT. Fig. 7-2 displays the security code screens. Transmitter Programming 43 Section 7: Transmitter programming 1066 Instruction Manual December 2014 LIQ_MAN_1066 Program MAIN MENU FIGurE 7-2. Setting a Security Code 1.234µS/cm 25.0ºC Program Outputs Measurement Temperature 1.234µS/cm Security 25.0ºC Security Calibration/Hold: 000 All: 000 Diagnostic Setup Reset Analyzer 7.6 Security Access 7.6.1 How the Security Code Works When entering the correct access code for the Calibration/Hold security level, the Calibration and Hold menus are accessible. This allows operators or technicians to perform routine maintenance. This security level does not allow access to the Program or Display menus. When entering the correct access code for All security level, the user has access to all menu functions, including Programming, Calibration, Hold and Display. 7.6.2 Procedure 1. If a security code has been programmed, selecting the Calibrate, Hold, Program or Display top menu items causes the security access screen to appear 2. Enter the three-digit security code for the appropriate security level. 1.234µS/cm 25.0ºC Security Code 3. If the entry is correct, the appropriate menu screen appears. If the 000 entry is incorrect, the Invalid Code screen appears. The Enter Security Code screen reappears after 2 seconds. 7.7 using hold 7.7.1 Purpose The transmitter output is always proportional to measured value. To prevent improper operation of systems or pumps that are controlled directly by the current output, place the analyzer in hold before removing the sensor for calibration and maintenance. Be sure to remove the transmitter from hold once calibration is complete. During hold, both outputs remain at the last value. Once in hold, all current outputs remain on Hold indefinitely. 44 Transmitter Programming 1066 Instruction Manual Section 7: Transmitter programming LIQ_MAN_1066 December 2014 7.7.2 Hold MAIN MENU FIGurE 7-3. using hold 1.234µS/cm 25.0ºC Hold Hold: No 1.234µS/cm 25.0ºC Hold outputs? No Yes Using the Hold Function To hold the outputs, 1. Press MENU. The main menu screen appears. Choose hold. 2. The hold outputs? screen appears. Choose Yes to place the analyzer in hold. Choose no to take the analyzer out of hold. 3. The Hold screen will then appear and hold will remain on indefinitely until hold is disabled. See Figure 7-3. 7.8 resetting Factory Default Settings 7.8.1 Purpose This section describes how to restore factory calibration and default values. The process also clears all fault messages and returns the display to the first Quick Start screen. The 1066 offers three options for resetting factory defaults. 1. Reset all settings to factory defaults 2. Reset sensor calibration data only 3. Reset analog output settings only 7.8.2 Procedure To reset to factory defaults, reset calibration data only or reset analog outputs only, follow the Reset Analyzer flow diagram. Transmitter Programming 45 Section 7: Transmitter programming December 2014 1066 Instruction Manual LIQ_MAN_1066 FIGurE 7-4. resetting Factory Default Settings 46 Transmitter Programming 1066 Instruction Manual Section 8: programming Measurements LIQ_MAN_1066 December 2014 Section 8: Programming Measurements 8.1 Introduction The 1066 automatically recognizes the measurement input upon first power-up and each time the transmitter is powered. Completion of Quick Start screens upon first power up enable measurements, but additional steps may be required to program the transmitter for the desired measurement application. This section covers the following programming and configuration functions: 1. Selecting measurement type or sensor type (all sections) 2. Identifying the preamp location (pH-see Sec. 8.2) 3. Enabling manual temperature correction and entering a reference temperature (all sections) 4. Enabling sample temperature correction and entering temperature correction slope (selected sections) 5. Defining measurement display resolution (pH and amperometric) 6. Defining measurement display units (all sections) 7. Adjusting the input filter to control display and output reading variability or noise (all sections) 8. Selecting a measurement range (conductivity – see Secs 8.4, 8.5) 9. Entering a cell constant for a contacting or toroidal sensor (see Secs 8.4, 8.5) 10. Creating an application-specific concentration curve (conductivity-see Secs 8.4, 8.5) 11. Enabling automatic pH correction for free chlorine measurement (Sec. 8.6.1) To fully configure the transmitter, you may use the following: 1. Reset Transmitter function to reset factory defaults and configure to the desired measurement. Follow the Reset Transmitter menu to reconfigure the transmitter to display new measurements or measurement units. 2. Program menus to adjust any of the programmable configuration items. Use the following configuration and programming guidelines for the applicable measurement. Programming Measurements 47 Section 8: programming Measurements 1066 Instruction Manual December 2014 LIQ_MAN_1066 8.2 ph Measurement programming 8.2.1 Description The section describes how to configure the 1066 transmitter for pH measurements. The following programming and configuration functions are covered. 1. Measurement type: pH Select pH, ORP, Redox. 2. Preamp location: Transmitter Identify preamp location (automatic detection for SMART pH sensors) 3. Filter: 4 sec Override the default input filter, enter 0-999 seconds 4. Reference Z: Low Select low or high reference impedance 5. Resolution: 0.01pH Select 0.01pH or 0.1pH for pH display resolution To configure pH: 1. Press MEnu 2. Scroll down to program. Press ENTER. 3. Scroll down to Measurement. Press ENTER. The adjacent screen format will appear (factory defaults are shown). To program any function, scroll to the desired item and press ENTER. 1.234µS/cm 25.0ºC SN Configure Measure: pH Preamp: Analyzer Sol’n Temp Corr: Off Resolution: 0.01pH Filter: 4 sec Reference Z: Low The following sub-sections provide you with the initial display screen that appears for each configuration function. Use the flow diagram for pH programming and the 1066 live screen prompts for each function to complete configuration and programming. 8.2.2 Measurement The display screen for selecting the measurement is shown. The default value is displayed in bold type. Refer to the pH/ORP Programming flow diagram to complete this function. 8.2.3 1.234µS/cm 25.0ºC SN Measurement pH ORP Redox Preamp The display screen for identifying the Preamp location is shown. The default value is displayed in bold type. Refer to the pH/ORP Programming flow diagram to complete this function. 1.234µS/cm 25.0ºC SN Preamp Analyzer Sensor/JBox note: Sensor/JBox must be selected to support SMART pH sensors from Rosemount Analytical. 48 Programming Measurements 1066 Instruction Manual Section 8: programming Measurements LIQ_MAN_1066 8.2.4 December 2014 Solution Temperature Correction The display screen for selecting the Solution temperature correction algorithm is shown. The default value is displayed in bold type. Refer to the pH/ORP Programming flow diagram to complete this function. 8.2.5 Resolution The display screen for selecting 0.01pH or 0.1pH for pH display resolution is shown. The default value is displayed in bold type. Refer to the pH/ORP Programming flow diagram to complete this function. 8.2.7 25.0ºC 1.234µS/cm 25.0ºC SN Resolution 0.01pH 0.1pH 1.234µS/cm 25.0ºC SN Input filter 04 sec Reference Impedance The display screen for selecting Low or High Reference impedance is shown. The default value is displayed in bold type. Refer to the pH/ORP Programming flow diagram to complete this function. 8.3 1.234µS/cm SN Sol’n Temp Coeff. - 0.032pH/ºC Filter The display screen for entering the input filter value in seconds is shown. The default value is displayed in bold type. Refer to the pH/ORP Programming flow diagram to complete this function. 8.2.8 25.0ºC Temperature Coefficient The display screen for entering the custom solution temperature coefficient is shown. The default value is displayed in bold type. Refer to the pH/ORP Programming flow diagram to complete this function. 8.2.6 1.234µS/cm SN Sol’n Temp Corr. Off Ultra Pure Water High pH Custom 1.234µS/cm 25.0ºC SN Reference Z Low High orp Measurement programming The section describes how to configure the 1066 transmitter for ORP measurements. The following programming and configuration functions are covered: 1. Measurement type: pH Select pH, ORP, Redox. 2. Preamp location: Transmitter Identify preamp location 3. Filter: 4 sec Override the default input filter, enter 0-999 seconds 4. Reference Z: Low Select low or high reference impedance 5. Sensor wiring scheme: Normal or Reference to Ground Programming Measurements 49 Section 8: programming Measurements 1066 Instruction Manual December 2014 LIQ_MAN_1066 To configure ORP: 1. Press MEnu 2. Scroll down to program. Press ENTER. 3. Scroll down to Measurement. Press ENTER. 1.234µS/cm 25.0ºC SN Configure Measure: pH Preamp: Analyzer Flter: 4 sec Reference Z: Low The adjacent screen format will appear (factory defaults are shown). To program any displayed function, scroll to the desired item and press ENTER. The following sub-sections provide you with the initial display screen that appears for each configuration function. Use the flow diagram for orp programming at the end of Sec. 6 and the 1066 live screen prompts for each function to complete configuration and programming. 8.3.1 Measurement The display screen for selecting the measurement is shown. The default value is displayed in bold type. Refer to the pH/ORP Programming flow diagram to complete this function. 8.3.2 1.234µS/cm pH ORP Redox Preamp 1.234µS/cm The display screen for identifying the Preamp location is shown. The default value is displayed in bold type. Refer to the pH/ORP Programming flow diagram to complete this function. 8.3.3 Reference Impedance The display screen for Selecting Low or high Reference impedance is shown. The default value is displayed in bold type. Refer to the pH/ORP Programming flow diagram to complete this function. 50 25.0ºC SN Preamp Analyzer Sensor/JBox Filter The display screen for entering the input filter value in seconds is shown. The default value is displayed in bold type. Refer to the pH/ORP Programming flow diagram to complete this function. 8.3.4 25.0ºC SN Measurement 1.234µS/cm 25.0ºC SN Input filter 04 sec 1.234µS/cm 25.0ºC SN Reference Z Low High Programming Measurements 1066 Instruction Manual Section 8: programming Measurements LIQ_MAN_1066 December 2014 8.4 Contacting Conductivity Measurement programming 8.4.1 Description The section describes how to configure the 1066 transmitter for conductivity measurements using contacting conductivity sensors. The following programming and configuration functions are covered. 1. Measure: Conductivity Select Conductivity, Resistivity, TDS. Salinity or % conc 2. Type: 2-Electrode Select 2-Electrode or 4-Electrode type sensors 3. Cell K: 1.00000/cm Enter the cell Constant for the sensor 4. Measurement units 5. Filter: 2 sec Override the default input filter, enter 0-999 seconds 6. Range: Auto Select measurement Auto-range or specific range 7. Temp Comp: Slope Select Temp Comp: Slope, Neutral Salt, Cation or Raw 8. Slope: 2.00%/°C Enter the linear temperature coefficient 9. Ref Temp: 25.0°C Enter the Reference temp 10. Cal Factor: default=0.95000/cm Enter the Cal Factor for 4-Electrode sensors from the sensor tag 1.234µS/cm To configure the contacting conductivity: 1. Press MENU 2. Scroll down to Program. Press ENTER. 3. Scroll down to Measurement. Press ENTER. The adjacent screen format will appear (factory defaults are shown). To program any displayed function, scroll to the desired item and press ENTER. 25.0ºC SN Configure Type: 2-Electrode Measure: Cond Range: Auto Cell K: 1.00000/cm RTD Offset: 0.00ºC RTD Slope: 0 Temp Comp: Slope Slope: 2.00%/°C Ref Temp: 25.0°C Filter: 2 sec Custom Setup The following sub-sections provide you with the initial display screen that appears for each configuration function. Use the flow diagram for contacting conductivity programming at the end of Sec. 8 and the 1066 live screen prompts for each function to complete configuration and programming. 8.4.2 Sensor Type The display screen for selecting 2-Electrode or 4-Electrode type sensors is shown. The default value is displayed in bold type. Refer to the contacting conductivity Programming flow diagram to complete this function. Programming Measurements 1.234µS/cm 25.0ºC SN Type 2-Electrode 4-Electrode 51 Section 8: programming Measurements 1066 Instruction Manual December 2014 8.4.3 LIQ_MAN_1066 Measure The display screen for selecting the measurement is shown. The default value is displayed in bold type. Refer to the contacting conductivity Programming flow diagram to complete this function. 1.234µS/cm 25.0ºC SN Measurement Conductivity Resistivity TDS Salinity NaOH (0-12%) HCl (0-15%) Low H2SO4 High H2SO4 NaCl (0-20%) Custom Curve 8.4.4 Range The display screen for Selecting Auto-ranging or a specific range is shown. The default value is displayed in bold type. Note: Ranges are shown as conductance, not conductivity. Refer to the contacting conductivity Programming flow diagram to complete this function. 8.4.5 Cell Constant 8.4.6 RTD Offset The display screen for entering a cell Constant for the sensor is shown. The default value is displayed in bold type. Refer to the contacting conductivity Programming flow diagram to complete this function. The display screen for Entering the RTD Offset for the sensor is shown. The default value is displayed in bold type. Refer to the contacting conductivity Programming flow diagram to complete this function. 8.4.7 8.4.8 RTD Slope The display screen for entering the RTD slope for the sensor is shown. The default value is displayed in bold type. Refer to the contacting conductivity Programming flow diagram to complete this function. Temp Comp The display screen for Selecting Temperature Compensation as Slope, Neutral Salt, Cation or Raw is shown. The default value is displayed in bold type. Refer to the contacting conductivity Programming flow diagram to complete this function. 52 1.234µS/cm 25.0ºC SN Range Auto 50 µS 500 µS 2000 µS 20 mS 200 mS 600 mS 1.234µS/cm 25.0ºC SN Cell Constant 1.00000 /cm 1.234µS/cm 25.0ºC SN RTD Offset 0.00°C 1.234µS/cm 25.0ºC SN RTD Slope 2.00%/ºC 1.234µS/cm 25.0ºC SN Temp Comp Slope Neutral Salt Cation Raw Programming Measurements 1066 Instruction Manual Section 8: programming Measurements LIQ_MAN_1066 December 2014 8.4.9 Slope 8.4.10 Reference Temp The display screen for Entering the conductivity/temp Slope is shown. The default value is displayed in bold type. Refer to the contacting conductivity Programming flow diagram to complete this function. The display screen for manually entering the Reference temperature is shown. The default value is displayed in bold type. Refer to the contacting conductivity Programming flow diagram to complete this function. 8.4.11 8.4.12 Filter The display screen for entering the input filter value in seconds is shown. The default value is displayed in bold type. Refer to the contacting conductivity Programming flow diagram to complete this function. Custom Setup 1.234µS/cm 1.234µS/cm 25.0ºC SN Ref Temp (25.0ºC normal) +25.0ºC 1.234µS/cm 25.0ºC SN Input filter 02 sec 1.234µS/cm 25.0ºC The display screens for creating a custom curve for converting conductivity to concentration is shown. Refer to the contacting conductivity Programming flow diagram to complete this function. SN Custom Curve Configure Enter Data Points Calculate Curve When the custom curve data entry is complete, press ENTER. The display will confirm the determination of a custom curve fit to the entered data by displaying this screen: SN Calculate Curve Custom curve fit completed. In Process Cal recommended. If the custom curve fit is not completed or is unsuccessful, the display will read as follows and the screen will return to the beginning custom curve screen. SN Calculate Curve Failure 1.234µS/cm 8.4.13 25.0ºC SN Slope 2.00 %/ºC 1.234µS/cm 25.0ºC 25.0ºC Cal Factor Upon initial installation and power up, if 4-electrode was selected for the sensor type in the Quick Start menus, the user enters a Cell Constant and a “Cal Factor” using the instrument keypad. The cell constant is needed to convert measured conductance to conductivity as displayed on the transmitter screen. The “Cal Factor” entry is needed increase the accuracy of the live conductivity readings, especially at low conductivity readings below 20uS/cm. Both the Cell Constant and the “Cal Factor” are printed on the tag attached to the 4-electrode sensor/cable. Programming Measurements 1.234µS/cm 25.0ºC SN Cal Factor 0.95000/cm 53 Section 8: programming Measurements 1066 Instruction Manual December 2014 LIQ_MAN_1066 8.5 Toroidal Conductivity Measurement programming 8.5.1 Description The section describes how to configure the 1066 transmitter for conductivity measurements using inductive/toroidal sensors. The following programming and configuration functions are covered: 1. Measure: Conductivity Select Conductivity, Resistivity, TDS. Salinity or % conc 2. Sensor Model: 228 Select sensor type 3. Measurement units 4. Range selection 5. Cell K: 3.00000/cm Enter the cell Constant for the sensors 6. Temp Comp: Slope Select Temp Comp: Slope, Neutral Salt, Cation or Raw 7. Slope: 2.00%/°C Enter the linear temperature coefficient 8. Ref Temp: 25.0°C Enter the Reference temp 9. Filter: 2 sec Override the default input filter, enter 0-999 seconds To configure toroidal conductivity: 1. Press MENU 2. Scroll down to Program. Press ENTER. 