Emerson 397 TUpH pH/ORP Sensor Instruction Sheet
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Instruction Manual LIQ_MAN_ABR_397 397 November 2013 TUpH pH Sensors For additional information, please refer visit our website at www.rosemountanalytical.com. Specifications 397 Performance and Physical Specifications CAUTION Sensor/Process Application Compatibility pH Range: AccuGlass: 0–14 pH Wetted Materials: glass, polypropylene, EP Interconnecting Cable: 15 ft (4.6 m), for use with remote preamplifier Temperature Rating: 0 to 100 °C (32 to 176 °F) Pressure Range: 100–790 kPa abs (0–100 psig) Minimum Conductivity: 75 μS/cm, nominal 100 μS/cm Weight/Shipping Weight: 0.45 kg/0.9 kg (1 lb/2 lb) Process Connections: NONE; must use Quik-Loc Kit which includes a 1 in. MNPT Process Connection The wetted sensor materials may not be compatible with process composition and operating conditions. Application compatibility is entirely the responsibility of the user. Quick-Loc Kit Physical Specifications Process Connections: 1-in. MNPT Wetted Materials: 316 SST, EP, PEEK Weight/Shipping Weight: 0.45 kg/0.9 kg (1 lb/2 lb) Storage WARNING Before removing the sensor, be absolutely certain that the process pressure is reduced to 0 psig and the process temperature is lowered to a safe level! ATEX DIRECTIVE Special Conditions for safe use 1. All pH/ORP sensors have a plastic enclosure which must only be cleaned with a damp cloth to avoid the danger due to a build up of an electrostatic charge. 2. All pH/ORP sensor Models are intended to be in contact with the process fluid and may not meet the 500V r.m.s. a.c. test to earth. This must be taken into consideration at installation 1. It is recommended that electrodes be stored in their original shipping containers until needed. 2. Do not store at temperatures below -5 °C (23 °F). 3. Electrodes should be stored with a protective cap containing KCl solution. 4. For overnight storage, immerse the sensor in tap water or 4 pH buffer solution. 5. A pH glass electrode has a limited shelf life of one year. Sensor Installation Electrode Preparation For recommended installation, see Figure 2 1. Remove electrode from shipping container. 2. Remove the protective boot covering the electrode bulb. 3. Rinse away salt film with clean water, then shake the electrode so that the internal solution fills the bulb, thus removing any air trapped there. Note Do not allow lubricant to coat electrode bulb or reference junction. If it does, wipe it clean before installation. For sensor dimensions, see Figure 1. For wiring, see Figures 3 - 13. 397 November 2013 Instruction Manual LIQ_MAN_ABR_397 Figure 1. Dimensional Drawings For the 397 in the Quik-Loc Unit DWG. No. REV. 40039702 C Note The EP gasket (see drawing #40039702) provided with the coupler should be periodically inspected. If gasket shows signs of corrosion, replacement will be necessary to ensure a proper and secure seal between the coupler and adapter. Quik-Loc Kit 23757-00 23757-01 2 A Sensor Length 6.15 in. / 156 mm DWG. No. REV. 40039704 B DWG. No. REV. 40039701 C B Insertion Depth 1.4 in. / 35 mm 2.0 in. / 50 mm Instruction Manual LIQ_MAN_ABR_397 397 November 2013 Quick-Loc Mounting Wrap the pipe threads of the coupler with Teflon tape before placing it into the process pipe. The coupler can be connected to any 1 in. process connection and must be mounted within 80° of vertical, with the electrode facing down. Once the coupler is in place, the adapter should be positioned onto the back end of the sensor. Remove the parafilm wrapping from the two 0-rings on the sensor, grease the o-rings with the lube provided, and feed the sensor cable through the adapter. Once the adapter is slipped over the sensor’s back end, the retaining ring (which is included with every 397 sensor) should be installed on the black, grooved, back end of the sensor body. The retaining ring secures the sensor into the adapter. The adapter/sensor assembly is now ready to be inserted into the coupler. With both arms of the coupler in the released position, insert the adapter/sensor assembly into the coupler. Note The adapter can not be inserted completely or properly unless both arms are in the fully released position (see Figure 1). Once the adapter has been properly placed in the coupler, both arms should be positioned in the locked position. Note SAFETY WARNING It is recommended that a thermometer, drain valve to relieve pressure, and pressure gauge be inserted near the Quik-Loc assembly (see Figure 2). WARNING Once the Quik-Loc unit is installed the operator should wait for the process to cool to a safe temperature, use the pressure drain valve to relieve all process pressure and observe the pressure on the pressure gauge for proper removal of the sensor without spray or bodily injury. The Quik-Loc kit used with the 397 TUpH sensor is not recommended for use with hazardous, corrosive, or strong oxidizing chemicals due to a risk of spray or bodily injury. SAFETY WARNING It is the responsibility of each company using the QuikLoc Kit/ 397 TUpH Sensor to train