3. Scroll down to Measurement. Press ENTER. The adjacent screen format will appear (factory defaults are shown). To program any displayed function, scroll to the desired item and press ENTER. 1.234µS/cm 25.0ºC SN Configure Model: 228 Measure: Cond Range: Auto Cell K: 3.00000/cm RTD Offset: 0.00ºC RTD Slope: 0 Temp Comp: Slope Slope: 2.00%/°C Ref Temp: 25.0°C Filter: 2 sec Custom Setup The following sub-sections provide you with the initial display screen that appears for each configuration function. Use the flow diagram for toroidal conductivity programming at the end of Sec. 8 and the 1066 live screen prompts for each function to complete configuration and programming. 8.5.2 Sensor Type The display screen for selecting the sensor model is shown. The default value is displayed in bold type. Refer to the toroidal conductivity Programming flow diagram to complete this function. 1.234µS/cm 25.0ºC SN Model 228 225 226 247 Other 54 Programming Measurements 1066 Instruction Manual Section 8: programming Measurements LIQ_MAN_1066 8.5.3 December 2014 Measure The display screen for selecting the measurement is shown. The default value is displayed in bold type. Refer to the toroidal conductivity Programming flow diagram to complete this function. 1.234µS/cm 25.0ºC Measurement Conductivity Resistivity TDS Salinity NaOH (0-12%) HCl (0-15%) Low H2SO4 High H2SO4 NaCl (0-20%) Custom Curve 8.5.4 Range The display screen for Selecting Auto-ranging or a specific range is shown. The default value is displayed in bold type. Note: Ranges are shown as conductance, not conductivity. Refer to the toroidal conductivity Programming flow diagram to complete this function. noTE: when manually changing ranges, a zero calibration and recalibration in a solution of known conductivity must be performed with the toroidal sensor wired to the instrument. refer to sec. 9.5.2 zeroing the Instrument and sec. 9.5.3 Calibrating the Sensor in a Conductivity Standard. 8.5.5 1.234µS/cm 25.0ºC SN Range Auto 50-600 µS 0.5-100 mS 90-1500 mS Cell Constant The display screen for entering a cell Constant for the sensor is shown. The default value is displayed in bold type. Refer to the toroidal conductivity Programming flow diagram to complete this function. 1.234µS/cm 25.0ºC Cell Constant 2.7000 /cm noTE: When manually changing ranges, the Cell Constant may change through the calibration process. 8.5.6 Temp Comp The display screen for Selecting Temperature Compensation as Slope, Neutral Salt, or Raw is shown. The default value is displayed in bold type. Refer to the toroidal conductivity Programming flow diagram to complete this function. Programming Measurements 1.234µS/cm 25.0ºC Temp Comp Slope Raw 55 Section 8: programming Measurements 1066 Instruction Manual December 2014 8.5.7 LIQ_MAN_1066 Slope The display screen for Entering the conductivity/temp Slope is shown. The default value is displayed in bold type. Refer to the toroidal conductivity Programming flow diagram to complete this function. 8.5.8 Ref Temp 8.5.9 Filter The display screen for manually Entering the Reference temperature is shown. The default value is displayed in bold type. Refer to the toroidal conductivity Programming flow diagram to complete this function. The display screen for entering the input filter value in seconds is shown. The default value is displayed in bold type. Refer to the toroidal conductivity Programming flow diagram to complete this function. 1.234µS/cm 25.0ºC SN Slope 2.00%/ºC 1.234µS/cm 25.0ºC SN Ref Temp (25.0ºC normal) +25.0ºC 1.234µS/cm 25.0ºC SN Input filter 02 sec using the highest range (90mS to 1500mS) in very low conductivity processes below 100µS (conductance) might generate a high noise value relative to the actual process value. In these cases, it is recommended to increase the input filter setting above the default value of 2 sec. to suppress the effect of noise. 8.5.10 Custom Setup The display screens for creating custom curves for converting conductivity to concentration is shown. Refer to the toroidal conductivity Programming flow diagram to complete this function. When the custom curve data entry is complete, press ENTER. The display will confirm the determination of a custom curve fit to the entered data by displaying this screen: If the custom curve fit is not completed or is unsuccessful, the display will read as follows and the screen will return to the beginning custom curve screen. 56 1.234µS/cm 25.0ºC SN Custom Curve Configure Enter Data Points Calculate Curve 1.234µS/cm 25.0ºC SN Calculate Curve Custom curve fit completed. In Process Cal recommended. 1.234µS/cm 25.0ºC SN Calculate Curve Failure Programming Measurements 1066 Instruction Manual Section 8: programming Measurements LIQ_MAN_1066 8.6 December 2014 Chlorine Measurement programming The 1066 can measure any of three variants of Chlorine: • Free Chlorine • Total Chlorine • Monochloramine The section describes how to configure the 1066 transmitter for Chlorine measurements. 8.6.1 Free Chlorine Measurement Programming This Chlorine sub-section describes how to configure the 1066 transmitter for Free Chlorine measurement using amperometric chlorine sensors. Automatic temperature compensation is available using Auto or Manual pH correction. For maximum accuracy, use automatic temperature compensation. The following programming and configuration functions are covered: 1. Measure: Free Chlorine Select Free Chlorine, Total Cl, Monochloramine 2. Units: ppm Select units ppm or mg/L 3 Resolution: 0.001 Select display resolution 0.01 or 0.001 4. Free Cl Correct: Live Select Live/Continuous pH correction or Manual 5. Manual pH: 7.00 pH For Manual pH correction, enter the pH value 6. Filter: 5sec Override the default input filter, enter 0-999 seconds To configure chlorine for free chlorine: 1. Press MENU 2. Scroll down to Program. Press ENTER. 3. Scroll down to Measurement. Press ENTER. The adjacent screen format will appear (factory defaults are shown). To program any displayed function, scroll to the desired item and press ENTER. 1.234µS/cm 25.0ºC SN Configure Measure: Free Chlorine Units: ppm Filter: 5sec Free Cl Correct: Live Manual pH: 7.00 pH Resolution: 0.001 The following sub-sections provide you with the initial display screen that appears for each configuration function. Use the flow diagram for chlorine programming at the end of Sec. 8 and the 1066 live screen prompts for each function to complete configuration and programming. Programming Measurements 57 Section 8: programming Measurements 1066 Instruction Manual December 2014 LIQ_MAN_1066 8.6.1.1 Measure 8.6.1.2 Units 8.6.1.3 8.6.1.4 The display screen for selecting the measurement is shown. The default value is displayed in bold type. Refer to the Chlorine Programming flow diagram to complete this function. The display screen for selecting units as ppm or mg/L is shown. The default value is displayed in bold type. Refer to the Chlorine Programming flow diagram to complete this function. Filter The display screen for entering the input filter value in seconds is shown. The default value is displayed in bold type. Refer to the Chlorine Programming flow diagram to complete this function. Free Chlorine pH Correction The display screen for Selecting Live/Continuous pH correction or Manual pH correction is shown. The default value is displayed in bold type. Refer to the Chlorine Programming flow diagram to complete this function. 8.6.1.5 8.6.1.6 58 Manual pH Correction The display screen for manually entering the pH value of the measured process liquid is shown. The default value is displayed in bold type. Refer to the Chlorine Programming flow diagram to complete this function. Resolution The display screen for selecting display resolution as 0.001 or 0.01 is shown. The default value is displayed in bold type. Refer to the Chlorine Programming flow diagram to complete this function. 1.234µS/cm 25.0ºC SN Measurement Free Chlorine Total Chlorine Monochloramine 1.234µS/cm 25.0ºC SN Units ppm mg/L 1.234µS/cm 25.0ºC SN Input filter 05 sec 1.234µS/cm 25.0ºC SN Free Cl pH Correction Live/Continuous Manual 1.234µS/cm 25.0ºC SN Manual pH 07.00 pH 1.234µS/cm 25.0ºC SN Resolution 0.001 0.01 Programming Measurements 1066 Instruction Manual Section 8: programming Measurements LIQ_MAN_1066 8.6.2 8.6.2.1 December 2014 Total Chlorine Measurement Programming Description This Chlorine sub-section describes how to configure the 1066 transmitter for Total Chlorine measurement using amperometric chlorine sensors. The following programming and configuration functions are covered: 1. Measure: Free Chlorine Select Free Chlorine, pH Ind. Free Cl. Total Cl, Monochloramine 2. Units: ppm Select units ppm or mg/L 3. Resolution: 0.001 Select display resolution 0.01 or 0.001 4. Filter: 5sec Override the default input filter, enter 0-999 seconds To configure chlorine measurement for total chlorine: 1. Press MENU 2. Scroll down to Program. Press ENTER. 3. Scroll down to Measurement. Press ENTER. 1.234µS/cm 25.0ºC SN Configure Measure: Free Chlorine Units: ppm Filter: 5sec Resolution: 0.001 The adjacent screen format will appear (factory defaults are shown). To program any displayed function, scroll to the desired item and press ENTER. The following sub-sections provide you with the initial display screen that appears for each configuration function. Use the flow diagram for chlorine programming at the end of Sec. 6 and the 1066 live screen prompts for each function to complete configuration and programming. 8.6.2.2 Measure 8.6.2.3 Units 8.6.2.4 The display screen for selecting the measurement is shown. The default value is displayed in bold type. Refer to the chlorine Programming flow diagram to complete this function. The display screen for selecting units as ppm or mg/L is shown. The default value is displayed in bold type. Refer to the Chlorine Programming flow diagram to complete this function Filter The display screen for entering the input filter value in seconds is shown. The default value is displayed in bold type. Refer to the Chlorine Programming flow diagram to complete this function. Programming Measurements 1.234µS/cm 25.0ºC SN Measurement Free Chlorine Total Chlorine Monochloramine 1.234µS/cm 25.0ºC SN Units ppm mg/L 1.234µS/cm 25.0ºC SN Input filter 05 sec 59 Section 8: programming Measurements 1066 Instruction Manual December 2014 8.6.2.5 8.6.3 LIQ_MAN_1066 Resolution 1.234µS/cm The display screen for selecting display resolution as 0.001 or 0.01 is shown. The default value is displayed in bold type. Refer to the Chlorine Programming flow diagram to complete this function. 25.0ºC SN Resolution 0.001 0.01 Monochloramine Measurement Programming This Chlorine sub-section describes how to configure the 1066 transmitter for Monochloramine measurement using amperometric chlorine sensors. The following programming and configuration functions are covered: 1. Measure: Free Chlorine Select Free Chlorine, pH Ind. Free Cl. Total Cl, Monochloramine 2. Units: ppm Select units ppm or mg/L 3. Resolution: 0.001 Select display resolution 0.01 or 0.001 4. Filter: 5sec Override the default input filter, enter 0-999 seconds To configure chlorine for monochloramine: 1. Press MENU 2. Scroll down to Program. Press ENTER. 3. Scroll down to Measurement. Press ENTER. 1.234µS/cm 25.0ºC SN Configure Measure: Free Chlorine Units: ppm 5sec Filter: Resolution: 0.001 The following screen format will appear (factory defaults are shown). To program any displayed function, scroll to the desired item and press ENTER. The following sub-sections provide you with the initial display screen that appears for each configuration function. Use the flow diagram for chlorine programming at the end of Sec. 8 and the 1066 live screen prompts for each function to complete configuration and programming. 8.6.3.1 8.6.3.2 Measure: Monochloramine The display screen for selecting the measurement is shown. The default value is displayed in bold type. Refer to the Chlorine Programming flow diagram to complete this function. Units The display screen for selecting units as ppm or mg/L is shown. The default value is displayed in bold type. Refer to the Chlorine Programming flow diagram to complete this function. 60 1.234µS/cm 25.0ºC SN Measurement Free Chlorine Total Chlorine Monochloramine 1.234µS/cm 25.0ºC SN Units ppm mg/L Programming Measurements 1066 Instruction Manual Section 8: programming Measurements LIQ_MAN_1066 8.6.3.3 8.6.3.4 December 2014 Filter The display screen for entering the input filter value in seconds is shown. The default value is displayed in bold type. Refer to the Chlorine Programming flow diagram to complete this function. Resolution The display screen for selecting display resolution as 0.001 or 0.01 is shown. The default value is displayed in bold type. Refer to the Chlorine Programming flow diagram to complete this function. 8.7 1.234µS/cm 25.0ºC SN Input filter 05 sec 1.234µS/cm 25.0ºC SN Resolution 0.001 0.01 oxygen Measurement programming This section describes how to configure the 1066 transmitter for dissolved and gaseous oxygen measurement using amperometric oxygen sensors. The following programming and configuration functions are covered: 1. Sensor type: Select Water/Waste, Trace. BioRx, BioRx-Other, Brew, %O2 In Gas 2. Measure type: Select Concentration, % Saturation, Partial Pressure, Oxygen in Gas 3. Units: ppm Select ppm, mg/L, ppb, g/L, % Sat, %O2-Gas, ppm Oxygen-Gas 4. Pressure Units: bar Select pressure units: mm Hg, in Hg, Atm, kPa, mbar, bar 5. Salinity: 00.0‰ Enter Salinity as ‰ 6. Filter: 5sec Override the default input filter, enter 0-999 seconds 7. Partial Press: mmHg Select mm Hg, in Hg. atm, kPa, mbar or bar for Partial pressure To configure Oxygen: 1. Press MENU 2. Scroll down to Program. Press ENTER. 3. Scroll down to Measurement. Press ENTER. The adjacent screen format will appear (factory defaults are shown). To program any displayed function, scroll to the desired item and press ENTER. 1.234µS/cm 25.0ºC SN Configure Type: Water/Waste Units: ppm Partial Press: mmHg Salinity: 00.0‰ Filter: 5sec Pressure Units: bar Use Press: At Air Cal Custom Setup The following sub-sections show the initial display screen that appears for each configuration function. Use the flow diagram for oxygen programming at the end of Sec. 6 and the 1066 live screen prompts for each function to complete configuration and programming. Programming Measurements 61 Section 8: programming Measurements 1066 Instruction Manual December 2014 LIQ_MAN_1066 1.234µS/cm 8.7.1 8.7.2 25.0ºC SN Type Water/Waste Trace Oxygen BioRx-Rosemount BioRx-Other Oxygen Measurement application The display screen for programming the measurement is shown. The default value is displayed in bold type. Refer to the Oxygen Programming flow diagram to complete this function. Brewing Oxygen In Gas Units 1.234µS/cm The display screen for selecting units as ppm , mg/L, ppb, μg/L, % Saturation, %Oxygen in Gas, or ppm Oxygen in Gas is shown. The default value is displayed in bold type. Refer to the Oxygen Programming flow diagram to complete this function. 25.0ºC SN Units ppm mg/L ppb µg/L % Saturation Partial Pressure % Oxygen In Gas ppm Oxygen In Gas 8.7.3 Partial Press 8.7.4 Salinity 1.234µS/cm The display screen for selecting pressure units for Partial pressure is shown. This selection is needed if the specified measurement is Partial pressure. The default value is displayed in bold type. Refer to the Oxygen Programming flow diagram to complete this function. The display screen for Entering the Salinity (as parts per thousand) of the process liquid to be measured is shown. The default value is displayed in bold type. Refer to the Oxygen Programming flow diagram to complete this function. 25.0ºC SN Partial Press mm Hg in Hg atm kPa mbar bar 1.234µS/cm 25.0ºC SN Salinity 00.0 ‰ Enter Salinity as ‰ 8.7.5 8.7.6 62 Filter The display screen for entering the input filter value in seconds is shown. The default value is displayed in bold type. Refer to the Oxygen Programming flow diagram to complete this function. Pressure Units 1.234µS/cm 05 sec 1.234µS/cm The display screen for selecting pressure units for atmospheric pressure is shown. This selection is needed for the display of atmospheric pressure. The default value is displayed in bold type. The user must enter a known value for local atmospheric pressure. Refer to the Oxygen Programming flow diagram to complete this function. 25.0ºC SN Input filter 25.0ºC Pressure Units mm Hg in Hg atm kPa mbar bar Programming Measurements 1066 Instruction Manual Section 8: programming Measurements LIQ_MAN_1066 8.8 December 2014 ozonE Measurement programming This section describes how to configure the 1066 transmitter for ozone measurement using amperometric ozone sensors. The following programming and configuration functions are covered: 1. Units: ppm Select ppm, mg/L, ppb, μg/L 2. Resolution: 0.001 Select display resolution 0.01 or 0.001 3. Filter: 5sec Override the default input filter, enter 0-999 seconds To configure Ozone: 1. Press MENU 2. Scroll down to Program. Press ENTER. 3. Scroll down to Measurement. Press ENTER. 1.234µS/cm 25.0ºC SN Configure Units: ppm Filter: 5 sec Resolution: 0.001 The adjacent screen format will appear (factory defaults are shown). To program any displayed function, scroll to the desired item and press ENTER. The following sub-sections show the initial display screen that appears for each configuration function. Use the flow diagram for ozone programming at the end of Sec. 6 and the 1066 live screen prompts for each function to complete configuration and programming. Note: Ozone measurement boards are detected automatically by the analyzer. No measurement selection is necessary. 8.8.1 Units 8.8.2 Filter 8.8.3 The display screen for selecting measurement units is shown. The default value is displayed in bold type. Refer to the Ozone Programming flow diagram to complete this function. The display screen for entering the input filter value in seconds is shown. The default value is displayed in bold type. Refer to the Ozone Programming flow diagram to complete this function. Resolution The display screen for selecting display resolution as 0.001 or 0.01 is shown. The default value is displayed in bold type. Refer to the Ozone Programming flow diagram to complete this function. Programming Measurements 1.234µS/cm 25.0ºC SN Units ppm mg/L ppb µg/L 1.234µS/cm 25.0ºC SN Input filter 05 sec 1.234µS/cm 25.0ºC SN Resolution 0.001 0.01 63 Section 8: programming Measurements December 2014 1066 Instruction Manual LIQ_MAN_1066 FIGurE 8-1. Configuring ph/orp Measurements 64 Programming Measurements Programming Measurements M E N U M A I N P r o g r a m 25.0ºC Reset Analyzer Frequency Security Outputs Measurement Temperature Program 1.234µS/cm 25.0ºC Configure? 1.234µS/cm Measurement contacting 25.0ºC 25.0ºC 25.0ºC 25.0ºC 25.0ºC Pt1: Pt1: Pt2: Pt2: Pt3: Pt3: Pt4: Pt4: Pt5: Pt5: 25.0ºC 1.000 ppm 1.000 µS/cm 1.000 ppm 1.000 µS/cm 1.000 ppm 1.000 µS/cm 1.000 ppm 1.000 µS/cm 1.000 ppm 1.000 µS/cm SN Data Points 1.234µS/cm SN Custom Config Units: ppm # of Points: 2 Ref Temp: 25.0 ºC Slope: 2.00 %/°C 25.0ºC 2.00 %/ºC 1.234µS/cm 25.0ºC SN Slope 1.234µS/cm Auto 0-50 µS 50-500 µS 500-2000 µS 2000 µS - 20 mS 20 mS - 200 mS 200 mS - 600 mS SN Range 25.0ºC 25.0ºC 1.234µS/cm SN Type 2-Electrode 4-Electrode 1.234µS/cm 1.234µS/cm 25.0ºC 25.0ºC 25.0ºC 25.0ºC 1.000 ppm SN PointM 1.234µS/cm % ppm mg/L g/L 25.0ºC SN Units 1.234µS/cm (25.0ºC normal) +25.0ºC SN Ref Temp 1.234µS/cm Slope Neutral Salt Cation Raw SN Temp Comp 1.234µS/cm 25.0ºC SN RTD Slope 1.234µS/cm 0.00°C 2.00%/ºC 25.0ºC SN RTD Offset 1.234µS/cm 1.00000 /cm SN Cell Constant LIQ_MAN_1066 SN Calculate Curve Custom curve fit completed. In Process Cal recommended. 1.234µS/cm progress … Curve fit in SN Calculate Curve 1.234µS/cm Configure Enter Data Points Calculate Curve SN Custom Curve 1.234µS/cm Cell K: 1.00000/cm RTD Offset: 0.00ºC RTD Slope: 0 Temp Comp: Slope Slope: 2.00%/°C Ref Temp: 25.0°C Filter: 2 sec Custom Setup Measure: Cond Type: 2-Electrode Range: Auto SN Configure 1.234µS/cm SN Measurement Conductivity Resistivity TDS Salinity 1.234µS/cm 1066 Instruction Manual Section 8: programming Measurements December 2014 Figure 8-2. Configure Contacting Measurements 65 66 M E N U M A I N P r o g r a m 25.0ºC Reset Analyzer Frequency Security Outputs Measurement Measurement Temperature Program 1.234µS/cm 25.0ºC Configure? 1.234µS/cm Measurement Toroidal 25.0ºC 228 Cond Auto 25.0ºC 25.0ºC 25.0ºC 25.0ºC Pt1: Pt1: Pt2: Pt2: Pt3: Pt3: Pt4: Pt4: Pt5: Pt5: 1.000 ppm 1.000 µS/cm 1.000 ppm 1.000 µS/cm 1.000 ppm 1.000 µS/cm 1.000 ppm 1.000 µS/cm 1.000 ppm 1.000 µS/cm SN Data Points 25.0ºC Units: ppm # of Points: 2 Ref Temp: 25.0 ºC slope: 2.00 %/°C SN Custom Config 25.0ºC 2.000 %/ºC 1.234µS/cm 25.0ºC SN Slope 1.234µS/cm 200µS Auto 50-600 µS 0.5-100 mS 90-1500 mS 1.234µS/cm 25.0ºC SN Range 1.234µS/cm Conductivity Resistivity TDS Salinity NaOH (0-12%) HCl (0-15%) Low H2SO4 High H2SO4 NaCl (0-20%) 25.0ºC 25.0ºC 25.0ºC 1.000 ppm SN PointM 1.234µS/cm SN Units 1.234µS/cm 25.0ºC (25.0ºC normal) SN Ref Temp 25.0ºC Slope Neutral Salt Raw SN Temp Comp 1.234µS/cm 2.00%/ºC 1.234µS/cm % ppm mg/L g/L 25.0ºC SN RTD Slope 1.234µS/cm 0.00°C +25.0ºC 25.0ºC SN RTD Offset 1.234µS/cm 3.00000 /cm SN Cell Constant 1.234µS/cm December 2014 Custom curve fit completed. In Process Cal recommended. SN Calculate Curve 1.234µS/cm SN Calculate Curve Curve fit in progress … 1.234µS/cm Configure Enter Data Points Calculate Curve SN Custom Curve 1.234µS/cm Cell K: 3.00000/cm RTD Offset: 0.00ºC RTD Slope: 0 Temp Comp: Slope Slope: 2.00%/°C Ref Temp: 25.0°C Filter: 2 sec Custom Setup Model: Measure: Range: SN Configure 1.234µS/cm 247 228 225 226 25.0ºC SN Model 1.234µS/cm 1.234µS/cm SN Measurement Section 8: programming Measurements 1066 Instruction Manual LIQ_MAN_1066 Figure 8-3. Configure Toroidal Measurements Programming Measurements Programming Measurements M E N U M A I N P r o g r a m 25.0ºC Reset Analyzer Frequency Security Outputs Alarms Measurement Measurement Temperature Program 1.234µS/cm 25.0ºC Configure? 1.234µS/cm Measurement Oxygen 25.0ºC 25.0ºC 25.0ºC At Air Cal mA Input 25.0ºC 25.0ºC 0.001 0.01 SN Resolution 1.234µS/cm mm Hg in Hg atm kPa mbar bar SN Partial Press 1.234µS/cm ppm mg/L ppb µg/L % Saturation Partial Pressure % Oxygen In Gas ppm Oxygen In Gas SN Use Pressure? 1.234µS/cm Salinity: 00.0‰ Filter: 5sec Pressure Units: bar Resolution: 0.001 Use Press: At Air Cal Type: Water/Waste Units: ppm Partial Press: mmHg SN Configure 1.234µS/cm Water/Waste Trace Oxygen BioRx-Rosemount BioRx-Other Brewing Oxygen In Gas SN Type 1.234µS/cm 25.0ºC SN Units 1.234µS/cm 25.0ºC 25.0ºC 25.0ºC Presssure Units 1.234µS/cm 05 sec SN Input filter 1.234µS/cm mm Hg in Hg atm kPa mbar bar 00.0 ‰ SN Salinity 1.234µS/cm 1066 Instruction Manual LIQ_MAN_1066 Section 8: programming Measurements December 2014 Figure 8-4. Configure oxygen Measurements 67 68 25.0ºC Security Diagnostic Setup Reset Analyzer Frequency Outputs Measurement Measurement Temperature Program 1.234µS/cm 25.0ºC Configure? 1.234µS/cm Measurement Chlorine 25.0ºC 25.0ºC Filter: 5sec Dual Cal: Disable Free Cl Correct: Live Manual pH: 7.00 pH Resolution: 0.001 Measure: Free Chlorine Units: ppm SN Configure 1.234µS/cm Free Chlorine Total Chlorine Monochloramine SN Measurement 1.234µS/cm 25.0ºC 25.0ºC SN Resolution 1.234µS/cm 05 sec SN Input filter 1.234µS/cm 0.001 0.01 ppm mg/L 25.0ºC SN Units 1.234µS/cm 25.0ºC 25.0ºC 07.00 pH SN Manual pH 1.234µS/cm Live/Continuous Manual SN Free Cl pH Correction 1.234µS/cm Section 8: programming Measurements December 2014 1066 Instruction Manual LIQ_MAN_1066 FIGurE 8-5. Configuring Chlorine Measurements Programming Measurements Program MAIN MENU Programming Measurements 25.0ºC Reset Analyzer Frequency Security Outputs Measurement Measurement Temperature Program 1.234µS/cm 25.0ºC Configure? 1.234µS/cm Measurement Ozone 25.0ºC ppm 5sec 0.001 Units: Filter: Resolution: SN Configure 1.234µS/cm 0.001 0.01 25.0ºC 25.0ºC 05 sec SN Input filter 1.234µS/cm SN Resolution 1.234µS/cm ppm mg/L ppb µg/L 25.0ºC SN Units 1.234µS/cm 1066 Instruction Manual LIQ_MAN_1066 Section 8: programming Measurements December 2014 FIGurE 8-5. Configuring ozone Measurements 69 Program MAIN MENU Section 8: programming Measurements December 2014 1066 Instruction Manual LIQ_MAN_1066 This page left intentionally blank 70 Programming Measurements 1066 Instruction Manual LIQ_MAN_1066 Section 9: Calibration December 2014 Section 9: Calibration 9.1 Introduction Calibration is the process of adjusting or standardizing the transmitter to a lab test or a calibrated laboratory instrument, or standardizing to some known reference (such as a commercial buffer). The auto-recognition feature of the transmitter will enable the appropriate calibration screens to allow calibration for any configuration of the transmitter. Completion of Quick Start upon first power up enables live measurements but does not ensure accurate readings in the lab or in process. Calibration should be performed with each attached sensor to ensure accurate, repeatable readings. This section covers the following calibration functions: 1. Auto buffer cal for pH (pH Cal - Sec. 9.2) 2. Manual buffer cal for pH (pH Cal - Sec. 9.2) 3. Set calibration stabilization criteria for pH (pH Cal - Sec. 9.2) 4. Standardization calibration (1-point) for pH, ORP and Redox (pH Cal - Sec. 9.2 and 9.3) 5. SMART sensor auto calibration upload 9.2 Calibration New sensors must be calibrated before use. Regular recalibration is also necessary. Use auto calibration instead of manual calibration. Auto calibration avoids common pitfalls and reduces errors. The transmitter recognizes the buffers and uses temperature-corrected pH values in the calibration. Once the 1066 successfully completes the calibration, it calculates and displays the calibration slope and offset. The slope is reported as the slope at 25°C. To calibrate the pH loop with a connected pH sensor, access the Calibration screen by pressing ENTER from the main screen and press ENTER. The following calibration routines are covered: 1. Auto Calibration - pH 2 point buffer calibration with auto buffer recognition 2. Manual Calibration - pH 2 point buffer calibration with manual buffer value entry 3. Standardization - pH 1 point buffer calibration with manual buffer value entry 4. Entering A Known Slope Value - pH Slope calibration with manual entry of known slope value 5. SMART sensor auto calibration – auto detection and upload of cal data To calibrate pH: 1. Press the MEnu button 2. Select Calibrate. Press EnTEr. 3. Select ph. Press ENTER. The following sub-sections show the initial display screen that appears for each calibration routine. Use the flow diagram for ph calibration at the end of Sec. 7 and the live screen prompts to complete calibration. Calibration 1.234µS/cm 25.0ºC SN Calibrate? pH Temperature 71 Section 9: Calibration December 2014 9.2.1 1066 Instruction Manual LIQ_MAN_1066 Auto Calibration This screen appears after selecting ph calibration. 1.234µS/cm 25.0ºC SN pH Cal Buffer Cal Standardize Slope: 59.16mV/pH 600 mV Offset: Note that pH auto calibration criteria can be changed. The following criteria can be adjusted: • • • Stabilization time (default 10 sec.) Stabilization pH value (default 0.02 pH) Type of Buffer used for AUTO CALIBRATION (default is Standard, non-commercial buffers). The following commercial buffer tables are recognized by the analyzer: • • • • Standard (NIST plus pH7) DIN 19267 Ingold Merck This screen will appear if the auto cal is successful. The screen will return to the pH Buffer Cal Menu. 1.234µS/cm 25.0ºC SN Setup Stable Time: 10 sec Stable Delta: 0.02 pH Buffer: Standard 1.234µS/cm 25.0ºC SN pH Auto Cal Slope: 59.16 mV/pH Offset: 60 mV The following screens may appear if the auto cal is unsuccessful. 1. A High Slope Error will generate this screen display: 2. A Low Slope Error will generate this screen display: 1.234µS/cm 25.0ºC SN pH Auto Cal High Slope Error Calculated: 62.11 mV/pH Max: 62.00 mV/pH Press EXIT 1.234µS/cm 25.0ºC SN pH Auto Cal Low Slope Error Calculated: 39.11mV/pH Min: 40.00 mV/pH Press EXIT 3. An Offset Error will generate this screen display: 1.234µS/cm 25.0ºC SN pH Auto Cal Offset Error Calculated: 61.22mV Max: 60.00mV Press EXIT 72 Calibration 1066 Instruction Manual LIQ_MAN_1066 9.2.2 December 2014 Manual Calibration – pH New sensors must be calibrated before use. Regular recalibration is also necessary. Use manual calibration if non-standard buffers are being used; otherwise, use auto calibration. Auto calibration avoids common pitfalls and reduces errors. The adjacent appears after selecting Manual pH calibration. 9.2.3 Section 9: Calibration 1.234µS/cm Entering a Known Slope Value – pH 1.234µS/cm If the electrode slope is known from other measurements, it can be entered directly in the 1066 transmitter. The slope must be entered as the slope at 25°C. 9.2.4 25.0ºC SN pH Manual Cal Buffer 1 Buffer 2 25.0ºC SN pH Slope@25ºC 59.16 mV/pH Standardization – pH The pH measured by the 1066 transmitter can be hanged to match 1.234µS/cm 25.0ºC the reading from a second or referee instrument. The process of makSN Enter Value 07.00pH ing the two readings agree is called standardization. During standardization, the difference between the two pH values is converted to the equivalent voltage. The voltage, called the reference offset, is added to all subsequent measured cell voltages before they are converted to pH. If a standardized sensor is placed in a buffer solution, the measured pH will differ from the buffer pH by an amount equivalent to the standardization offset. This screen may appear if pH Cal is unsuccessful. An Offset Error will generate this screen display: If the pH Cal is successful, the screen will return to the Cal sub-menu. 9.2.5 1.234µS/cm 25.0ºC SN Standardize Offset Error Calculated: 96mV Max: 60mV Press EXIT SMART sensor auto calibration upload – pH All calibration data including slope (mV/pH unit), offset (mV), glass impedance (MegOhms), and reference impedance (kOhms) is automatically downloaded to the SMART sensor upon successful calibration. This data transfer to the sensor is transparent and does not require any user action. Calibrated SMART sensors will be loop-calibrated when wired or attached (via VP8 cable connection) to any SMART-enabled Rosemount Analytical instrument. To calibrate any SMART sensor, choose any available calibration method. Note that new SMART sensors upon first shipment from Emerson are pre-calibrated and do not require buffer calibration or standardization to be used in process immediately. Calibration 73 Section 9: Calibration 1066 Instruction Manual December 2014 9.3 LIQ_MAN_1066 orp and redox Calibration For process control, it is often important to make the measured ORP or Redox agree with the ORP or Redox of a standard solution. During calibration, the measured ORP or Redox is made equal to the ORP or Redox of a standard solution at a single point. To calibrate the ORP loop with a connected ORP sensor, access the Calibration screen by pressing ENTER from the main screen and press ENTER. The following calibration routine is covered: 1. Standardization ORP 1 point buffer calibration with manual buffer value entry. To calibrate ORP: 1. Press the MENU button. 2. Select Calibrate. Press ENTER. 3. Select ORP and Redox. Press ENTER. 1.234µS/cm 25.0ºC SN Calibrate? ORP Temperature The following sub-sections show the initial display screen that appears for each calibration routine. Use the flow diagram for orp calibration at the end of Sec. 8 and the live screen prompts to complete calibration. 9.3.1 Standardization – ORP and Redox For process control, it is often important to make the measured ORP and Redox agree with the ORP and Redox of a standard solution. During calibration, the measured ORP and Redox is made equal to the ORP and Redox of a standard solution at a single point. This screen appears after selecting ORP and Redox calibration: 1.234µS/cm 25.0ºC SN Enter Value +0600 mV If the ORP and Redox Cal is successful, the screen will return to the Cal sub-menu. The following screen may appear if ORP and Redox Cal is unsuccessful. 74 1.234µS/cm 25.0ºC SN Standardize Offset Error Calculated: 61.22mV Max: 60.00mV Press EXIT Calibration 1066 Instruction Manual LIQ_MAN_1066 9.4 Section 9: Calibration December 2014 Contacting Conductivity Calibration New conductivity sensors rarely need calibration. The cell constant printed on the label is sufficiently accurate for most applications. CALIBRATING AN IN-SERVICE CONDUCTIVITY SENSOR After a conductivity sensor has been in service for a period of time, recalibration may be necessary. There are three ways to calibrate a sensor. a. Use a standard instrument and sensor to measure the conductivity of the process stream. It is not necessary to remove the sensor from the process piping. The temperature correction used by the standard instrument may not exactly match the temperature correction used by the 1066. To avoid errors, turn off temperature correction in both the transmitter and the standard instrument. b. Place the sensor in a solution of known conductivity and make the transmitter reading match the conductivity of the standard solution. Use this method if the sensor can be easily removed from the process piping and a standard is available. Be careful using standard solutions having conductivity less than 100 μS/cm. Low conductivity standards are highly susceptible to atmospheric contamination. Avoid calibrating sensors with 0.01/cm cell constants against conductivity standards having conductivity greater than 100 μS/cm. The resistance of these solutions may be too low for an accurate measurement. Calibrate sensors with 0.01/cm cell constant using method c. c. To calibrate a 0.01/cm sensor, check it against a standard instrument and 0.01/cm sensor while both sensors are measuring water having a conductivity between 5 and 10 μS/cm. To avoid drift caused by absorption of atmospheric carbon dioxide, saturate the sample with air before making the measurements. To ensure adequate flow past the sensor during calibration, take the sample downstream from the sensor. For best results, use a flow-through standard cell. If the process temperature is much different from ambient, keep connecting lines short and insulate the flow cell. To calibrate the conductivity loop with a connected contacting conductivity sensor, access the Calibration screen by pressing ENTER from the main screen and press ENTER. The following calibration routines are covered: 1. Zero Cal Zero the transmitter with the sensor attached 2. In Process Cal Standardize the sensor to a known conductivity 3. Cell K: 1.00000/cm Enter the cell Constant for the sensor 4. Meter Cal Calibrate the transmitter to a lab conductivity instrument 5. Cal Factor: 0.95000/cm Enter the Cal Factor for 4-Electrode sensors from the sensor tag To calibrate contacting conductivity: 1. Press the MENU button 2. Select Calibrate. Press ENTER. 