personnel of the injury risks associated with using a quick-release coupler that is placed in a hot or pressurized process. Once the arms of the coupler have been locked in position, use tamper-evident safety wire on the metal rings of the coupler arms to prevent unauthorized and/or untrained personnel from using the Quik-Loc unit. The Quik-Loc unit should be used only within the pressure and temperature limits stated for the 397 sensor. The sensor may obstruct flow through smaller pipes. Figure 2. Recommended Flow-Through and Insertion Installation for the 397 DWG. No. REV. 40039703 B 3 397 November 2013 Instruction Manual LIQ_MAN_ABR_397 Note For additional wiring information on this product, including sensor combinations not shown here, please refer to either our online wiring programs or the Manual DVD enclosed with each product. 1056, 1057, 56, 5081, 6081, 54e, and XMT : http://www3.emersonprocess.com/raihome/sp/liquid/wiring/XMT/ 1066 and sensors with SMART preamps: http://www2.emersonprocess.com/en-US/brands/rosemountanalytical/Liquid/Sensors/ Pages/Wiring_Diagram.aspx 1055: http://www3.emersonprocess.com/raihome/sp/liquid/wiring/1055/ Figure 3. 397 Standard Wiring Option used with 1054A, 1054B, 2054, and Preamplifiers PN 22698-02 and 22698-03 Figure 5. Wiring to 1181 pH Analyzer. 4 Figure 4. The 397 Option -62 for Wiring to 1054, 1055, 1181, 2081, 54, 54e, 81, 3081, 4081, 5081-P, Xmt-P, SoluComp, and 2700 Preamplifier (PN 23054-03). Also for use with remote Junction Box PN 23555-00. Instruction Manual LIQ_MAN_ABR_397 397 November 2013 Figure 6. Preparing Coax Cable for Wiring to 54e, 1055, 81, 2081, 3081, 4081, 5081, and Xmt. Figure 7. Wiring to 2081 Figure 8. Wiring to 54e, 81, 3081, 4081, and 5081 Figure 9. Wiring to Xmt-P-XX-10 5 397 November 2013 Figure 10. Wiring to 1054A, 1054B, and 2054 Figure 11. Wiring through Junction Box PN 23309-04 (03) and Remote Preamplifier 6 Instruction Manual LIQ_MAN_ABR_397 Instruction Manual LIQ_MAN_ABR_397 397 November 2013 Figure 12. Wiring to 1055-01-10-22-32 Figure 13. Wiring to 1055-11-22-32 through a Remote Junction Box 7 397 Instruction Manual November 2013 LIQ_MAN_ABR_397 Rev. G Two Point Buffer Calibration Select two stable buffer solutions (at least two pH units apart), preferably pH 4.0 and 10.0. Note A pH 7 buffer solution reads a mV value of approx. zero, and pH buffers read approximately ± 59.1 mV for each pH unit above or below pH 7. Check the pH buffer manufacturer specifications for millivolt values at various temperatures since it may affect the actual value of the buffer solution mV/pH value. 1. Immerse sensor in the first buffer solution. Allow sensor to equilibrate to the buffer temperature (to avoid errors due to temperature differences between the buffer solution and sensor temperature) and wait for reading to stabilize. Value of buffer can now be acknowledged by analyzer/transmitter. 2. Once the first buffer has been acknowledged by the analyzer/transmitter, rinse the buffer solution off of the sensor with distilled or deionized water. 3. Repeat steps 1 and 2 using the second buffer solution. 4. The theoretical slope value, according to the Nernst equation for calculating pH, is approximately 59.17 mV/pH. Over time the sensor will age, both in the process and in storage, and will result in reduced slope values. To ensure accurate readings, it is recommended that the electrode be replaced when the slope value falls below 47 to 49 mV/pH. Recommended pH Sensor Standardization For maximum accuracy, the sensor can be standardized on-line or with a process grab sample after a buffer calibration has been performed and the sensor has been conditioned to the process. Standardization accounts for the sensor junction potential and other interferences. Standardization will not change the sensor’s slope but will simply adjust the analyzer’s reading to match that of the known process pH. Maintenance Electrodes should respond rapidly. Sluggishness, offsets, and erratic readings are indicators that the electrodes may need cleaning or replacement. 1. To remove oil deposit, clean the electrode with a mild non-abrasive detergent. 2. To remove scale deposits, soak electrodes for 30 to 60 minutes in a 5% hydrochloric acid solution. 3. Temperature effect on life expectancy: If glass electrode life expectancy is 100% @ 25 °C (77 °F), then it will be approximately 25% @ 80 °C (176 °F), and approximately 5% @ 120 °C (248 °F). facebook.com/EmersonRosemountAnalytical AnalyticExpert.com 8 Credit Cards for U.S. Purchases Only. twitter.com/RAIhome youtube.com/user/RosemountAnalytical ©2013 Rosemount Analytical, Inc. All rights reserved. Emerson Process Management 2400 Barranca Parkway Irvine, CA 92606 USA Tel: (949) 757-8500 Fax: (949) 474-7250 rosemountanalytical.com © Rosemount Analytical Inc. 2013 The Emerson logo is a trademark and service mark of Emerson Electric Co. Brand name is a mark of one of the Emerson Process Management family of companies. All other marks are the property of their respective owners. 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