1.234µS/cm 25.0ºC SN Calibrate? Conductivity Temperature 3. Select Conductivity. Press ENTER. The adjacent screen will appear. To calibrate Conductivity or Temperature, scroll to the desired item and press ENTER. Calibration 75 Section 9: Calibration 1066 Instruction Manual December 2014 LIQ_MAN_1066 The following sub-sections show the initial display screen that appears for each calibration routine. Use the flow diagram for Conductivity calibration at the end of Sec. 7 and the live screen prompts for each routine to complete calibration. The adjacent screen appears after selecting Conductivity calibration: 9.4.1 1.234µS/cm 25.0ºC SN Calibration Zero Cal In Process Cal Meter Cal Cell K: 1.00000/cm Entering the Cell Constant New conductivity sensors rarely need calibration. The cell constant printed on the label is sufficiently accurate for most applications. The cell constant should be entered: 1.234µS/cm 25.0ºC SN Cell Constant 1.00000 /cm • When the unit is installed for the first time • When the probe is replaced The display screen for entering a cell Constant for the sensor is shown. The default value is displayed in bold type. 9.4.2 Zeroing the Instrument This procedure is used to compensate for small offsets to the conductivity signal that are present even when there is no conductivity to be measured. This procedure is affected by the length of extension cable and should always be repeated if any changes in extension cable or sensor have been made. Electrically connect the conductivity probe as it will actually be used and place the measuring portion of the probe in air. Be sure the probe is dry. The adjacent screen will appear after selecting Zero Cal from the Conductivity Calibration screen: The adjacent screen will appear if zero Cal is successful. The screen will return to the conductivity Cal Menu. The adjacent screen may appear if zero Cal is unsuccessful. 9.4.3 1.234µS/cm 25.0ºC SN Zero Cal In Air In Water 1.234µS/cm 25.0ºC SN Zero Cal Sensor Zero Done 1.234µS/cm 25.0ºC SN Zero Cal Sensor Zero Fail Offset too high Press EXIT Calibrating the Sensor in a Conductivity Standard (in process cal) This procedure is used to calibrate the sensor and transmitter against a solution of known conductivity. This is done by submerging the probe in the sample of known conductivity, then adjusting the displayed value, if necessary, to correspond to the conductivity value of the sample. Turn temperature correction off and use the conductivity of the standard. Use a calibrated thermometer to measure temperature. The probe must be cleaned before performing this procedure. The adjacent screen will appear after selecting In Process Cal from the Conductivity Calibration screen: The adjacent screen will appear if In Process Cal is successful. The screen will return to the conductivity Cal Menu. 1.234µS/cm 25.0ºC SN InProcess Cal Wait for stable reading. The adjacent screen may appear if In Process Cal is unsuccessful. The screen will return to the conductivity Cal Menu. 76 Calibration 1066 Instruction Manual Section 9: Calibration LIQ_MAN_1066 December 2014 The adjacent screen will appear if In Process Cal is successful. The screen will return to the conductivity Cal Menu. 1.234µS/cm 1.234µS/cm The adjacent screen may appear if In Process Cal is unsuccessful. The screen will return to the conductivity Cal Menu. 25.0ºC SN InProcess Cal Updated cell constant: 1.00135/cm 25.0ºC SN InProcess Cal Calibration Error Press EXIT 9.4.4 Calibrating the Sensor To A Laboratory Instrument (meter cal) This procedure is used to check and correct the conductivity reading of the 1066 using a laboratory conductivity instrument. This is done by submerging the conductivity probe in a bath and measuring the conductivity of a grab sample of the same bath water with a separate laboratory instrument. The 1066 reading is then adjusted to match the conductivity reading of the lab instrument. 1.234µS/cm The adjacent screen will appear after selecting Meter Cal from the Conductivity Calibration screen: After pressing ENTER, the display shows the live value measured by the sensor If the meter cal is successful the screen will return to the conductivity Cal Menu. The adjacent screen will appear if Meter Cal is unsuccessful. The screen will return to the conductivity Cal Menu. 9.4.5 Calibration 25.0ºC SN Meter Cal Use precision resistors only 1.234µS/cm 25.0ºC SN Enter Value xx.xx kΩ 1.234µS/cm 25.0ºC SN Meter Cal Calibration Error Press EXIT Cal Factor 1.234µS/cm 25.0ºC Upon initial installation and power up, if 4-electrode was selected for the SN Cal Factor sensor type in the Quick Start menus, the user enters a Cell Constant and 0.95000 /cm a “Cal Factor” using the instrument keypad. The cell constant is needed to convert measured conductance to conductivity as displayed on the transmitter screen. The “Cal Factor” entry is needed increase the accuracy of the live conductivity readings, especially at low conductivity readings below 20uS/cm. Both the Cell Constant and the “Cal Factor” are printed on the tag attached to the 4-electrode sensor/cable. 77 Section 9: Calibration 1066 Instruction Manual December 2014 9.5 LIQ_MAN_1066 Toroidal Conductivity Calibration Calibration is the process of adjusting or standardizing the transmitter to a lab test or a calibrated laboratory instrument, or standardizing to some known reference (such as a conductivity standard). This section contains procedures for the first time use and for routine calibration of the 1066 transmitter. To calibrate the conductivity loop with a connected contacting conductivity sensor, access the Calibration screen by pressing ENTER from the main screen and press ENTER. The following calibration routines are covered: 1. Zero Cal Zero the transmitter with the sensor attached 2. In Process Cal Standardize the sensor to a known conductivity 3. Cell K: 1.00000/cm Enter the cell Constant for the sensor 4. Meter Cal Calibrate the transmitter to a lab conductivity instrument To calibrate toroidal conductivity: 1. Press the MENU button 2. Select Calibrate. Press ENTER. 3. Select Conductivity. Press ENTER. The adjacent screen will appear. To calibrate Toroidal Conductivity or Temperature, scroll to the desired item and press ENTER The following sub-sections show the initial display screen that appears for each calibration routine. Use the flow diagram for Conductivity calibration at the end of Sec. 7 and the live screen prompts to complete calibration. 1.234µS/cm The adjacent screen appears after selecting Conductivity calibration: 9.5.1 25.0ºC Calibration Zero Cal In Process Cal Cell K: 2.7000/cm Entering the Cell Constant New toroidal sensors always need to be calibrated. The cell constant provided on the sensor label is a nominal value and does not need to be entered. This procedure sets up the transmitter for the probe type connected to the transmitter. Each type of probe has a specific cell constant The display screen for entering a cell constant for the sensor is shown. The default value is displayed in bold type. 78 1.234µS/cm 25.0ºC Cell Constant 2.7000/cm Calibration 1066 Instruction Manual Section 9: Calibration LIQ_MAN_1066 9.5.2 December 2014 Zeroing the Instrument This procedure is used to compensate for small offsets to the conductivity signal that are present even when there is no conductivity to be measured. This procedure is affected by the length of extension cable and should always be repeated if any changes in extension cable or sensor have been made. Electrically connect the conductivity probe as it will actually be used and place the measuring portion of the probe in air. 1.234µS/cm The adjacent screen will appear after selecting Zero Cal from the Conductivity Calibration screen: 25.0ºC SN Zero Cal In Air In Water 1.234µS/cm The adjacent screen will appear if zero Cal is successful. The screen will return to the conductivity Cal Menu. The adjacent screen may appear if zero Cal is unsuccessful. 25.0ºC SN Zero Cal Sensor Zero Done 1.234µS/cm 25.0ºC SN Zero Cal Sensor Zero Fail Offset too high Press EXIT 9.5.3 Calibrating the Sensor in a Conductivity Standard (in process cal) This procedure is used to check and correct the conductivity reading of the 1066 to ensure that the reading is accurate. This is done by submerging the probe in the sample of known conductivity, then adjusting the displayed value, if necessary, to correspond to the conductivity value of the sample. The probe must be cleaned before performing this procedure. The temperature reading must also be checked and standardized if necessary, prior to performing this procedure. 1.234µS/cm The adjacent screen will appear after selecting In Process Cal from the Conductivity Calibration screen: 25.0ºC SN InProcess Cal Wait for stable reading. 1.234µS/cm 25.0ºC The following screen will appear if In Process Cal is successful. The screen will return to the conductivity Cal Menu. SN InProcess Cal Updated cell constant: 3.01350/cm This screen may appear if In Process Cal is unsuccessful. The screen will return to the conductivity Cal Menu. SN InProcess Cal Calibration Error 1.234µS/cm 25.0ºC Press EXIT Calibration 79 Section 9: Calibration 1066 Instruction Manual December 2014 9.6 LIQ_MAN_1066 Calibration – Chlorine The 1066 can measure three variants of Chlorine: • Free Chlorine • Total Chlorine • Monochloramine The section describes how to calibrate any compatible amperometric chlorine sensor. The following calibration routines are covered in the family of supported Chlorine sensors: • Air Cal • Zero Cal • In Process Cal 9.6.1 Calibration – Free Chlorine A free chlorine sensor generates a current directly proportional to the concentration of free chlorine in the sample. Calibrating the sensor requires exposing it to a solution containing no chlorine (zero standard) and to a solution containing a known amount of chlorine (full-scale standard). The zero calibration is necessary because chlorine sensors, even when no chlorine is in the sample, generate a small current called the residual current. The transmitter compensates for the residual current by subtracting it from the measured current before converting the result to a chlorine value. New sensors require zeroing before being placed in service, and sensors should be zeroed whenever the electrolyte solution is replaced. To calibrate the chlorine sensor, access the Calibration screen by pressing ENTER from the main screen and press ENTER. The following calibration routines are covered: 1. Zero Cal Zeroing the sensor in solution with zero free chlorine 2. Grab Cal Standardizing to a sample of known free chlorine concentration To calibrate free chlorine: 1. Press the MENU button 2. Select Calibrate. Press ENTER. 3. Select Free Chlorine. Press ENTER. The adjacent screen will appear. To calibrate Free Chlorine or Temperature, scroll to the desired item and press ENTER. 1.234µS/cm 25.0ºC SN Calibrate? Free Chlorine Temperature The following sub-sections show the initial display screen that appears for each calibration routine. Use the flow diagram for Chlorine calibration at the end of Sec. 7 and the live screen prompts to complete calibration. The adjacent screen appears after selecting Free Chlorine calibration: 80 1.234µS/cm 25.0ºC SN Calibration Zero Cal In Process Cal Calibration 1066 Instruction Manual Section 9: Calibration LIQ_MAN_1066 9.6.1.1 December 2014 Zeroing the Sensor 1.234µS/cm 25.0ºC SN Zero Cal Zeroing Wait The adjacent screen will appear during Zero Cal. Be sure sensor has been running in zero solution for at least two hours before starting zero step. 1.234µS/cm The adjacent screen will appear if In Zero Cal is successful. The screen will return to the Amperometric Cal Menu. 25.0ºC SN Zero Cal Sensor zero done 1.234µS/cm The adjacent screen may appear if In Zero Cal is unsuccessful. The screen will return to the Amperometric Cal Menu. 25.0ºC SN Zero Cal Sensor zero failed Press EXIT 9.6.1.2 In Process Calibration The adjacent screen will appear prior to In Process Cal 1.234µS/cm 25.0ºC SN InProcess Cal Wait for stable reading. If the In Process Cal is successful, the screen will return to the Cal sub-menu. The adjacent screen may appear if In Zero Cal is unsuccessful. The screen will return to the Amperometric Cal Menu. 1.234µS/cm 25.0ºC SN InProcess Cal Calibration Error Press EXIT 9.6.2 Calibration Calibration – Total Chlorine Total chlorine is the sum of free and combined chlorine. The continuous determination of total chlorine requires two steps. First, the sample flows into a conditioning system (TCL) where a pump continuously adds acetic acid and potassium iodide to the sample. The acid lowers the pH, which allows total chlorine in the sample to quantitatively oxidize the iodide in the reagent to iodine. In the second step, the treated sample flows to the sensor. The sensor is a membrane-covered amperometric sensor, whose output is proportional to the concentration of iodine. Because the concentration of iodine is proportional to the concentration of total chlorine, the transmitter can be calibrated to read total chlorine. Because the sensor really measures iodine, calibrating the sensor requires exposing it to a solution containing no iodine (zero standard) and to a solution containing a known amount of iodine (full-scale standard). The Zero calibration is necessary because the sensor, even when no iodine is present, generates a small current called the residual current. The transmitter compensates for the residual current by subtracting it from the measured current before converting the result to a total chlorine value. New sensors require zeroing before being placed in service, and sensors should be zeroed whenever the electrolyte solution is replaced. The best zero standard is deionized water. The purpose of the In Process Calibration is to establish the 81 Section 9: Calibration 1066 Instruction Manual December 2014 LIQ_MAN_1066 slope of the calibration curve. Because stable total chlorine standards do not exist, the sensor must be calibrated against a test run on a grab sample of the process liquid. Several manufacturers offer portable test kits for this purpose. To calibrate the chlorine sensor, access the Calibration screen by pressing ENTER from the main screen, and press ENTER. The following calibration routines are covered: 1. Zero Cal Zeroing the sensor in solution with zero total chlorine 2. Grab Cal Standardizing to a sample of known total chlorine concentration To calibrate total chlorine: 1. Press the MENU button 2. Select Calibrate. Press ENTER. 3. Select Total Chlorine. Press ENTER. The adjacent screen will appear. To calibrate Total Chlorine or Temperature, scroll to the desired item and press ENTER 1.234µS/cm 25.0ºC SN Calibrate? Total Chlorine Temperature The following sub-sections provide you with the initial display screen that appears for each calibration routine. Use the flow diagram for Chlorine calibration at the end 1.234µS/cm 25.0ºC of Sec. 9 and the live screen prompts to complete calibration. SN Calibration This adjacent screen appears after selecting Total Chlorine calibration: 9.6.2.1 Zeroing the Sensor The adjacent screen will appear during Zero Cal. Be sure sensor has been running in zero solution for at least two hours before starting zero step. Zero Cal In Process Cal 1.234µS/cm 25.0ºC SN Zero Cal Zeroing Wait 1.234µS/cm The adjacent screen will appear if In Zero Cal is successful. The screen will return to the Amperometric Cal Menu. The adjacent screen may appear if In Zero Cal is unsuccessful. The screen will return to the Amperometric Cal Menu. 25.0ºC SN Zero Cal Sensor zero done 1.234µS/cm 25.0ºC SN Zero Cal Sensor zero failed Press EXIT 9.6.2.2 In Process Calibration The adjacent screen will appear prior to In Process Cal If the In Process Cal is successful, the screen will return to the Cal submenu. The adjacent screen may appear if In Process Cal is unsuccessful. The screen will return to the Amperometric Cal Menu. 1.234µS/cm 25.0ºC SN InProcess Cal Wait for stable reading. 1.234µS/cm 25.0ºC SN InProcess Cal Calibration error Press EXIT 82 Calibration 1066 Instruction Manual Section 9: Calibration LIQ_MAN_1066 9.6.3 December 2014 Calibration – Monochloromine A monochloramine sensor generates a current directly proportional to the concentration of monochloramine in the sample. Calibrating the sensor requires exposing it to a solution containing no monochloramine (zero standard) and to a solution containing a known amount of monochloramine (full-scale standard). The Zero calibration is necessary because monochloramine sensors, even when no monochloramine is in the sample, generate a small current called the residual or zero current. The transmitter compensates for the residual current by subtracting it from the measured current before converting the result to a monochloramine value. New sensors require zeroing before being placed in service, and sensors should be zeroed whenever the electrolyte solution is replaced. The best zero standard is deionized water. The purpose of the In Process calibration is to establish the slope of the calibration curve. Because stable monochloramine standards do not exist, the sensor must be calibrated against a test run on a grab sample of the process liquid. Several manufacturers offer portable test kits for this purpose. To calibrate the chlorine sensor, access the Calibration screen by pressing ENTER from the main screen, and press ENTER. The following calibration routines are covered: 1. Zero Cal Zeroing the sensor in solution with zero total chlorine 2. Grab Cal Standardizing to a sample of known monochloramine concentration To calibrate monochloramine: 1. Press the MENU button 2. Select Calibrate. Press ENTER. 3. Select Monochloramine. Press ENTER. The adjacent screen will appear. To calibrate Monochloramine or Temperature, scroll to the desired item and press ENTER. 1.234µS/cm 25.0ºC SN Calibrate? Monochloramine Temperature The following sub-sections provide you with the initial display screen that appears for each calibration routine. Use the flow diagram for Chlorine calibration at the end of Sec. 9 and the live screen prompts to complete calibration. 1.234µS/cm The adjacent screen appears after selecting Monochloramine calibration: Calibration 25.0ºC SN Calibration Zero Cal In Process Cal 83 Section 9: Calibration 1066 Instruction Manual December 2014 9.6.4 LIQ_MAN_1066 Zeroing the Sensor The adjacent screen will appear during Zero Cal. Be sure sensor has been running in zero solution for at least two hours before starting zero step. 1.234µS/cm 1.234µS/cm The adjacent screen will appear if In Zero Cal is successful. The screen will return to the Amperometric Cal Menu. The adjacent screen may appear if In Zero Cal is unsuccessful. The screen will return to the Amperometric Cal Menu. 25.0ºC SN Zero Cal Zeroing Wait 25.0ºC SN Zero Cal Sensor zero done 1.234µS/cm 25.0ºC SN Zero Cal Sensor zero failed Press EXIT 9.6.5 In Process Calibration The adjacent screen will appear prior to In Process Cal 1.234µS/cm 25.0ºC If the In Process Cal is successful, the screen will return to the Cal submenu. SN InProcess Cal Wait for stable reading. The adjacent screen may appear if In Process Cal is unsuccessful. The screen will return to the Amperometric Cal Menu. SN InProcess Cal Calibration Error 1.234µS/cm 25.0ºC Press EXIT 9.7 84 Calibration – oxygen Oxygen sensors generate a current directly proportional to the concentration of dissolved oxygen in the sample. Calibrating the sensor requires exposing it to a solution containing no oxygen (zero standard) and to a solution containing a known amount of oxygen (full-scale standard). The Zero Calibration is necessary because oxygen sensors, even when no oxygen is present in the sample, generate a small current called the residual current. The transmitter compensates for the residual current by subtracting it from the measured current before converting the result to a dissolved oxygen value. New sensors require zeroing before being placed in service, and sensors should be zeroed whenever the electrolyte solution is replaced. The recommended zero standard is 5% sodium sulfite in water, although oxygen-free nitrogen can also be used. The 499A TrDO sensor, used for the determination of trace (ppb) oxygen levels, has very low residual current and does not normally require zeroing. The residual current in the 499A TrDO sensor is equivalent to less than 0.5 ppb oxygen. The purpose of the In Process Calibration is to establish the slope of the calibration curve. Because the solubility of atmospheric oxygen in water as a function of temperature and barometric pressure is well known, the natural choice for a full-scale standard is air-saturated water. However, air-saturated water is difficult to prepare and use, so the universal practice is to use air for calibration. From the point of view of the oxygen sensor, air and air-saturated water are Calibration 1066 Instruction Manual Section 9: Calibration LIQ_MAN_1066 December 2014 identical. The equivalence comes about because the sensor really measures the chemical potential of oxygen. Chemical potential is the force that causes oxygen molecules to diffuse from the sample into the sensor where they can be measured. It is also the force that causes oxygen molecules in air to dissolve in water and to continue to dissolve until the water is saturated with oxygen. Once the water is saturated, the chemical potential of oxygen in the two phases (air and water) is the same. Oxygen sensors generate a current directly proportional to the rate at which oxygen molecules diffuse through a membrane stretched over the end of the sensor. The diffusion rate depends on the difference in chemical potential between oxygen in the sensor and oxygen in the sample. An electrochemical reaction, which destroys any oxygen molecules entering the sensor, keeps the concentration (and the chemical potential) of oxygen inside the sensor equal to zero. Therefore, the chemical potential of oxygen in the sample alone determines the diffusion rate and the sensor current. When the sensor is calibrated, the chemical potential of oxygen in the standard determines the sensor current. Whether the sensor is calibrated in air or air-saturated water is immaterial. The chemical potential of oxygen is the same in either phase. Normally, to make the calculation of solubility in common units (like ppm DO) simpler, it is convenient to use water-saturated air for calibration. Automatic air calibration is standard. The user simply exposes the sensor to water-saturated air. The transmitter monitors the sensor current. When the current is stable, the transmitter stores the current and measures the temperature using a temperature element inside the oxygen sensor. The user must enter the barometric pressure. From the temperature the transmitter calculates the saturation vapor pressure of water. Next, it calculates the pressure of dry air by subtracting the vapor pressure from the barometric pressure. Using the fact that dry air always contains 20.95% oxygen, the transmitter calculates the partial pressure of oxygen. Once the transmitter knows the partial pressure of oxygen, it uses the Bunsen coefficient to calculate the equilibrium solubility of atmospheric oxygen in water at the prevailing temperature. At 25°C and 760 mm Hg, the equilibrium solubility is 8.24 ppm. Often it is too difficult or messy to remove the sensor from the process liquid for calibration. In this case, the sensor can be calibrated against a measurement made with a portable laboratory instrument. The laboratory instrument typically uses a membrane-covered amperometric sensor that has been calibrated against water-saturated air. To calibrate the oxygen sensor, access the Calibration screen by pressing ENTER from the main screen, select and press ENTER. The following calibration routines are covered: 1. Zero Cal Zeroing the sensor in a medium with zero oxygen 2. Air Cal Calibrating the sensor in a water-saturated air sample 3. In Process Cal Standardizing to a sample of known oxygen concentration 4. Sen@ 25°C:2500nA/ppm Entering a known slope value for sensor response To calibrate oxygen: 1. Press the MENU button 2. Select Calibrate. Press ENTER. 3. Select Oxygen. Press ENTER. The adjacent screen will appear. To calibrate Oxygen or Temperature, scroll to the desired item and press ENTER Calibration 1.234µS/cm 25.0ºC SN Calibrate? Oxygen Temperature 85 Section 9: Calibration 1066 Instruction Manual December 2014 LIQ_MAN_1066 The following sub-sections provide you with the initial display screen that appears for each calibration routine. Use the flow diagram for Oxygen calibration at the end of Sec. 9 and the live screen prompts for each routine to complete calibration. 1.234µS/cm 25.0ºC The adjacent screen appears after selecting Oxygen calibration: SN Calibration Air Cal Zero Cal In Process Cal Sen@ 25°C:2500nA/ppm Air calibration criteria can be changed. Zero Current: 1234nA The following criteria can be adjusted: • Stabilization time (default 10 sec.) • Stabilization pH value (default 0.05 ppm) • Salinity of the solution to be measured (default 00.0 parts per thousand) 1.234µS/cm The adjacent screen will appear to allow adjustment of these criteria: 25.0ºC SN Setup Stable Time: 10 sec Stable Delta: 0.05 ppm Salinity: 00.0 ‰ 1.234 nA 9.7.1 Zeroing the Sensor SN Zero Cal Zeroing Wait The adjacent screen will appear if In Zero Cal is successful. The screen will return to the Amperometric Cal Menu. SN Zero Cal Sensor zero done The adjacent screen may appear if In Zero Cal is unsuccessful. The screen will return to the Amperometric Cal Menu. SN Zero Cal Sensor zero failed The adjacent screen will appear during Zero Cal 1.234 nA 1.234 nA Press EXIT 9.7.2 Calibrating the Sensor in Air The adjacent screen will appear prior to Air Cal The adjacent screen will appear if In Air Cal is successful. The screen will return to the Amperometric Cal Menu. The adjacent screen may appear if In Air Cal is unsuccessful. The screen will return to the Amperometric Cal Menu. 1.234µS/cm 25.0ºC SN Air Cal Start Calibration Setup 1.234µS/cm 25.0ºC SN Air Cal Done 1.234µS/cm 25.0ºC SN Air Cal Failure Check Sensor Press EXIT 86 Calibration 1066 Instruction Manual Section 9: Calibration LIQ_MAN_1066 9.7.3 December 2014 Calibrating the Sensor Against A Standard Instrument (in process cal) The adjacent screen will appear prior to In Process Cal If the In Process Cal is successful, the screen will return to the Cal sub-menu. The adjacent screen may appear if In Zero Cal is unsuccessful. The screen will return to the Amperometric Cal Menu. 9.8 Calibration – ozone An ozone sensor generates a current directly proportional to the concentration of ozone in the sample. Calibrating the sensor requires exposing it to a solution containing no ozone (zero standard) and to a solution containing a known amount of ozone (full-scale standard). The Zero Calibration is necessary because ozone sensors, even when no ozone is in the sample, generate a small current called the residual or zero current. The transmitter compensates for the residual current by subtracting it from the measured current before converting the result to an ozone value. New sensors require zeroing before being placed in service, and sensors should be zeroed whenever the electrolyte solution is replaced. The best zero standard is deionized water. The purpose of the In Process Calibration is to establish the slope of the calibration curve. Because stable ozone standards do not exist, the sensor must be calibrated against a test run on a grab sample of the process liquid. Several manufacturers offer portable test kits for this purpose. To calibrate the ozone sensor, access the Calibration screen by pressing ENTER from the main screen, select and press ENTER. The following calibration routines are covered: 1. Zero Cal Zeroing the sensor in solution with zero total chlorine 2. Grab Cal Standardizing to a sample of known ozone concentration To calibrate ozone: 1. Press the MENU button 2. Select Calibrate. Press ENTER. 3. Select Ozone. Press ENTER. The adjacent screen will appear. To calibrate Ozone or Temperature, scroll to the desired item and press ENTER. Calibration 1.234µS/cm 25.0ºC SN Calibrate? Ozone Temperature 87 Section 9: Calibration 1066 Instruction Manual December 2014 LIQ_MAN_1066 The following sub-sections provide you with the initial display screen that appears for each calibration routine. Use the flow diagram for ozone calibration at the end of Sec. 9 and the live screen prompts to complete calibration. 1.234µS/cm The adjacent screen appears after selecting Ozone calibration: 9.8.1 Zeroing the Sensor The following screen will appear during Zero Cal The following screen will appear if In Zero Cal is successful. The screen will return to the Amperometric Cal Menu. The following screen may appear if In Zero Cal is unsuccessful. The screen will return to the Amperometric Cal Menu. 25.0ºC SN Calibration Zero Cal In Process Cal 1.234 nA SN Zero Cal Zeroing Wait 1.234 nA SN Zero Cal Sensor zero done 1.234 nA SN Zero Cal Sensor zero failed Press EXIT 1.234µS/cm 9.8.2 25.0ºC In Process Calibration SN InProcess Cal Wait for stable reading. If the In Process Cal is successful, the screen will return to the Cal submenu. The following screen may appear if In Zero Cal is unsuccessful. The screen will return to the Amperometric Cal Menu. SN InProcess Cal Calibration Error The following screen will appear after selecting In Process Cal 1.234µS/cm 25.0ºC Press EXIT 88 Calibration 1066 Instruction Manual Section 9: Calibration LIQ_MAN_1066 9.9 December 2014 Calibrating Temperature Most liquid analytical measurements require temperature compensation (except ORP and Redox). The 1066 performs temperature compensation automatically by applying internal temperature correction algorithms. Temperature correction can also be turned off. If temperature correction is off, the 1066 uses the manual temperature entered by the user in all temperature correction calculations. To calibrate temperature, access the Calibration screen by pressing ENTER from the main screen, select Temperature and press ENTER. The following calibration routine is covered: 1. Temperature with manual temperature entry To calibrate temperature: 1. Press the MENU button 2. Select Calibrate. Press ENTER. 3. Select Temperature. Press ENTER. The adjacent screen will appear. 1.234µS/cm 25.0ºC SN Calibrate +025.0°C The following sub-section provides you with the initial display screen that appears for temperature calibration. Use the flow diagram for Temp calibration at the end of Sec. 7 to complete calibration. 9.9.1 Calibration The adjacent screen will appear during Temperature Cal. If the sensor Temperature offset is greater than 5 ºC from the default value, the following screen will appear: You may continue by selecting Yes or suspend this operation by selecting No. If the Temp Cal is successful, the screen will return to the Cal Menu. 1.234µS/cm 25.0ºC SN Calibrate Cal in progress. Please wait. 1.234µS/cm 25.0ºC SN Temp Offset > 5°C Continue? No Yes note: To select automatic or manual temp compensation or to program temperature units as °C or °F, refer to Sec. 7.3 – Programming Temperature in this manual. Calibration 89 90 1.234µS/cm 25.0ºC 25.0ºC 25.0ºC 25.0ºC 060 mV SN pH Offset 25.0ºC 59.16 mV/pH SN pH Slope@25ºC 25.0ºC Cal in progress. Please wait. SN Standardize 1.234µS/cm 07.00pH 1.234µS/cm 25.0ºC 1.234µS/cm 25.0ºC 1.234µS/cm 25.0ºC Cal in progress. Please wait. SN Manual Cal Offset Error Calculated: Max: Press EXIT 96mV 60mV SN Standardize Manual BufferM 1.234µS/cm Stable Time: 10 sec Stable Delta: 0.02 pH Buffer: Standard SN Setup 25.0ºC Standard DIN 19267 Ingold Merck 1.234µS/cm 1.234µS/cm 1.234µS/cm 25.0ºC 25.0ºC Place Sensor in Buffer 1 Press ENTER SN pH Auto Cal Slope: 59.16mV/pH Offset: 60 mV SN pH Manual Cal 25.0ºC SN Buffer 1.234µS/cm 1.234µS/cm 25.0ºC 25.0ºC 25.0ºC 25.0ºC 25.0ºC 25.0ºC 25.0ºC Slope: 59.16 mV/pH Offset: 60 mV SN pH Auto Cal 1.234µS/cm Cal in progress. Please wait. SN pH Auto Cal 1.234µS/cm 10.01pH SN pH Auto Buffer 2 1.234µS/cm Wait SN pH Auto Buffer 2 1.234µS/cm Place Sensor in Buffer 1 Press ENTER SN pH Auto Cal 1.234µS/cm 07.01pH SN pH Auto Buffer 1 1.234µS/cm Wait SN pH Auto Buffer 1 December 2014 Changing slope overrides buffer Cal 25.0ºC Changing offset overrides buffer Cal 1.234µS/cm 25.0ºC SN pH Auto Cal 1.234µS/cm TDS Salinity NaOH HCl Low H2SO4 High H2SO4 NaCl Resistivity Custom Conc’n Temperature Start AutoCal Setup 1.234µS/cm Buffer 1 Buffer 2 25.0ºC SN Calibrate? SN pH Manual Cal SN Enter Value 1.234µS/cm Auto Manual 07.00pH 1.234µS/cm 25.0ºC Free Chlorine Total Chlorine Chloramine Ozone Oxygen pH ORP Redox Conductivity 1.234µS/cm SN pH Buffer Cal 1.234µS/cm 25.0ºC Calibrate? 1.234µS/cm 25.0ºC SN pH Cal 1.234µS/cm C a l i b r a t e Buffer Cal Standardize Slope: 59.16mV/pH Offset: 600 mV M E N U M A I N Section 9: Calibration 1066 Instruction Manual LIQ_MAN_1066 FIGurE 9-1. Calibrate ph Calibration Calibration M E N U M A I N C a l i b r a t e 25.0ºC Calibrate? 1.234µS/cm 25.0ºC Use precision resistors only 25.0ºC 25.0ºC 25.0ºC xx.xx kΩ SN Enter Value 1.234µS/cm 10.00 uS/cm SN Enter Value 1.234µS/cm 25.0ºC 25.0ºC 25.0ºC 25.0ºC Cal in progress. Please wait. SN Meter Cal 1.234µS/cm Cal in progress. Please wait. SN InProcess Cal 1.234µS/cm Press ENTER if reading is stable. SN InProcess Cal 1.234µS/cm 25.0ºC Zeroing Wait SN Zero Cal 25.0ºC Updated cell constant: 1.00135/cm SN InProcess Cal 25.0ºC SN Zero Cal 1.234µS/cm Sensor must be dry and in air 1.234µS/cm 25.0ºC SN Zero Cal 1.234µS/cm Sensor Zero Done 1.234µS/cm 25.0ºC SN Zero Cal Zeroing Wait 1.234µS/cm Sensor must be In 0% solution SN Zero Cal 1.234µS/cm In Air In Water 25.0ºC 25.0ºC SN Zero Cal 1.234µS/cm SN InProcess Cal 1.234µS/cm Wait for stable reading. Zero Cal In Process Cal Meter Cal Cell K: 1.00000/cm SN InProcess Cal Take sample; Press ENTER. 25.0ºC SN Calibration 1.234µS/cm LIQ_MAN_1066 SN Meter Cal 1.234µS/cm Temperature Conductivity 1.234µS/cm TDS Salinity NaOH HCl Low H2SO4 High H2SO4 NaCl Resistivity’ Resistivity’ CustomConc’n Conc’n Custom SN Calibrate? 25.0ºC Free Chlorine pH Independ. Free Cl Total Chlorine Chloramine Ozone Oxygen pH ORP Redox 1.234µS/cm 1066 Instruction Manual Section 9: Calibration December 2014 Figure 9-2. Calibrate Contacting and Toroidal Conductivity 91 92 M E N U M A I N C a l i b r a t e 25.0ºC Calibrate? 1.234µS/cm TDS Salinity NaOH HCl Low H2SO4 High H2SO4 NaCl Resistivity’ Custom Conc’n Temperature Conductivity SN Calibrate? 25.0ºC Free Free Chlorine Chlorine pH Independ. Free Cl Total Chlorine Total Chlorine Chloramine Chloramine Ozone Oxygen pH ORP Redox 1.234µS/cm 25.0ºC 25.0ºC Wait for stable reading SN InProcess Cal 1.234µS/cm Zero Cal In Process Cal SN Calibration 1.234µS/cm 25.0ºC 25.0ºC Press ENTER if reading is stable. SN InProcess Cal 1.234µS/cm Zeroing Wait SN Zero Cal 1.234µS/cm 25.0ºC 25.0ºC Cal in progress. Please wait. SN InProcess Cal 1.234µS/cm 10.00 ppm SN Enter Value 1.234µS/cm Take sample; Press ENTER. SN InProcess Cal 1.234µS/cm Sensor zero done 25.0ºC 25.0ºC SN Zero Cal 1.234µS/cm Section 9: Calibration December 2014 1066 Instruction Manual LIQ_MAN_1066 Figure 9-3. Calibrate Free Chlorine, Total Chlorine, and Monochloramine Calibration Calibration M E N U M A I N C a l i b r a t e 25.0ºC Calibrate? 1.234µS/cm 25.0ºC 25.0ºC Wait for stable reading 25.0ºC SN InProcess Cal 1.234µS/cm Press ENTER if reading is stable. Zeroing Wait 25.0ºC Take sample; Press ENTER. 25.0ºC SN Air Cal 1.234µS/cm 25.0ºC 25.0ºC 25.0ºC 10.00 ppm SN Enter Value 1.234µS/cm Stable Time: 10 sec Stable Delta: 0.05 ppm Salinity: 00.0 ‰ SN Setup 1.234µS/cm Start Calibration Setup SN InProcess Cal 1.234µS/cm Sensor zero done SN Zero Cal 1.234µS/cm Zero Current: 1234nA Air Cal Zero Cal In Process Cal Sen@ 25°C:2500nA/ppm 25.0ºC SN Zero Cal 25.0ºC SN Calibration 1.234µS/cm 1.234µS/cm 25.0ºC 25.0ºC 25.0ºC 25.0ºC 25.0ºC Cal in progress. Please wait. SN InProcess Cal 1.234µS/cm 00.0 ‰ SN Salinity 1.234µS/cm 0.05 ppm SN Stable Delta 1.234µS/cm 10 sec SN Stable Time 1.234µS/cm Done 25.0ºC 25.0ºC SN Air Cal 1.234µS/cm Wait Air Cal 1.234µS/cm 760 mm Hg SN Air Pressure LIQ_MAN_1066 SN InProcess Cal 1.234µS/cm Conductivity 1.234µS/cm Temperature Free Chlorine Total Chlorine Chloramine Ozone Oxygen pH ORP Redox SN Calibrate? TDS Salinity NaOH HCl Low H2SO4 High H2SO4 NaCl Resistivity CustomConc’n 1.234µS/cm 1066 Instruction Manual Section 9: Calibration December 2014 Figure 9-4. Calibrate oxygen 93 94 M E N U M A I N C a l i b r a t e 25.0ºC Calibrate? 1.234µS/cm 25.0ºC TDS Salinity NaOH HCl Low H2SO4 High H2SO4 NaCl Resistivity Custom Conc’n Temperature Conductivity SN Calibrate? Free Chlorine Total Chlorine Chloramine Ozone Oxygen pH ORP Redox 1.234µS/cm 25.0ºC 25.0ºC Wait for stable reading SN InProcess Cal 1.234µS/cm Zero Cal In Process Cal SN Calibration 1.234µS/cm 1.234µS/cm SN InProcess Cal Press ENTER if reading is stable. Zeroing Wait 25.0ºC 25.0ºC SN Zero Cal 1.234µS/cm 25.0ºC 25.0ºC Cal in progress. Please wait. SN InProcess Cal 1.234µS/cm 10.00 ppm SN Enter Value 1.234µS/cm Take sample; Press ENTER. SN InProcess Cal 1.234µS/cm Sensor zero done 25.0ºC 25.0ºC SN Zero Cal 1.234µS/cm Section 9: Calibration December 2014 1066 Instruction Manual LIQ_MAN_1066 Figure 9-5. Calibrate ozone Calibration Calibration M E N U M A I N C a l i b r a t e 25.0ºC Calibrate? 1.234µS/cm Temperature Total Chlorine Chloramine Ozone Oxygen pH ORP Redox Conductivity SN Calibrate? 25.0ºC TDS Salinity NaOH HCl Low H2SO4 High H2SO4 NaCl Resistivity CustomConc’n Free Chlorine 1.234µS/cm 25.0ºC 25.0ºC Stable Time: 10sec Stable Delta: 1 mV SN Setup 1.234µS/cm 25.0ºC 1.234µS/cm 25.0ºC 25.0ºC 25.0ºC 0001 mV 25.0ºC SN Standard M 1.234µS/cm 0000ppm SN Stable Delta 1.234µS/cm SN Standard M 1.234µS/cm Stabilizing Wait SN Stable Time 010 sec 25.0ºC SN Standardize Cal in progress. Please wait. 1.234µS/cm SN 2-Point Cal 1.234µS/cm Standard 1 Standard 2 +0600 mV Standardize 2-Pt Calibration Slope: 0mV/decade Offset: 0 mV Setup SN ISE Cal 1.234µS/cm 25.0ºC SN Enter Value 1.234µS/cm 1066 Instruction Manual LIQ_MAN_1066 Section 9: Calibration December 2014 FIGurE 9-6. Calibrate orp 95 96 M E N U M A I N C a l i b r a t e 25.0ºC Calibrate? 1.234µS/cm Free Chlorine Total Chlorine Chloramine Ozone Oxygen pH ORP Redox Conductivity 1.234µS/cm 25.0ºC Temperature Temperature TDS Salinity NaOH HCl Low H2SO4 High H2SO4 NaCl Resistivity Custom Conc’n SN Calibrate? 25.0ºC +025.0°C SN Calibrate 1.234µS/cm 25.0ºC Cal in progress. Please wait. SN Calibrate 1.234µS/cm 25.0ºC SN Temp Offset > 5°C Continue? No Yes 1.234µS/cm Section 9: Calibration December 2014 1066 Instruction Manual LIQ_MAN_1066 FIGurE 9-7. Calibrate Temperature Calibration 1066 Instruction Manual Section 10: hArT Communication LIQ_MAN_1066 December 2014 Section 10: HART Communications ® 10.1 Introduction The 1066 transmitter can communicate with a HART host using HART Revision 5 or HART Revision 7. The revision of HART used by the 1066 can be selected using the keypad/display or a HART master such as AMS or the 475 Handheld Communicator. The default version of HART is Revision 5. Since some HART hosts cannot accommodate HART 7, the choice of HART Revision should be based on the capabilities of the host, and should be chosen as a first step in configuration. If HART Revision 7 can be used with the host, it does offer a number of advantages over Revision 5, including long tag name, time stamped data, and measurement status, and enhanced burst mode. When hArT 5 is chosen, the Device Revision of the 1066 is Device Revision 1; when hArT 7 is chosen the Device Revision is revision 2 (or greater). The Device Revision of the DD (Device Description) and install files for AMS and DeltaV used should be the same as the Device Revision of the 1066. A single HART 5 (Device Revision 1) or HART 7 (Device Revision 2 or greater) DD (Device Description) is used for all model codes of the 1066, which include the pH/ORP, conductivity, oxygen, chlorine, and ozone transmitters. All 1066 transmitters have the same HART device identification, as outlined below: hArT 5 Device Identification (1066 revision 1): Manufacturer Name: Rosemount Analytical Inc. Model Name: 1066 Manufacturer ID: 46 (0x2E) Device Type Code: 33 (0x0021) hArT protocol revision: 5.1 Device revision: 1 hArT 7 Device Identification (1066 revision 2): Manufacturer Name: Rosemount Analytical Inc. Model Name: 56 Manufacturer ID: 46 (0x2E) Device Type Code: 11809 (0x2E21) hArT protocol revision: 7.3 Device revision: 2 10.2 physical Installation and Configuration 10.2.1 HART Wiring and Output Configuration HART communications is superimposed on Analog Output 1 for all of the measurements and parameters of the 1066. HART Communications 97 Section 10: hArT Communication December 2014 10.2.2 1066 Instruction Manual LIQ_MAN_1066 HART Multidrop (Bus) Configuration The HART Polling Address should be left at its default value of “0”, unless the 1066 is used in a Multidrop configuration with up to 14 other transmitters. When the Polling Address is greater than “0”, the 4-20 mA output is held at 4 mA or below, and does not change in response to changes in the measurement in HART 5. In HART 7, Loop Current Mode should be set to “Off” to hold the current output to a minimum value. 10.2.3 HART Configuration To access the HART Configuration screens, select the “HART” menu item in the Main Menu. If HART 7 is chosen (Univ Cmd Rev = 7), the following controls are available: FIGurE 10-1. hArT 7 Configuration Screen: Basic Definitions • univ Cmd rev – toggles between HART version 5 and HART version 7. If the HART host being used can accommodate HART 7, HART 7 should be chosen due to its larger feature set. If the host can only use HART 5, then HART 5 must be chosen. note: If the 1066 is connected to a HART host and the HART version is changed, the host will likely detect the transmitter as a new transmitter with a different device revision number. 98 • polling address – Choose “0” unless Multidrop is being used. If Multidrop is being used, each transmitter should have its own polling address of from 1 to 15. • Loop current mode – Set Output 1 current to a minimum value for multidrop applications (HART 7 only). • Find Device Cmd – Setting Find Device to “On”, enables the 1066 to be identified by the host. The transmitter returns identity information including device type, revision level, and device ID (HART 7 only). HART Communications 1066 Instruction Manual Section 10: hArT Communication LIQ_MAN_1066 December 2014 • Burst Message 0, 1, 2 – Toggles burst messages 0, 1, and/or 2 on or off (HART 7 only). See the end of section 10.2 for the HART burst commands available. If HART 5 is chosen (Univ Cmd Rev = 5), the following controls are available: FIGurE 10-2. hArT 5 Configuration Screen: Basic Definitions • univ Cmd rev – toggles between HART version 5 and HART version 7. If the HART host being used can accommodate HART 7, HART 7 should be chosen due to its larger feature set. If the host can only use HART 5, then HART 5 must be chosen. note: If the 1066 is connected to a HART host and the HART version is changed, the host will likely detect the transmitter as a new transmitter with a different device revision number. • polling address – Choose “0” unless Multidrop is being used. If Multidrop is being used, each transmitter should have its own polling address of from 1 to 15. • Burst Mode – Toggles the single HART 5 burst message on or off. See below for the HART burst commands available. Burst Commands Available in hArT 5 and hArT 7 If burst messages are enabled by setting the burst messages to on, the information in the burst message can be selected using a HART host from the following commands: • Burst command: off – Turns burst mode off Cmd 1 – Bursts the Primary Value Cmd 2 – Bursts Loop Current + % of range of the Primary Value Cmd 3 – Bursts Dynamic Variables (PV, SV, TV, & QV) + Loop Current Cmd 9 – Bursts up to 8 Device Variables with time stamp and status and Cmd 48 Additional Transmitter Status (HART 7 only) Cmd 33 – Bursts 4 Device Variables Cmd 48 – Bursts Additional Transmitter Status Bits (HART 7 only) Cmd 93 – Bursts Trend Data (HART 7 only) 10.3 Measurements Available via hArT A number of live measurements are made available by HART in addition to the main measurements such as pH or Conductivity. All of these measurements are called Device Variables, which can be mapped to the Dynamic Variables PV, SV, TV, and QV for regular reading by the typical HART host. HART Communications 99 Section 10: hArT Communication December 2014 1066 Instruction Manual LIQ_MAN_1066 Each 1066 transmitter type, 1066P, 1066C, etc. will have its own set of Device Variables, based on the secondary measurements used in making the main measurement. Appendix 10.1 shows the Device Variable for the each transmitter type, and the Dynamic Variables, which they can be mapped to. 10.4 Diagnostics Available via hArT 10.4.1 Status Information – Device Status Bits Bit 0 primary variable out of Limits: This bit is set when PV is out of its limits. Bit 1 non-primary variable out of Limits: This bit is set when any active device variable other than the Primary variable is out of its limits. Bit 2 Loop Current Saturated: This bit is set when Analog Output 1 is not fixed, and it is less than 3.8 mA or greater than 22.0 mA. Bit 3 Loop Current Fixed: This bit is set when Analog Output 1 is being simulated, calibrated, or when a device failure is detected and the Analog Output 1 is configured to output a fixed value. Bit 4 More Status Available: The “more status available” bit will be set when the device status condition occurs (i.e. bit goes from 0 to 1) on at least one of the Additional Transmitter Status bits are set. Bit 5 Cold Start: This bit is set when a Master Reset is performed either by Command 42, or a power cycle. 2 bits are maintained internally, for primary and secondary masters. Bit 6 Configuration Changed: This bit is set when a configuration or calibration parameter is changed either through a write command or a local interface command. 2 bits are maintained internally, for primary and secondary masters. Bit 7 Field Device Malfunction: This bit is set when a fault condition is detected in the device electronics or sensor. 10.4.2 Status Information – Extended Device Status Bits (HART 7 only) Bit 0 Maintenance required: This bit is set when a device fault is detected. Bit 1 100 Device variable Alert: HART Communications 1066 Instruction Manual Section 10: hArT Communication LIQ_MAN_1066 December 2014 This bit is set when any enabled device variable status is not good. Bit 2 Critical power Failures: This bit is not supported and will always be cleared on 1066. 10.4.3 10.5 10.5.1 Additional Transmitter Status (Command 48) Additional Transmitter Status provides diagnostic status bits specific to the condition of sensors, electronics, and the memory of the 1066. Calibration errors and notification of events, such as calibration in progress and relay activation are also indicated by status bits. Appendix 10.2 shows these bits organized according to the 1066 transmitter measurement type. hArT hosts A HART host can access live measurements, diagnostic messages, and provide a tool for configuring the measurement and calibrating the 1066. The configuration parameters for the 1066 transmitter are listed in Appendix 10.3. Two examples of HART hosts are shown below. AMS Intelligent Device Manager The AMS Device Intelligent Device Manager is member of the AMS Suite of asset management applications, which provides tools for configuration, calibration, diagnosing, and documenting FIGurE 10-3. Main Measurement and overall Status HART Communications 101 Section 10: hArT Communication December 2014 1066 Instruction Manual LIQ_MAN_1066 FIGurE 10-4. Device variables and Dynamic variables FIGurE 10-5. Diagnostic Messages (Additional Transmitter Status) 102 HART Communications 1066 Instruction Manual LIQ_MAN_1066 Section 10: hArT Communication December 2014 FIGurE 10-6. Configuration FIGurE 10-7. Calibration HART Communications 103 Section 10: hArT Communication 1066 Instruction Manual December 2014 10.5.2 LIQ_MAN_1066 transmitters and valves. The following AMS windows are examples of these functions: FIGurE 10-8. 475 Field Communicator 475 Field Communicator HART (and Fieldbus) devices can be accessed in the field using the 475, which provides the same basic functionality as the AMS Intelligent Device Manager. Asset management information can be uploaded into the AMS database from the 475 for a common database for asset 10.6 Wireless Communication using the 1066 The 1066 can communicate by Wireless HART using the Smart Wireless THUM Adaptor and the 1420 Smart Wireless Gateway. All the information available with the wired device can be accessed wirelessly, making it possible to have the measurements and benefits of HART communication in locations where running cable would be difficult or prohibitively expensive. FIGurE 10-9. Wireless Communication using the 1066 Although HART 5 or HART 7 can burst the Dynamic Variables (PV, SV, TV, & QV), HART 7 should be used with the THUM because up to 8 Device Variables can be continually burst using Command 9. 10.7 104 Field Device Specification (FDS) For more details on the implementation of HART in the 1066 and its command structure, the Field Device Specification for the relevant Device Revision should be consulted. They can be downloaded from our website. HART Communications 1066 Instruction Manual Section 10: hArT Communication LIQ_MAN_1066 December 2014 AppEnDIx 10.1 – Device variables 1066 ph Device variables Device variable name Assignable to Dynamic variables variable range primary value Type: pH (1) PV, SV, TV or QV 0 to 14 pH ORP (2) PV, SV, TV or QV -1500 to 1500 mV Redox (3) PV, SV, TV or QV -1500 to 1500 mV SV, TV or QV -15 to 200 °C other Device variables: Temperature 5 to 360 °F Sensor mV input TV or QV -750 to 750 mV Sensor Glass impedance TV or QV 0 to 2000 Mμ Sensor Reference impedance TV or QV 0 to 10000 kμ Assignable to Dynamic variables variable range 1066C and 1066T Device variables Device variable name primary value Type: Conductivity (7) PV, SV, TV or QV 0 to 2000000 µS/cm Resistivity (8) PV, SV, TV or QV 0 to 50000000 μ-cm NaOH (9) PV, SV, TV or QV 0 to 12 % HCl (10) PV, SV, TV or QV 0 to 15 % Low H2SO4 (11) PV, SV, TV or QV 0 to 25 % High H2SO4 (12) PV, SV, TV or QV 96 to 99.7 % NaCl (13) PV, SV, TV or QV 0 to 25 % Custom Concentration (14) PV, SV, TV or QV 0 to 1000 ppm % Concentration: 0 to 1000 mg/L 0 to 100 g/L 0 to 100 % 0 to 1000 None TDS (15) PV, SV, TV or QV 0 to 10000 ppm Salinity (16) PV, SV, TV or QV 0 to 36 ppth SV, TV or QV -25 to 200 °C other Device variables: Temperature -13 to 360 °F Temperature resistance TV or QV 0 to 100000 μ Conductance TV or QV 0 to 2000000 µS Input resistance TV or QV 0 to 500 kμ Raw Conductivity TV or QV 0 to 2000000 µS/cm Raw Resistivity TV or QV 0 to 50000000 ohm-cm HART Communications 105 Section 10: hArT Communication 1066 Instruction Manual December 2014 LIQ_MAN_1066 1066Do Device variables Device variable name Assignable to Dynamic variables variable range primary value Type: Oxygen (17) PV, SV, TV or QV 0 to 100 ppm 0 to 1000 ppb 0 to 100 mg/L 0 to 1000 µg/L 0 to 300 % Saturation 0 to 760 mmHg 0 to 30 inHg 0 to 1 bar 0 to 1000 mbar 0 to 100 kPa 0 to 1 atm other Device variables: Temperature PV, SV, TV or QV Temperature resistance Sensor input current TV or QV PV, SV, TV or QV -15 to 200 °C 5 to 360 °F 0 to 100000 μ 0 to 100000 nA Assignable to Dynamic variables variable range primary value Type: Ozone (18) PV, SV, TV or QV 0 to 20 ppm 0 to 1000 ppb 0 to 20 mg/L 0 to 1000 µg/L other Device variables: Temperature PV, SV, TV or QV Temperature resistance Sensor input current TV or QV PV, SV, TV or QV -15 to 200 °C 5 to 360 °F 0 to 100000 μ 0 to 100000 nA Assignable to Dynamic variables variable range primary value Type: Chlorine (19) PV, SV, TV or QV 0 to 20 ppm 0 to 1000 ppb 0 to 20 mg/L 0 to 1000 µg/L other Device variables: Temperature PV, SV, TV or QV Temperature resistance Sensor input current pH (free chlorine pH compensation) TV or QV PV, SV, TV or QV SV, TV or QV -15 to 200 °C 5 to 360 °F 0 to 100000 μ 0 to 100000 nA 0 to 14 pH 1066oz Device variables Device variable name 1066CL Device variables Device variable name 106 HART Communications 1066 Instruction Manual Section 10: hArT Communication LIQ_MAN_1066 December 2014 AppEnDIx 10.2 – Additional Transmitter Status – Command 48 Status Bits 1066 ph Device variables Byte / Bit Meaning / Class Device Status Bits Set 1/0 Cpu Error / Error The software checksum is not as expected. The CPU memory has been corrupted. 4 – More Status Available 7 – Field Device Malfunction 1/1 Self-Test Fail / Error An electronic component is out of specification. 4 – More Status Available 7 – Field Device Malfunction 1/2 Factory Data Error / Error 4 – More Status Available An error was detected in the factory segment of the non-volatile memory. At 7 – Field Device Malfunction least one factory configuration parameter has been corrupted. 1/3 hardware/Software Mismatch / Error The software is not compatible with the hardware. 4 – More Status Available 7 – Field Device Malfunction 1/4 Internal Communications Error / Error The analog input electronics is non-responsive. 4 – More Status Available 7 – Field Device Malfunction 3/0 Keypad Error / Warning At least one key in the device keypad is stuck. This condition makes the local 4 – More Status Available operator interface unuseable. If no other alerts are present, the device can still perform its other functions normally. 3/1 user Data Error / Warning An error was detected in the non-volatile memory. One or more user config4 – More Status Available uration parameter may be corrupted. Reset analyzer to factory defaults and re-configure the device. If the problem persists, replace device. 3/2 need Factory Calibration / Warning The device's non-volatile memory has been corrupted. The device measurements may be out of specification. 4 – More Status Available 3/3 Software Mismatch / Warning The input CPU software is not fully compatible with the main CPU software. 4 – More Status Available 3/7 reset In progress / other The transmitter's configuration is being reset to factory defaults. 4 – More Status Available 6/6 Maintenance required / other 4 – More Status Available 6/1 Device variable Alert / other 4 – More Status Available 8/0 Simulation Active / Mode A device variable is being simulated. 4 – More Status Available 8/1 non-volatile Memory Defect / Warning 4 – More Status Available 8/2 volatile Memory Defect / Error 4 – More Status Available 8/3 Watchdog reset Executed / other 4 – More Status Available 8/4 power Supply Condition out of range / Warning 4 – More Status Available 8/5 Environmental Condition out of range / Warning 4 – More Status Available 8/6 Electronic Defect / Error Reset device or turn power off then on. If problem persists, replace device. 4 – More Status Available HART Communications 107 Section 10: hArT Communication December 2014 1066 Instruction Manual LIQ_MAN_1066 1066 ph Device variables continued Byte / Bit Meaning / Class Device Status Bits Set 8/7 Device Locked / Mode Locked device prevents all host modifications. Unlock device to make changes to the device. 4 – More Status Available 10 / 0 Analog Channel 1 Saturated / Warning The primary variable is outside the analog output range. 1. Check the primary value. 2. Check the analog output scaling. 4 – More Status Available 10 / 1 Analog Channel 2 Saturated / Warning The secondary variable is outside the analog output range. 1. Check the secondary value. 2. Check the analog output scaling. 4 – More Status Available 13 / 0 Analog Channel 1 Fixed / Mode Output 1 is either being tested, calibrated, or accidentally left on hold. A fault condition could also set the analog output to a fixed value. If there is no active fault, wait for test or calibration to end or take Output 1 out of hold mode. 4 – More Status Available 13 / 1 Analog Channel 2 Fixed / Mode Output 2 is either being tested, calibrated, or accidentally left on hold. A fault condition could also set the analog output to a fixed value. If there is no active fault, wait for test or calibration to end or take Output 2 out of hold mode. 4 – More Status Available Temperature Status Bits Byte / Bit Meaning / Class 108 Device Status Bits Set 0/0 Temperature Error / Error The temperature measuring circuit is open or shorted. Check the wiring and the temperature element in the sensor. If the temperature element in the sensor is open or shorted, replace the sensor. 4 – More Status Available 7 – Field Device Malfunction 2/0 Temperature high / Warning The measured temperature is above the temperature range of the transmitter and can damage the sensor. The temperature limits are: 1066P / 1066DO, CL, and OZ: Temperature > 150°C 1066C and 1066T: Temperature > 300°C 1. Check process temperature. 2. Check sensor and its wiring. 1 – non-primary variable out of Limits 4 – More Status Available 2/1 Temperature Low / Warning The measured temperature is below the temperature range of the transmitter and can damage the sensor. The temperature limits are: 1066P / 1066DO, CL, and OZ: Temperature < -15°C 1066C and 1066T: Temperature -25°C 1. Check process temperature. 2. Check sensor and its wiring. 1 – non-primary variable out of Limits 4 – More Status Available 2/2 rTD Sense Line open / Warning The sense line of the temperature sensor is not connected. 1. Check sensor wiring. 2. If a 2-wire RTD is being used for temperature compensation, use wire jumper to connect sense and return terminals. 4 – More Status Available 5/1 Temperature Calibration In progress / other A temperature calibration is or has been performed. 4 – More Status Available HART Communications 1066 Instruction Manual Section 10: hArT Communication LIQ_MAN_1066 December 2014 1066ph/orp Status Bits Byte / Bit Meaning / Class Device Status Bits Set 0/1 reference Impedance Too high / Error The reference impedance is above the high fault setpoint. The reference electrode may be coated or plugged. 1. Clean or replace the sensor. 2. Check sensor wiring. 3. Increase the setpoint value. 4. Set the reference impedance level to high. 4 – More Status Available 7 – Field Device Malfunction 0/2 Glass Impedance Too high / Error The glass impedance is above the high fault setpoint. The glass electrode may be severely coated. 1. Clean or replace sensor. 2. Check sensor wiring. 3. Increase the glass impedance high fault setpoint. 4 – More Status Available 7 – Field Device Malfunction 0/3 Broken ph Glass / Error The glass impedance is too low. The glass electrode of the pH sensor may be 4 – More Status Available cracked. 1. Check sensor. Replace sensor if cracks are present. 7 – Field Device Malfunction 2. Check sensor wiring. 3. Check preamplifier location configuration. 2/3 ph voltage Too high / Warning The sensor voltage is outside the expected range for a pH measurement. 1. Check sensor wiring. 2. Replace sensor. 4/0 ph Slope Too high / Warning The pH slope calculated during buffer calibration exceeded the maximum slope limit. 1. Check the buffers used and retry buffer calibration. 4 – More Status Available 2. Increase the maximum slope limit (default is 62 mV/pH). Note: A slope of 62 mV/pH or greater indicates that there has been an error made during calibration or a faulty pH sensor. 3. Replace sensor. 4/1 ph Slope Too Low / Warning The pH slope calculated during buffer calibration was below the minimum slope limit. The pH electrode may be worn out, damaged, or coated. 1. Check and clean sensor, then retry buffer calibration. 2. Decrease minimum slope limit (default is 40 mV/pH). Note that a pH sensor with a slope less than 50 mV/pH is usually near the end of its useful life. 3. Replace sensor. 4 – More Status Available 4/2 zero offset Error / Warning The zero offset from a buffer calibration or single point standardization has exceeded the limit. The reference electrode may be poisoned or plugged. 1. Check and clean sensor, then retry buffer calibration. 2. Increase maximum offset limit (default is 60mV). Note that a pH sensor with an offset of 60 mV or greater is likely poisoned and has to be replaced. 3. Replace sensor. 4 – More Status Available 4/3 Calibration Error / Warning 4 – More Status Available 5/4 ph Standardization In progress / other A pH standardization is being or has been performed. 4 – More Status Available 5/5 Buffer Calibration In progress / other A pH buffer calibration is being or has been performed. 4 – More Status Available 5/6 Stabilization In progress / other A pH sensor is stabilizing or has been stabilizing. 4 – More Status Available HART Communications 4 – More Status Available 109 Section 10: hArT Communication December 2014 1066 Instruction Manual LIQ_MAN_1066 1066C and 1066T Status Bits continued Byte / Bit 110 Meaning / Class Device Status Bits Set 2/5 need zero Calibration / Warning The sensor offset is too high resulting in a negative reading. This trigger point for this alert is dependent upon the conductivity measurement technology: 1066C: (conductance - zero offset) < -2µS 1066T: (conductance - zero offset) < -50µS A sensor zero calibration should be performed. 4 – More Status Available 2/6 Concentration out of range / Warning The measured concentration is outside the conductivity range where a valid concentration can be derived for the following 5 concentrations: 0 to 20% NaCl 0 to 12% NaOH 0 to 15% HCl 0 to 25% H2SO4 96 to 99.7% H2SO4. If there are no other fault conditions check process temperature and check that the actual concentration is outside the range for which curve is defined. 4 – More Status Available 2/7 Input out of range / Warning The input is outside the device measurement range. the range limits are: 1066C (2- electrode conductivity): Conductance > 500mS 1066CT (4- electrode conductivity): (Conductance > 3000mS) or (Vcond < 0mV) 1066T: Conductance > 1500mS 1. Check sensor wiring. 2. Replace sensor. 4 – More Status Available 4/3 Calibration Error / Warning An error occurred in the last calibration procedure. Check sensor and repeat the calibration procedure. 4 – More Status Available 4/4 Sensor zero Error / Warning An error occurred in the last sensor zero procedure. Check sensor and repeat sensor zero procedure. 4 – More Status Available 5/2 Sensor zero In progress / other A sensor zero is being or has been performed. 4 – More Status Available 5/3 zero Cal In Water In progress / other A zero calibration in water is being or has been performed. 4 – More Status Available 5/4 Meter Calibration In progress / other A meter calibration is being or has been performed. 4 – More Status Available 5/5 Curve Fit In progress / other A curve fit is being or has been performed. 4 – More Status Available HART Communications 1066 Instruction Manual LIQ_MAN_1066 Section 10: hArT Communication December 2014 1066Do, 1066CL, 1066oz Statuss Bits Byte / Bit Meaning / Class 2/4 SEnSor_CurrEnT > 300 nA for OXYGEN BioRx - Other SENSOR_CURRENT > 800 nA for OXYGEN Brewing SENSOR_CURRENT > 106 uA for OXYGEN Oxygen in Gas SENSOR_CURRENT > 350 nA for Ozone SENSOR_CURRENT > 5 uA for Free Chlorine SENSOR_CURRENT > 40 uA for Total Chlorine SENSOR_CURRENT > 20 uA for Monochloramine Device Status Bits Set 4 – More Status Available 1. Make sure the device configuration matches the sensor being used. 2. Check sensor wiring. 3. Replace sensor. 2/5 need zero Calibration / Warning The sensor offset is too high resulting in a negative reading. The sensor zero limits are: PV < -0.5 if unit is ppm or mg/L PV < -50 if unit is ppb or ug/L PV < -2.0 % for % Saturation PV < -2.0 % for Concentration in Gas PV < -20 ppm for Concentration in Gas PV < -30 mmHg for Partial Pressure 4 – More Status Available Perform sensor a zero calibration. 4/3 Calibration Error / Warning There has been a calibration error. Check the sensor. 4/4 Sensor zero Error / Warning An error occurred in the last sensor zero procedure. Check sensor and repeat sensor zero procedure. 5/2 Sensor zero In progress / other A sensor zero is being or has been performed. 4 – More Status Available 5/3 Air Cal In progress / other An air calibration is being or has been performed. 4 – More Status Available 5/6 Stabilization In progress / other The sensor is stabilizing or has stabilized. 4 – More Status Available HART Communications 4 – More Status Available 111 Section 10: hArT Communication 1066 Instruction Manual December 2014 LIQ_MAN_1066 AppEnDIx 10.3 – 1066 hArT Configuration parameters parameters Common to All 1066 Transmitters Type input_filter_type Selects between continuous and adaptive filtering of the measurement. pv_damping_value Provides the filter time constant. instrument_software_version The software version of the main processor. input_software_version The software version of the input processor. Display parameters: Enumeration / range read/Write Default ENUM Adaptive Continuous R/W Adaptive FLOAT 0.0 -- 99.0 seconds R/W 0 FLOAT R FLOAT R loi_language Selects the language to be displayed by the 1066. ENUM loi_warnings Enables or disables the display of transmitter warnings. ENUM loi_configuration_code Locks and unlocks access to configuration from the keypad display of the 1066. "000" disables. English Français Español Deutsch Enable Disable Italiano Português Chinese Russian R/W English R/W Enable UINT (2) R/W 0 loi_calibration_code Locks and unlocks access to calibration from the keypad display of the 1066. "000" disables. UINT (2) R/W 0 loi_main_display_upper Selects the measurement displayed on the upper portion of the main display. ENUM Assign PV Blank R/W Assign PV ENUM Compensating pH (free Cl) Temperature PV Blank R/W Temperature ENUM Valid List per 1066 Model R/W ENUM Valid List per 1066 Model R/W ENUM Valid List per 1066 Model R/W ENUM Valid List per 1066 Model R/W loi_main_display_center Selects the measurement displayed on the center portion of the main display. loi_main_display_left Selects the measurement or output displayed on the left portion of the display. loi_main_display_lower_left Selects the measurement or output displayed on the lower left portion of the display. loi_main_display_right Selects the measurement or output displayed on the right portion of the display. loi_main_display_lower_right Selects the measurement or output displayed on the lower right portion of the display. valid List Input mv Glass Impedance 1066ph/orp: ref Impedance Slope zero offset valid List 1066C/T: raw Conductivity raw resistivity valid List 1066Do/CL/oz: Input Current ph (if free chlorine) All 1066: 112 valid List Ao 1 Current Ao 1 % output Ao 2 Current Ao 2 % output HART Communications 1066 Instruction Manual Section 10: hArT Communication LIQ_MAN_1066 December 2014 1066 Temperature parameters Type Enumeration / range read/Write Default rtd_offset The temperature offset resulting from a temperature calibration. FLOAT R/W 0 rtd_slope The slope (dimensionless) resulting from a two point temperature calibration. (Valid for cell constants < 0.02 1/cm) FLOAT R/W 1 R/W Automatic R/W 25.0 C read/Write Default R/W 0.0 mV R/W 59.16 mV/pH R/W 60 temp_comp_mode Selects automatic or manual temperature compensation. manual_temperature If manual temperature compensation is chosen, provides a constant temperature value used by the transmitter. ENUM Manual Automatic FLOAT 1066 ph/orp Type zero_offset The zero offset of a pH sensor resulting from a calibration. ph_slope The slope of a pH sensor resulting from a buffer calibration. zero_offset_limit The maximum value of the zero offset allowed for a successful calibration. min_ph_slope The minimum value of the slope allowed for a successful calibration. max_ph_slope The maximum value of the slope allowed for a successful calibration. ph_stabilization_time The period of time used to determine stability of a pH sensor during automatic calibration. Enumeration / range FLOAT FLOAT 40 -- 62 mV/pH FLOAT FLOAT 40 -- 62 mV/pH R/W 40 mV/pH FLOAT 40 -- 62 mV/pH R/W 62 mV/pH FLOAT 0 -- 99 seconds R/W 10 seconds FLOAT 0.01 -- 1.0 pH R/W 0.02 pH ph_buffer_standard The types of pH buffers available for automatic calibration. ENUM Standard / Nist DIN 19267 Ingold Merck Fisher R/W Standard / Nist preamp_location The location of the preamplifier in a pH measurement. ENUM analyzer sensor / J-box R/W reference_impedance_level Configures the transmitter to use reference electrodes with impedances less than 500 kohm (low) or greater than 500 kohm (high). ENUM Low High R/W ph_solution_temperature_correction Configures the transmitter to correct the pH measurement for changes in the pH of the solution with temperature. ENUM Off ultra pure water high pH ammonia custom ph_solution_temperature_coefficient The coefficient used to correct solution pH when using custom solution pH temperature correction. FLOAT -9.999 -- 9.999 pH/deg C ph_stabilization_value The pH change used to determine stability of a pH sensor during automatic calibration. HART Communications Low Off R/W 0.000 pH/degC 113 Section 10: hArT Communication 1066 Instruction Manual December 2014 LIQ_MAN_1066 1066 ph/orp continued Type Enumeration / range read/Write Default ph_display_resolution Changes the resolution of the displayed pH value. ENUM 0.01 pH 0.1 pH R/W 0.01 pH ph_sensor_isopotential The pH at which the millivolt output of the pH sensor remains constant with temperature changes; virtually always 7.00 pH. FLOAT 0.00 -- 14.00 pH R/W 7.00 pH FLOAT 0.0 -- 9,999.0 kohm R/W 500.0 kohm FLOAT 0.0 -- 9,999.0 Mohm R/W 1,500 Mohm ENUM Off On R/W Off ENUM Off On R/W Off Advanced Basic R/W Advanced refz_high_fault_setpoint The high setpoint that triggers a reference electrode impedance alert. glassz_high_fault_setpoint The high setpoint that triggers a glass pH electrode impedance alert. diagnostics_switch Turns the glass and reference electrode impedance measurements on and off. glassz_temperature_correction Turns temperature correction of the glass impedance measurement on and off. glassz_measurement_type Toggles between a basic glass impedance measurement, and ENUM an advanced impedance measurement that is more accurate. calculated_offset The preliminary zero offset calculated by a pH calibration before it is accepted by the transmitter. calculated_slope The preliminary slope calculated by a pH calibration before it is accepted by the transmitter. 114 FLOAT R/W FLOAT R/W HART Communications 1066 Instruction Manual Section 10: hArT Communication LIQ_MAN_1066 December 2014 1066C and 1066T Type Enumeration / range read/Write Default conductivity_unit The conductivity unit used by the measurement. ENUM mS/cm mS/cm R/W mS/cm cell_constant The cell constant of the conductivity sensor being used, typically determined by calibration. FLOAT 0.0001-- 100.0 /cm R/W 1.00 /cm cable_correction Selects automatic or manual cable resistance correction. ENUM Manual Automatic R/W Automatic FLOAT 0.0 -- 99.99 ohm R/W 0.0 ohm manual_cable_resistance The known cable resistance used in manual cable correction. zero_offset_in_air The zero offset determined by a zero calibration in air. zero_offset_in_soln The zero offset determined by a zero calibration in a solution. FLOAT R only 0.0 mS FLOAT R only 0.00% custom_curve_num_data_points The number of conductivity and concentration points to be used to calculate a custom concentration curve. ENUM R/W 3 2 3 4 5 Custom Curve Concentration Data points: custom_curve_concentration_1 FLOAT R/W custom_curve_concentration_2 FLOAT R/W custom_curve_concentration_3 FLOAT R/W custom_curve_concentration_4 FLOAT R/W custom_curve_concentration_5 FLOAT R/W custom_curve_conductivity_1 FLOAT R/W custom_curve_conductivity_2 FLOAT R/W custom_curve_conductivity_3 FLOAT R/W custom_curve_conductivity_4 FLOAT R/W custom_curve_conductivity_5 FLOAT R/W Custom Curve Conductivity Data points: HART Communications 115 Section 10: hArT Communication 1066 Instruction Manual December 2014 LIQ_MAN_1066 1066C Type read/Write Default R/W 2-Electrode R/W Automatic R/W Off R/W 0.95 /cm R/W Linear slope R/W 2.0 %/degree C R/W 25.0 C read/Write Default ENUM 228 225 226 247 Other R/W 228 ENUM Automatic 50-600mS 0.5-100mS 90-1500mS R/W Automatic ENUM Linear slope Raw / None R/W Linear slope FLOAT R/W 2.0 %/degree C FLOAT R/W 25.0 C electrode_type Type of contacting conductivity sensor being used by the transmitter. ENUM cond_range Selects a particular range for the conductivity measurement or automatic ranging for 2 and 4 electrode sensors. ENUM Enumeration / range 2-Electrode 4-Electrode 2-Electrode: 4-Electrode: series_cap_correction Turns capacitance correction on and off. ENUM cell_factor The second calibration constant used by a 4 electrode sensor in addition to cell constant. FLOAT Automatic 0-50mS 40-500mS 400-2000mS 1.8-20mS 18-200mS Automatic 0-42mS/cm 36-200mS/cm 180-1000mS/cm 0.9-10mS/cm 9-600mS/cm Off On temp_comp_type The type of temperature compensation used by the transmitter. ENUM Linear slope Neutral salt Cation Raw / None temp_comp_slope Provides a slope value used in linear temperature compensation. FLOAT 0.2 -- 9.99 %/degreec C reference_temperature The temperature that temperature compensation corrects to. It is usually 25 C. FLOAT 1066T Type toroidal_sensor_model Selects the model of toroidal sensor being used for enhanced accuracy. cond_range Selects a particular range for the conductivity measurement or automatic ranging for toroidal sensors. temp_comp_type The type of temperature compensation used by the transmitter. temp_comp_slope Provides a slope value used in linear temperature compensation. reference_temperature The temperature that temperature compensation corrects to. It is usually 25 C. 116 Enumeration / range HART Communications 1066 Instruction Manual Section 10: hArT Communication LIQ_MAN_1066 December 2014 1066oz/CL/Do Type polar_voltage The polarization voltage used by the transmitter; automatically set by sensor selection. temp_coeff The temperature coefficient used to compensate temperature; automatically set by sensor selection. amp_sensor_sensitivity The response of the sensor to changes in concentration, determined by calibration. amp_sensor_zero_current The current output of the sensor when the concentration is 0. It is determined by a zero calibration. Enumeration / range read/Write Default FLOAT R/W 0 FLOAT R/W 0 FLOAT 0.1 -- 1,000,000.0 nA/ppm R/W 2,500 nA/ppm FLOAT -999.9 -- 999.9 nA R/W 0.0 nA 1066oz ozone_resolution The resolution of the displayed ozone measurement. Type Enumeration / range read/Write Default ENUM 0.001 0.01 R/W 0.001 read/Write Default R/W Free Chlorine 1066CL Type Enumeration / range Free Chlorine Total Chlorine Chloramine chlorine_type The type of chlorine being measured. ENUM chlorine_resolution The resolution of the displayed chlorine measurement. ENUM 0.001 ppm 0.01 ppm R/W 0.001 ppm ph_correction_mode Turns automatic pH compensation of free chlorine measurements on and off. ENUM On Off R/W Off manual_ph Provides a constant pH value, if manual pH compensation of a free chlorine measurement is used. FLOAT 0.00 -- 14.00 pH R/W 7.00 pH HART Communications 117 Section 10: hArT Communication 1066 Instruction Manual December 2014 LIQ_MAN_1066 1066Do Type read/Write Default ENUM Water/Waste Trace Oxygen BioRx-Rosemount BioRx-Other Brewing Oxygen In Gas R/W Water/Waste oxygen_measurement_type The type of oxygen measurement being made. ENUM Concentration in Liquid Percent Saturation Partial Pressure Concentration in Gas R/W Concentratio n in Liquid oxygen_salinity The salinity of the process solution, which is used by the transmitter to correct for the effect of salinity on the oxygen measurement. FLOAT 0.0 - 99.9 ppth R/W 0.0 ppth pressure_units The units of pressure used by the oxygen measurement. ENUM mmHg inHg psi atm kPa mbar bar R/W mmHg oxygen_process_pressure The process pressure used by the transmitter to calculate percent oxygen in gas or % saturation. FLOAT R/W 760.0 mmHg oxygen_air_pressure The barometric pressure used by the transmitter during an air calibration. FLOAT R/W 760.0 mmHg oxygen_units The available units used for the various oxygen measurement types. ENUM R/W oxygen_sensor_type The type of oxygen sensor used. Enumeration / range units: Concentration in ppm ppb Liquid: mg/L mg/L percent Saturation units: % partial pressure units: mmhg inhg psi atm oxygen In Gas units: ppm % ppm % kpa mbar bar mmHg % air_cal_stabilization_time The period of time used to determine stability of an oxygen sensor during an air calibration. FLOAT 0 -- 99 seconds R/W 10 seconds air_cal_stabilization_value The change in the oxygen measurement used to determine stability of an oxygen sensor during an air calibration. FLOAT 0.001 -- 9,999.0 R/W 0.05 air_cal_stabilization_value_unit The unit used during an air calibration. FLOAT R/W ppm 118 HART Communications 1066 Instruction Manual Section 10: hArT Communication LIQ_MAN_1066 December 2014 AppEnDIx 10.4 – 475 Menu Tree for 1066 hArT 7 1. overview 1.1. Device Status 1.2. Comm Status 1.3. PV 1.4. SV 1.5. Loop Current 1.6. % of Range 1.7. Find Device 1.8. Device Information 1.8.1. Identification 1.8.1.1. Tag 1.8.1.2. Long Tag 1.8.1.3. Model 1.8.1.4. Serial Number 1.8.1.5. Date 1.8.1.6. Descriptor 1.8.1.7. Message 1.8.2. Revision Numbers 1.8.2.1. Universal 1.8.2.2. Field Device 1.8.2.3. DD Revision 1.8.2.4. Hardware 1.8.2.5. Instrument Software 1.8.2.6. Input Software 2. Configure 2.1. Guided Setup 2.1.1. Basic Setup 2.2. Manual Setup 2.2.1. Device Information 2.2.1.1. Tag 2.2.1.2. Long Tag 2.2.1.3. Descriptor 2.2.1.4. Message 2.2.1.5. Date 2.2.1.6. Current Date 2.2.1.7. Current Time 2.2.1.8. Set Date and Time 2.2.2. Measurement (1066 ph/orp) 2.2.2.1. PV is 2.2.2.2. Preamp Location 2.2.2.3. Soln Temp Correct’n (pH only) 2.2.2.4. Temp Coefficient (PV is pH and Soln Temp Correct’n is Custom) 2.2.2.5. Resolution (pH only) 2.2.2.6. Sensor Isopotential (pH only) 2.2.2.7. Input Filter 2.2.2.8. Filter Type 2.2.2.9. Reference Imp 2.2.3. Measurement (1066 Do) 2.2.3.1. Sensor Type 2.2.3.2. Measurement Type 2.2.3.3. PV Unit 2.2.3.4. Salinity 2.2.3.5. Pressure Unit 2.2.3.6. Input Filter 2.2.3.7. Filter Type 2.2.3.8. Polar Voltage 2.2.3.9. Temp Coefficient HART Communications 119 Section 10: hArT Communication 1066 Instruction Manual December 2014 LIQ_MAN_1066 2.2.4. Measurement (1066 oz) 2.2.4.1. PV Unit 2.2.4.2. Resolution 2.2.4.3. Input Filter 2.2.4.4. Filter Type 2.2.4.5. Polar Voltage 2.2.4.6. Temp Coefficient 2.2.5. Measurement (1066 CL) 2.2.5.1. Measurement Type 2.2.5.2. PV Unit 2.2.5.3. Resolution 2.2.5.4. pH Correction (Free Chlorine Measurement Type only) 2.2.5.4.1. pH Correction If pH Correction is manual 2.2.5.4.2. Manual pH If pH Correction is Live/Continuous 2.2.5.4.3. Preamp Location 2.2.5.4.4. Resolution 2.2.5.4.5. Sensor Isopotential 2.2.5.4.6. Soln Temp Correct’n 2.2.5.5. Input Filter 2.2.5.6. Filter Type 2.2.5.7. Polar Voltage 2.2.5.8. Temp Coefficient 2.2.6. Measurement (1066 C and 1066 T) 2.2.6.1. Measurement Type 2.2.6.2. PV Unit 2.2.6.3. Sensor Config 2.2.6.3.1. Sensor Type (Contacting Model) 2.2.6.3.2. Sensor Model (Toroidal Model) 2.2.6.3.3. Range 2.2.6.3.4. Cell Constant 2.2.6.3.5. Cell Factor (4-Electrode) 2.2.6.3.6. RTD Offset (Cell Constant < 0.02) 2.2.6.3.7. RTD Slope (Cell Constant < 0.02) 2.2.6.4. Setup Custom Curve (Custom Curve Measurement) 2.2.6.5. Temp Comp 2.2.6.5.1. Temp Comp Type 2.2.6.5.2. Temp Slope 2.2.6.5.3. Reference Temp 2.2.6.6. Cable Correction (2-Electrode or Toroidal) 2.2.6.6.1. Series Cap Corr 2.2.6.6.2. Cable R. Correction 2.2.6.6.3. Cable Resistance 2.2.6.7. Input Filter 2.2.6.8. Filter Type 2.2.7. Temperature 2.2.7.1. Temperature Unit 2.2.7.2. Temp Comp 2.2.7.3. Manual Value (If Temp Comp is Manual) 2.2.8. Analog outputs 2.2.8.1. Output 1 2.2.8.1.1. Primary Variable 2.2.8.1.2. PV URV 2.2.8.1.3. PV LRV 2.2.8.1.4. Scale 2.2.8.1.5. Dampening 2.2.8.1.6. Fault Mode 2.2.8.1.7. Fault Value 120 HART Communications 1066 Instruction Manual Section 10: hArT Communication LIQ_MAN_1066 December 2014 2.2.8.2. Output 2 2.2.8.2.1. Secondary Variable 2.2.8.2.2. SV URV 2.2.8.2.3. SV LRV 2.2.8.2.4. Scale 2.2.8.2.5. Dampening 2.2.8.2.6. Fault Mode 2.2.8.2.7. Fault Value 2.2.9. Communications 2.2.9.1. Burst Message 1 2.2.9.1.1. Burst Message 2.2.9.1.2. Message Content 2.2.9.1.3. Update Rate 2.2.9.1.3.1. Trigger Mode 2.2.9.1.3.2. Trigger Level 2.2.9.1.3.3. Trigger Level Unit 2.2.9.1.3.4. Classification 2.2.9.1.3.5. Update Rate 2.2.9.1.3.6. Default Update Rate 2.2.9.2. Burst Message 2 2.2.9.2.1. Burst Message 2.2.9.2.2. Message Content 2.2.9.2.3. Update Rate 2.2.9.2.3.1. Trigger Mode 2.2.9.2.3.2. Trigger Level 2.2.9.2.3.3. Trigger Level Unit 2.2.9.2.3.4. Classification 2.2.9.2.3.5. Update Rate 2.2.9.2.3.6. Default Update Rate 2.2.9.3. Burst Message 3 2.2.9.3.1. Burst Message 2.2.9.3.2. Message Content 2.2.9.3.3. Update Rate 2.2.9.3.3.1. Trigger Mode 2.2.9.3.3.2. Trigger Level 2.2.9.3.3.3. Trigger Level Unit 2.2.9.3.3.4. Classification 2.2.9.3.3.5. Update Rate 2.2.9.3.3.6. Default Update Rate 2.2.9.4. Event Notification 2.2.9.4.1. Event Message 2.2.9.4.2. Unack Update Rate 2.2.9.4.3. Default Update Rate 2.2.9.4.4. Debounce Interval 2.2.9.4.5. Pending Events 2.2.9.4.6. Acknowledge Event (If there are pending events) 2.2.9.5. 12-Point Sample 2.2.9.5.1. Data Sampling 2.2.9.5.2. Device Variable 2.2.9.5.3. Sample Interval 2.2.9.5.4. 12-Point Sample (Data Sampling is not Off) 2.2.9.6. Variable Mapping 2.2.9.6.1. PV is 2.2.9.6.2. SV is 2.2.9.6.3. TV is 2.2.9.6.4. QV is 2.2.9.7. Multidrop 2.2.9.7.1. Polling Address 2.2.9.7.2. Loop Current Mode HART Communications 121 Section 10: hArT Communication December 2014 1066 Instruction Manual LIQ_MAN_1066 2.2.10. Device Display 2.2.10.1. Main Display Format 2.2.10.1.1. Upper 2.2.10.1.2. Center 2.2.10.1.3. Left 2.2.10.1.4. Lower Left 2.2.10.1.5. Right 2.2.10.1.6. Lower Right 2.2.10.2. Display Language 2.2.10.3. Warnings 2.2.10.4. Display Contrast 2.2.11.Security 2.2.11.1. HART Lock 2.2.11.1.1. Lock State 2.2.11.1.2. Lock/Unlock 2.2.11.2. Local Operator Interface 2.2.11.2.1. Configuration Code 2.2.11.2.2. Calibration Code 2.3. Alert Setup 2.3.1. Diagnostics (1066 ph/orp/redox only) 2.3.1.1. Reference Imp 2.3.1.1.1. High Fault Setpoint 2.3.1.2. Glass Impedance (pH only) 2.3.1.2.1. High Fault Setpoint 2.3.1.2.2. Temp Correction 2.3.1.2.3. Measurement Type 3. Service Tools 3.1. Alerts 3.2. Variables 3.3. Trends 3.4. Maintenance 3.4.1. 1066 Do (1066 Do only) 3.4.1.1. Oxygen 3.4.1.2. Temperature 3.4.1.3. Input Current 3.4.1.4. Air Calibration 3.4.1.5. Air Calibration Setup 3.4.1.6. Zero Calibration 3.4.1.7. In-Process Cal 3.4.1.8. Sensitivity@25C 3.4.1.9. Zero Current 3.4.2. 1066 CL /1066 oz (1066 CL /1066 oz only) 3.4.2.1. Chlorine/Ozone 3.4.2.2. Temperature 3.4.2.3. Input Current 3.4.2.4. Zero Calibration 3.4.2.5. In-Process Cal 3.4.2.6. Sensitivity@25C 3.4.2.7. Zero Current 122 HART Communications 1066 Instruction Manual Section 10: hArT Communication LIQ_MAN_1066 December 2014 3.4.3. 1066 ph/orp (ph only) 3.4.3.1. pH 3.4.3.2. pH Buffer Calibration 3.4.3.3. Standardize pH 3.4.3.4. pH Slope 3.4.3.5. Zero Offset 3.4.3.6. Calibration Setup 3.4.3.6.1. Limits 3.4.3.6.1.1. Minimum Slope 3.4.3.6.1.2. Maximum Slope 3.4.3.6.1.3. Maximum Offset 3.4.3.6.2. Automatic Buffer Recognition 3.4.3.6.2.1. Buffer Standard 3.4.3.6.2.2. Stable Time 3.4.3.6.2.3. Stable Delta 3.4.4. 1066 ph/orp (orp/redox only) 3.4.4.1. ORP/Redox 3.4.4.2. Calibrate ORP/Redox 3.4.4.3. Zero Offset 3.4.4.4. Maximum Offset 3.4.5. 1066 C/1066 T (1066 C/1066 T only) 3.4.5.1. Conductivity 3.4.5.2. Raw Conductivity 3.4.5.3. Temperature 3.4.5.4. Zero Calibration 3.4.5.5. In-Process Calibration 3.4.5.6. Cell Constant 3.4.5.7. Cell Factor (4 electrode) 3.4.5.8. Zero Offset 3.4.5.9. Soln Offset (%Concentration) 3.4.6. Temperature 3.4.6.1. Temperature 3.4.6.2. Calibrate Temp 3.4.6.3. RTD Offset 3.4.7. Analog outputs 3.4.7.1. Output 1 3.4.7.1.1. Loop Current 3.4.7.1.2. Calibrate Output 1 3.4.7.2. Output 2 3.4.7.2.1. SV Current 3.4.7.2.2. Calibrate Output 2 3.4.8. Meter 3.4.8.1. Input Resistance 3.4.8.2. Meter Calibration 3.4.9. reset/restore 3.4.9.1. Reset Device 3.4.9.2. Load Default Configuration 3.4.9.3. Reset Configuration Changed 3.5. Simulate 3.5.1. PV (show current PV type label) 3.5.2. Temperature 3.5.3. End Variable Simulation (If any variable is being simulated) 3.5.4. Output 1 3.5.5. Output 2 HART Communications 123 Section 10: hArT Communication 1066 Instruction Manual December 2014 LIQ_MAN_1066 This page left intentionally blank 124 HART Communications 1066 Instruction Manual Section 11: return of Material LIQ_MAN_1066 December 2014 Section 11: Return of Material 11.1 General To expedite the repair and return of instruments, proper communication between the customer and the factory is important. Before returning a product for repair, call 1-949-757-8500 for a Return Materials Authorization (RMA) number. 11.2 Warranty repair The following is the procedure for returning instruments still under warranty: 1. Call Rosemount Analytical for authorization. 2. To verify warranty, supply the factory sales order number or the original purchase order number. In the case of individual parts or sub-assemblies, the serial number on the unit must be supplied. 3. Carefully package the materials and enclose your “Letter of Transmittal” (see Warranty). If possible, pack the materials in the same manner as they were received. 4. Send the package prepaid to: Rosemount Analytical 2400 Barranca Parkway Irvine, CA 92606 Attn: Factory Repair RMA No. ____________ Mark the package: Returned for Repair Model No. ___________ 11.3 IMporTAnT please see second section of “return of Materials request” form. Compliance with the oShA requirements is mandatory for the safety of all personnel. MSDS forms and a certification that the instruments have been disinfected or detoxified are required. non-Warranty repair The following is the procedure for returning for repair instruments that are no longer under warranty: 1. Call Rosemount Analytical for authorization. 2. Supply the purchase order number, and make sure to provide the name and telephone number of the individual to be contacted should additional information be needed. 3. Do Steps 3 and 4 of Section 10.2. noTE Consult the factory for additional information regarding service or repair. Return of Materials 125 EC Declaration of Conformity December 2014 126 1066 Instruction Manual LIQ_MAN_1066 EC Declaration of Conformity 1066 Instruction Manual LIQ_MAN_1066 EC Declaration of Conformity EC Declaration of Conformity December 2014 127 EC Declaration of Conformity 1066 Instruction Manual December 2014 LIQ_MAN_1066 This page left intentionally blank 128 1066 Instruction Manual EC Declaration of Conformity LIQ_MAN_1066 December 2014 This page left intentionally blank 129 LIQ_MAN_1066 Rev. G December 2014 facebook.com/EmersonRosemountAnalytical 8 AnalyticExpert.com Credit Cards for U.S. Purchases Only. twitter.com/RAIhome youtube.com/user/RosemountAnalytical Emerson process Management ©2013 Rosemount Analytical, Inc. All rights reserved. 2400 Barranca Parkway Irvine, CA 92606 USA Tel: (949) 757-8500 Fax: (949) 474-7250 The Emerson logo is a trademark and service mark of Emerson Electric Co. Brand name is a mark of one of the Emerson Process Management family of companies. All other marks are the property of their respective owners. rosemountanalytical.com © Rosemount Analytical Inc. 2013 The contents of this publication are presented for information purposes only, and while effort has been made to ensure their accuracy, they are not to be construed as warranties or guarantees, express or implied, regarding the products or services described herein or their use or applicability. All sales are governed by our terms and conditions, which are available on request. 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